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    • 7. 发明专利
    • Method and apparatus for manufacturing silicon carbide single crystal
    • 用于制造单晶碳化硅的方法和装置
    • JP2011219336A
    • 2011-11-04
    • JP2010092960
    • 2010-04-14
    • Denso CorpToyota Central R&D Labs IncToyota Motor Corpトヨタ自動車株式会社株式会社デンソー株式会社豊田中央研究所
    • URAGAMI YASUSHIKONDO HIROYUKIADACHI AYUMIGUNJISHIMA TSUKURU
    • C30B29/36
    • PROBLEM TO BE SOLVED: To provide an apparatus for manufacturing a silicon carbide single crystal which allows to supply an appropriate amount of carbon atoms to a SiC single crystal while suppressing mixing of an inclusion (a large mass) of carbon powder discharged from a crucible with the SiC single crystal.SOLUTION: In a hollow of a crucible 4, a cylindrical material 10 which has a diameter smaller than the inner diameter of a container body 2 and is made of metal carbide is disposed apart from an inner wall 2a of the container body 2 along the inner wall 2a on a powder raw material 8. While, on a lid member 3, a coating film 3b of metal carbide is formed on the side of the container body 2 from a seed crystal 7 of an inner wall 3a of the lid member 3. This suppresses discharge of masses of carbon powder from the lid member 3, and an appropriate amount of the carbon powder discharged from the inner wall 2a of the container body 2 is supplied to the SiC single crystal 9 during growth.
    • 要解决的问题:提供一种用于制造碳化硅单晶的装置,其允许向SiC单晶提供适量的碳原子,同时抑制从碳化硅单晶排出的夹杂物(大量)的碳粉的混合 具有SiC单晶的坩埚。 解决方案:在坩埚4的中空中,直径小于容器主体2的内径并且由金属碳化物制成的圆柱形材料10与容器主体2的内壁2a分开设置 沿着内壁2a在粉末原料8上。同时,在盖构件3上,从容器主体2的内壁3a的晶种7形成金属碳化物的涂膜3b 从而抑制碳粉末从盖部件3的排出,在生长时向碳化硅单晶9供给适当量的从容器主体2的内壁2a排出的碳粉末。 版权所有(C)2012,JPO&INPIT
    • 8. 发明专利
    • Method for producing silicon carbide single crystal
    • 生产碳化硅单晶的方法
    • JP2011219294A
    • 2011-11-04
    • JP2010088627
    • 2010-04-07
    • Denso CorpToyota Central R&D Labs IncToyota Motor Corpトヨタ自動車株式会社株式会社デンソー株式会社豊田中央研究所
    • KONDO HIROYUKIADACHI AYUMIGUNJISHIMA TSUKURU
    • C30B29/36C30B23/06
    • PROBLEM TO BE SOLVED: To provide a method for producing a SiC single crystal, by which cracking and distortion of the SiC single crystal are suppressed.SOLUTION: In the method for producing a SiC single crystal, projection growth wherein the SiC single crystal 6 is grown to have such a projection shape that the central part of the SiC single crystal 6 is projected from the outer edge part and recess growth wherein the central part of the SiC single crystal 6 is recessed from the outer edge part are performed in order. A tensile stress is generated in the vicinity of the central part of the SiC single crystal 6 and a compression stress is generated in the outer edge part during the projection growth, and a compression stress is generated in the vicinity of the central part of the SiC single crystal 6 and a tensile stress is generated in the outer edge part during the recess growth. Then, a reverse stress is generated when the SiC single crystal 6 is cooled. Thereby, when the SiC single crystal 6 is cooled, a region where both of the compression stress and tensile stress are generated is provided in the vicinity of the central part of the SiC single crystal 6, and a region where both of the compression stress and tensile stress are generated is provided similarly in the outer edge part. Consequently, it is possible to suppress cracking and distortion of the SiC single crystal during cooling.
    • 待解决的问题:提供一种SiC单晶的制造方法,其中SiC单晶的破裂和变形被抑制。 解决方案:在SiC单晶的制造方法中,SiC单晶6生长为具有使SiC单晶6的中央部从外缘部突出的突起形状的突起生长和凹部 其中SiC单晶6的中心部分从外边缘部分凹陷的生长依次进行。 在SiC单晶6的中央部附近产生拉伸应力,在投影生长期间在外缘部产生压缩应力,在SiC的中心部附近产生压缩应力 单晶6,并且在凹部生长期间在外边缘部分产生拉伸应力。 然后,当SiC单晶6被冷却时产生反向应力。 因此,当SiC单晶6被冷却时,在SiC单晶6的中央部附近设置压缩应力和拉伸应力两者的区域,压缩应力和 在外边缘部分类似地设置拉伸应力。 因此,可以抑制冷却时SiC单晶的开裂和变形。 版权所有(C)2012,JPO&INPIT