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1. 发明授权

US5164442A Rubber composition 失效
公开(公告)号：US5164442A
公开(公告)日：1992-11-17
申请号：US504364
申请日：1990-04-04
申请人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura , Hiroyuki Ohata , Harukazu Okuda
发明人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura , Hiroyuki Ohata , Harukazu Okuda
IPC分类号： C08F283/12 , C08K3/00 , C08K5/00 , C08K13/02 , C08L51/08 , C08L83/10
CPC分类号： C08L83/10 , C08F283/122 , C08K13/02 , C08L51/085
摘要： The polymeric ingredient of the inventive rubber composition is an acrylic polymer modified with a mercapto-containing organopolysiloxane as prepared by the emulsion polymerization of an acrylic monomer in an aqueous emulsion of the organopolysiloxane. Characteristically, the acrylic monomer is copolymerized with another monomer having an active halogen atom or an epoxy group. By virtue of this unique formulation of the rubbery polymer, the inventive rubber composition prepared by compounding the rubbery polymer with a reinforcing filler and a specified curing or crosslinking agent can be vulcanized to give a vulcanizate having excellent mechanical properties, heat resistance, oil resistance and cold resistance as a combination of the features of silicone rubbers and acrylic rubbers.

2. 发明授权

US5059648A Rubber composition 失效
标题翻译：橡胶组合物
公开(公告)号：US5059648A
公开(公告)日：1991-10-22
申请号：US427049
申请日：1989-10-25
申请人： Motoo Fukushima , Tsutomu Nakamura , Hiroyuki Ohata , Harukazu Okuda
发明人： Motoo Fukushima , Tsutomu Nakamura , Hiroyuki Ohata , Harukazu Okuda
IPC分类号： C08K5/05 , C08L21/00 , C08L83/10
CPC分类号： C08L21/00 , C08F265/04 , C08F283/124 , C08K5/05 , C08L23/16 , C08L83/10 , C08K3/04 , C08K3/36 , C08L2205/03 , C08L7/00 , C08L71/02
摘要： A rubber composition based on a rubbery polymer and a silica-based reinforcing filler can be imparted with a greatly improved workability in roll milling and molding as well as in the mechanical properties of the vulcanizates prepared therefrom when the rubber composition is admixed with an acetylene alcohol or an alkylene-oxide adduct of acetylene alcohol presumably by virtue of the improvement in the dispersibility of the reinforcing filler in the rubbery matrix. The improvement obtained by the addition of the acetylene alcohol compound is not limited to the dispersibility of silica fillers but also to the dispersibility of carbon black when the rubbery polymer is an organopolysiloxane-modified acrylic polymer.

3. 发明授权

US4722975A Crosslinkable copolymer composition and a method for the preparation thereof 失效
标题翻译：可交联共聚物组合物及其制备方法
公开(公告)号：US4722975A
公开(公告)日：1988-02-02
申请号：US800433
申请日：1985-11-21
申请人： Kunio Itoh , Yasuo Tarumi , Tsutomu Nakamura , Hiroyuki Ohata , Tsutomu Matsuo , Harukazu Okuda
发明人： Kunio Itoh , Yasuo Tarumi , Tsutomu Nakamura , Hiroyuki Ohata , Tsutomu Matsuo , Harukazu Okuda
IPC分类号： C08F8/42
CPC分类号： C08F8/42
摘要： The inventive copolymer composition is satisfactorily curable or vulcanizable into, for example, a rubbery elastomer even by an organic peroxide contained therein as a crosslinking agent. The crosslinkable copolymer comprised therein is a polymer having, in a molecule, at least two monomeric units each having a vinyl-containing organosilicon pendant group represented by the general formula (Vi.sub.m R.sup.1.sub.n SiO).sub.a Vi.sub.b R.sup.2.sub.c Si--, in which Vi is a vinyl group, R.sup.1 is a hydrogen atom or a group selected from the class consisting of monovalent hydrocarbon groups free from aliphatic unsaturation, hydroxy group and hydrolyzable groups excepting halogen atoms, R.sup.2 is a hydrogen atom or a monovalent hydrocarbon group, m is 1, 2 or 3, n is zero, 1 or 2, a is 1, 2 or 3, b is zero, 1 or 2 and c is zero, 1 or 2 with the proviso that a+b=1, 2 or 3 and a+b+c=3. Such a copolymer can be prepared by the copolymerization of a first ordinary ethylenically unsaturated monomer and a second monomer having, simultaneously in a molecule, an ethylenically unsaturated linkage copolymerizable with the first monomer and the vinyl-containing organosilicon group of the above given formula.
摘要翻译：本发明的共聚物组合物甚至可以通过其中含有的有机过氧化物作为交联剂令人满意地固化或硫化成例如橡胶弹性体。包含在其中的可交联共聚物是分子中具有至少两个单体单元的聚合物，每个单体单元具有由通式（VimR1nSiO）aVibR2cSi-表示的含乙烯基的有机硅侧基，其中Vi是乙烯基，R1是氢原子或选自不含脂肪族不饱和键的一价烃基，羟基和除卤素原子外的可水解基团的基团，R 2为氢原子或一价烃基，m为1,2或3，n为0 ，1或2，a为1,2或3，b为0,1或2，c为0,1或2，条件是a + b = 1,2或3，a + b + c = 3。这种共聚物可以通过共聚第一普通烯键式不饱和单体和第二单体来制备，该单体在分子中同时具有可与上述给定式的第一单体和含乙烯基的有机硅基团共聚的烯属不饱和键。

4. 发明授权

US06414078B1 Conductive silicone rubber composition 失效
标题翻译：导电硅橡胶组合物
公开(公告)号：US06414078B1
公开(公告)日：2002-07-02
申请号：US09680282
申请日：2000-10-06
申请人： Motoo Fukushima , Tsutomu Nakamura , Mikio Iino
发明人： Motoo Fukushima , Tsutomu Nakamura , Mikio Iino
IPC分类号： C08K308
CPC分类号： H01B1/22 , C08G77/20 , C08K2201/013 , C08L83/04 , Y10T428/12028 , C08L83/00 , C08L2666/54
摘要： In a silicone rubber composition comprising an organopolysiloxane having at least two aliphatic unsaturated groups and a curing agent, metallized particles of inorganic material or organic resin are effectively dispersed to give a conductive composition which cures into a conductive silicone rubber part having a low and stable volume resistivity.
摘要翻译：在包含具有至少两个脂族不饱和基团的有机聚硅氧烷和固化剂的硅橡胶组合物中，无机材料或有机树脂的金属化颗粒被有效地分散，得到固化成具有低且稳定体积的导电硅橡胶部分的导电组合物电阻率。

5. 发明授权

US06469090B2 Electrically conductive liquid silicone rubber composition 失效
标题翻译：导电液体硅橡胶组合物
公开(公告)号：US06469090B2
公开(公告)日：2002-10-22
申请号：US09760796
申请日：2001-01-17
申请人： Syuuichi Azechi , Tsutomu Nakamura , Motoo Fukushima
发明人： Syuuichi Azechi , Tsutomu Nakamura , Motoo Fukushima
IPC分类号： C08K331
CPC分类号： H01B1/22 , B29K2083/005 , Y10T428/12028
摘要： An electrically conductive liquid silicone rubber composition having (A) 100 parts by weight of an organopolysiloxane having a viscosity of 10-100,000 centipoise at 25° C., (B) 1-100 parts by weight of a finely divided silica powder, (C) 30-700 parts by weight of a metal powder or an electrically conductive metal-plated powder, and (D) a curing agent in an amount sufficient to cure the organopolysiloxane. The composition has a low volumetric resistivity, a stable electrical resistance and can be injection-molded and cured to give an outstanding silicone rubber that is useful in electrical components and electrical contacts employed in high-conductivity applications.
摘要翻译：一种导电液体硅橡胶组合物，其具有（A）100重量份在25℃粘度为10-100,000厘泊的有机聚硅氧烷，（B）1-100重量份的细碎二氧化硅粉末（C ）30-700重量份的金属粉末或导电金属镀粉末，和（D）固化剂，其量足以固化有机聚硅氧烷。该组合物具有低体积电阻率，稳定的电阻，并且可以注塑和固化，得到优异的硅橡胶，其可用于高导电性应用中使用的电气部件和电接触。

6. 发明授权

US4876344A Novel organosilicon compounds 失效
标题翻译：新型有机硅化合物
公开(公告)号：US4876344A
公开(公告)日：1989-10-24
申请号：US277632
申请日：1988-11-29
申请人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura
发明人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura
IPC分类号： C07D251/38 , C07F7/18 , C08G59/40 , C08K5/548
CPC分类号： C07F7/1816 , C07D251/38 , C08K5/548
摘要： Organosilicon compounds of the following formula, or hydrolyzates thereof, ##STR1## ps in which Rhu 1 l and Rhu 2 l are independently a hydrogen atom or an alkyl group having from 1 to 8 carbon atoms, m is an integer of from 1 to 8, and n is an integer of from 1 to 3. The compound is useful as a vulcanizing agent particularly for vulcanizable elastomer compositions comprising inorganic fillers.
摘要翻译：下式的有机硅化合物或其水解产物，其中R 1和L 2独立地为氢原子或具有1至8个碳原子的烷基，m为1至8的整数，n为1〜3的整数。该化合物特别用于含有无机填料的可硫化弹性体组合物，可用作硫化剂。

7. 发明授权

US4761452A Oil-resistant rubber composition 失效
标题翻译：耐油橡胶组合物
公开(公告)号：US4761452A
公开(公告)日：1988-08-02
申请号：US883535
申请日：1986-07-09
申请人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura
发明人： Kunio Itoh , Motoo Fukushima , Tsutomu Nakamura
IPC分类号： C08L23/00 , C08K3/00 , C08L23/16 , C08L33/00 , C08L33/04 , C08L33/08 , C08L43/04
CPC分类号： C08L43/04 , C08L23/16 , C08L2312/08
摘要： A rubber composition capable of giving a highly oil-resistant vulcanizate with an organic peroxide as the vulcanizing agent is proposed. The composition is a blend of an EPM or EPDM rubber and an acrylic rubber loaded with a reinforcing filler, of which the latter rubber is a copolymer having at least two vinylsilyl groups in a molecule as the pendant groups introduced by the copolymerization of one or more acrylic monomers with a vinylsilyl-containing organosilicon compound having an aliphatically unsaturated group copolymerizable with the acrylic monomers in a molecule, such as CH.sub.2 .dbd.CH--CO--O--CH.sub.2 CH.sub.2 CH.sub.2 --Si-- and CH.sub.2 .dbd.CH--C.sub.6 H.sub.4 --Si--. The covulcanizate has the high mechanical strengths of the EPM or EPDM rubber and the high oil resistance of the acrylic rubber in combination.
摘要翻译：提出了能够以有机过氧化物作为硫化剂赋予高耐油硫化橡胶的橡胶组合物。该组合物是EPM或EPDM橡胶和装载有增强填料的丙烯酸橡胶的共混物，其中后者橡胶是在分子中具有至少两个乙烯基甲硅烷基的共聚物，作为通过一个或多个丙烯酸类单体与具有乙烯基甲硅烷基的有机硅化合物在分子中具有可与丙烯酸单体共聚的脂族不饱和基团，例如CH 2 = CH-CO-O-CH 2 CH 2 CH 2 -Si-和CH 2 = CH-C 6 H 4 -Si。共硫化橡胶具有EPM或EPDM橡胶的高机械强度和丙烯酸橡胶的高耐油性组合。

8. 发明授权

US09287027B2 Rare earth metal-based permanent magnet 有权
标题翻译：稀土金属永磁体
公开(公告)号：US09287027B2
公开(公告)日：2016-03-15
申请号：US12990341
申请日：2008-05-14
申请人： Yukimitsu Miyao , Tsutomu Nakamura
发明人： Yukimitsu Miyao , Tsutomu Nakamura
IPC分类号： H01F1/057 , B32B15/04 , C22C9/00 , C22C13/00 , H01F41/02
CPC分类号： H01F1/0577 , C22C9/00 , C22C13/00 , H01F41/026 , Y10T428/32 , Y10T428/325
摘要： An objective of the present invention is to provide a rare earth metal-based permanent magnet with improved adhesion properties. A rare earth metal-based permanent magnet of the present invention as a means for achieving the objective has a laminated plating film, and is characterized in that the plating film comprises as an outermost surface layer a SnCu alloy plating film having a film thickness in a range from 0.1 μm to 2 μm, the composition of the SnCu alloy plating film is 35 mass % or more but less than 55 mass % of Sn and the rest being Cu, and a base plating film having two or more layers including at least a Ni plating film and a Cu plating film which are formed as the lower layer under the SnCu alloy plating film, and among the base plating film, the Ni plating film is located just below the SnCu alloy plating film. A joined structure fabricated using the rare earth metal-based permanent magnet of the present invention exhibits favorable initial adhesion strength when combined with a silicone-based adhesive, and is less deteriorated in adhesion strength even after a moisture resistance test.
摘要翻译：本发明的目的是提供一种具有改进的粘合性能的稀土金属基永磁体。本发明的稀土金属类永磁体作为实现目的的手段具有叠层电镀膜，其特征在于，所述镀膜包含作为最外表面层的SnCu合金镀膜，膜厚度为在0.1μm〜2μm的范围内，SnCu合金镀膜的成分为Sn的35质量％以上且小于55质量％，其余为Cu，并且具有两层以上的基底镀膜至少含有 Ni镀覆膜和Cu电镀膜，在SnCu合金镀膜之下形成为下层，并且在底镀膜中，Ni镀膜位于SnCu合金镀膜的正下方。使用本发明的稀土类金属类永磁体制造的接合结构，与硅酮类粘合剂组合时，表现出良好的初期粘合强度，即使在耐湿试验之后，粘合强度也劣化。

9. 发明授权

US08907001B2 Use of a pretreated precipitated silica as a reinforcing filler for silicon elastomer and the curable silicone elastomer compositions thus obtained by cold mixing 有权
标题翻译：使用预处理的沉淀二氧化硅作为硅弹性体的增强填料和通过冷混合获得的可固化的硅氧烷弹性体组合物
公开(公告)号：US08907001B2
公开(公告)日：2014-12-09
申请号：US12461283
申请日：2009-08-06
申请人： Agnès Pottier , Kyu-Min Hwang , Minoru Igarashi , Tsutomu Nakamura , Nahohiko Harada
发明人： Agnès Pottier , Kyu-Min Hwang , Minoru Igarashi , Tsutomu Nakamura , Nahohiko Harada
IPC分类号： C08K9/06
CPC分类号： C08K9/06
摘要： The invention relates to the use of a precipitated silica, pretreated by at least one organosilane hydrophobic compound or one hydrophobic silicone oil, as a reinforcing filler for silicone elastomer, the pretreated silica being incorporated in the silicone elastomer by cold mixing and having the following features: —a BET specific surface ranging from 50 to 450 m2/g, —a water wettability lower than 80, —a sulfur content lower than 0.1% by weight. The invention is directed to the curable silicone elastomer composition thus obtained.
摘要翻译：本发明涉及使用由至少一种有机硅烷疏水化合物或一种疏水性硅油预处理的沉淀二氧化硅作为有机硅弹性体的增强填料，预处理的二氧化硅通过冷混合而结合在有机硅弹性体中，具有以下特征： - BET比表面积为50-450m2 / g， - 水润湿性低于80， - 硫含量低于0.1％（重量）。本发明涉及由此获得的可固化的硅氧烷弹性体组合物。

10. 发明授权

US08784748B2 Dry test strip for measuring calcium 有权
标题翻译：用于测量钙的干试纸
公开(公告)号：US08784748B2
公开(公告)日：2014-07-22
申请号：US13457291
申请日：2012-04-26
申请人： Tsutomu Nakamura
发明人： Tsutomu Nakamura
IPC分类号： G01N33/52 , G01N33/84
CPC分类号： G01N33/526 , G01N33/523 , G01N33/84
摘要： A dry test strip for measuring calcium is comprising a support, a reagent layer provided on the support, and a reagent holding layer provided on the reagent layer, and containing, as reagents, o-cresolphthalene complexone, a magnesium selective masking agent, and a pH buffer for adjusting the pH of the environment for reaction of the o-cresolphthalene complexone with calcium to 10.0-11.0, wherein such reagents are present in either the reagent layer or the reagent holding layer or the both layers.
摘要翻译：用于测量钙的干试条包括载体，设置在载体上的试剂层和设在试剂层上的试剂保持层，并含有作为试剂的邻甲酚酞配合物，镁选择性掩蔽剂和用于调节邻甲酚酞配合物与钙的反应环境pH至10.0-11.0的pH缓冲剂，其中这些试剂存在于试剂层或试剂保持层或两层中。

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