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1. 发明授权

US5188130A Chemical heat source comprising metal nitride, metal oxide and carbon 失效
标题翻译：化学热源包含金属氮化物，金属氧化物和碳
公开(公告)号：US5188130A
公开(公告)日：1993-02-23
申请号：US443636
申请日：1989-11-29
申请人： Mohammad R. Hajaligol , Seetharama C. Deevi , Sarojini D. Ariprala , Donald B. Losee , Bruce E. Waymack , Michael L. Watkins
发明人： Mohammad R. Hajaligol , Seetharama C. Deevi , Sarojini D. Ariprala , Donald B. Losee , Bruce E. Waymack , Michael L. Watkins
IPC分类号： A24F47/00 , A24B15/16 , C01B21/06 , C09K5/00 , C09K5/16
CPC分类号： A24B15/165 , C09K5/16
摘要： A chemical heat source comprising metal nitride, metal oxide and carbon, particularly useful in smoking articles, and methods of making the heat source are provided. The metal nitride of the heat source has an ignition temperature substantially lower than conventional carbonaceous heat sources, while at the same time provides sufficient heat to release a flavored aerosol from a flavor bed for inhalation by the smoker. Upon combustion the heat source produces virtually no carbon monoxide. The metal nitride is prepared by pre-forming the starting materials into a desired shape, and converting them to metal nitride in situ, without substantially altering the shape of the starting materials.

2. 发明授权

US5322075A Heater for an electric flavor-generating article 失效
标题翻译：加热器用于电动香料生成物品
公开(公告)号：US5322075A
公开(公告)日：1994-06-21
申请号：US943318
申请日：1992-09-10
申请人： Seetharama C. Deevi , Mohammad R. Hajaligol , Herbert Herman , Charles T. Higgins , Michael L. Watkins , Bruce E. Waymack , Sung Yi
发明人： Seetharama C. Deevi , Mohammad R. Hajaligol , Herbert Herman , Charles T. Higgins , Michael L. Watkins , Bruce E. Waymack , Sung Yi
IPC分类号： A24F47/00 , H05B3/44 , A24F1/22
CPC分类号： A24F47/008 , H05B3/44
摘要： A smoking article is provided in which a flavor-generating medium is heated electrically to release an aerosol for inhalation by a consumer. The smoking article includes a heater having resistive heating elements printed on a flexible substrate. The heater can be manufactured by circuit board mass production techniques, and can be formed to fit inside an article of the same shape and size as a conventional cigarette. Alternatively, the heater comprises an array of heating elements onto which charges of flavor-generating medium are deposited. The heating elements are connected in a manner which allows the temperature increase in the heater to be concentrated in individually selected heating elements, and requires a minimal number of electrical conductors.
摘要翻译：提供了一种吸烟制品，其中产生香味的介质被电加热以释放用于消费者吸入的气溶胶。吸烟制品包括加热器，其具有印刷在柔性基底上的电阻加热元件。加热器可以通过电路板批量生产技术制造，并且可以形成为适合与常规香烟相同形状和尺寸的制品内部。或者，加热器包括加热元件的阵列，在其上沉积味道产生介质的电荷。加热元件以允许加热器中的温度升高集中在单独选择的加热元件中并且需要最少数量的电导体的方式连接。

3. 发明授权

US5240014A Catalytic conversion of carbon monoxide from carbonaceous heat sources 失效
标题翻译：来自碳源的一氧化碳的催化转化
公开(公告)号：US5240014A
公开(公告)日：1993-08-31
申请号：US556732
申请日：1990-07-20
申请人： Seetharama C. Deevi , Mohammad R. Hajaligol , Diane S. Kellogg , Bruce E. Waymack
发明人： Seetharama C. Deevi , Mohammad R. Hajaligol , Diane S. Kellogg , Bruce E. Waymack
IPC分类号： A24D3/16 , A24B15/16 , A24F47/00 , C01B31/00
CPC分类号： A24F47/004 , A24B15/165
摘要： An improved carbonaceous heat source suitable for use in a smoking article is provided. The heat source is formed by mixing a carbon component, a catalytic precursor and a binder, forming the mixture into a shape, and supplying heat to the mixture. Upon combustion of the heat source, the catalytic precursor forms a catalyst that converts carbon monoxide produced during combustion of the heat source into a benign substance.

4. 发明授权

US5247949A Method for producing metal carbide heat sources 失效
标题翻译：生产金属碳化物热源的方法
公开(公告)号：US5247949A
公开(公告)日：1993-09-28
申请号：US639241
申请日：1991-01-09
申请人： Seetharama C. Deevi , Mohammad R. Hajaligol , Donald B. Losee, Jr.
发明人： Seetharama C. Deevi , Mohammad R. Hajaligol , Donald B. Losee, Jr.
IPC分类号： A24D1/18 , A24B15/16 , A24F47/00 , C01B31/00 , C01B31/30 , C06B43/00 , C10L5/40
CPC分类号： C10L5/40 , A24B15/165 , A24F47/004 , Y02E50/30
摘要： This invention relates to a heat source comprising metal carbide and a method for preparing the same using a reducing/carbidizing atmosphere. The metal carbide heat sources of this invention have ignition temperatures that are substantially lower than conventional carbon particles normally used in carbonaceous heat sources, while at the same time provide sufficient heat to release a flavored aerosol from a flavor bed for inhalation by the smoker. Upon combustion, the heat sources produce substantially no carbon monoxide.

5. 发明授权

US5468936A Heater having a multiple-layer ceramic substrate and method of fabrication 失效
标题翻译：具有多层陶瓷基板的加热器及其制造方法
公开(公告)号：US5468936A
公开(公告)日：1995-11-21
申请号：US35733
申请日：1993-03-23
申请人： Seetharama C. Deevi , Mohammad R. Hajaligol , Pamela D. Lieberman , Walter A. Nichols , Michael L. Watkins
发明人： Seetharama C. Deevi , Mohammad R. Hajaligol , Pamela D. Lieberman , Walter A. Nichols , Michael L. Watkins
IPC分类号： H05B3/14 , H05B3/16 , H05B3/26
CPC分类号： H05B3/141
摘要： A heater having a multiple-layer ceramic substrate and a method for fabricating the heater are provided. The heater consists-of a plurality of ceramic layers which are laminated to form a single ceramic substrate. A plurality of resistive heating elements are deposited onto the multiple-layer ceramic substrate, which are connectable to a power source via conductive elements which extend through the substrate to the resistive heating elements. The heater may also include a terminal that allows for convenient electrical and mechanical interfacing to a smoking article.
摘要翻译：提供具有多层陶瓷基板的加热器及其制造方法。加热器由多个陶瓷层构成，层叠以形成单个陶瓷基板。多个电阻加热元件被沉积到多层陶瓷基片上，该多层陶瓷基片可经由穿过基片延伸到电阻加热元件的导电元件连接到电源。加热器还可以包括允许方便的电气和机械连接到吸烟制品的端子。

6. 发明授权

US5246018A Manufacturing of composite heat sources containing carbon and metal species 失效
标题翻译：制造含碳和金属物质的复合热源
公开(公告)号：US5246018A
公开(公告)日：1993-09-21
申请号：US732619
申请日：1991-07-19
申请人： Seetharama C. Deevi , Sarojini Deevi , Mohammad R. Hajaligol , Harry V. Lanzillotti , Arnys C. Lilly, Jr. , D. Bruce Losee , Michael L. Watkins
发明人： Seetharama C. Deevi , Sarojini Deevi , Mohammad R. Hajaligol , Harry V. Lanzillotti , Arnys C. Lilly, Jr. , D. Bruce Losee , Michael L. Watkins
IPC分类号： A24B15/16 , A24F47/00
CPC分类号： A24F47/004 , A24B15/165
摘要： This invention relates to improved methods for making a composite heat source comprising carbon and metal species. The composite heat source made by the methods of this invention have ignition temperatures that are substantially lower than carbonaceous heat sources, while at the same time provide sufficient heat to release a flavored aerosol from a flavor bed for inhalation by the smoker. Upon combustion, the heat source produces substantially no carbon monoxide. The metal species may be prepared by mixing a metal oxide, metal and a carbon source, pre-forming the metal oxide/metal/carbon source mixture into a shape and converting the mixture to metal species in situ, without substantially altering the original shape of the mixture.
摘要翻译：本发明涉及制备包含碳和金属物质的复合热源的改进方法。通过本发明方法制成的复合热源具有明显低于碳质热源的点火温度，同时提供足够的热量以从香味床上释放由吸烟者吸入的调味气溶胶。在燃烧时，热源基本上不产生一氧化碳。金属物质可以通过混合金属氧化物，金属和碳源来制备，将金属氧化物/金属/碳源混合物预成形为一种形状，并将混合物原位转化为金属物质，而基本上不改变原始形状混合物。

7. 发明授权

US06660109B2 Method of manufacturing aluminide sheet by thermomechanical processing of aluminide powders 失效
标题翻译：通过铝化物粉末的热机械加工制造铝化物片的方法
公开(公告)号：US06660109B2
公开(公告)日：2003-12-09
申请号：US09984871
申请日：2001-10-31
申请人： Mohammad R. Hajaligol , Clive Scorey , Vinod K. Sikka , Seetharama C. Deevi , Grier Fleishhauer , A. Clifton Lilly, Jr. , Randall M. German
发明人： Mohammad R. Hajaligol , Clive Scorey , Vinod K. Sikka , Seetharama C. Deevi , Grier Fleishhauer , A. Clifton Lilly, Jr. , Randall M. German
IPC分类号： C21D800
CPC分类号： C22C33/0278 , B22F3/18 , B22F5/006 , B22F9/082 , B22F2003/248 , B22F2009/0824 , B22F2009/088 , B22F2998/10 , C21D8/0205 , C21D8/0236 , C21D8/0273 , C22C1/0491 , B22F3/115 , B22F3/16 , B22F3/24
摘要： A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 &mgr;m. Final stress relief annealing can be carried out in the B2 phase temperature range.
摘要翻译：从具有金属间合金组成如粉末铁，镍或钛铝化物的粉末制备片材的粉末冶金方法。可以将片材制造成具有改善的室温延展性，电阻率，耐循环疲劳性，耐高温氧化性，低和高温强度和/或耐高温下垂的电阻加热元件。铁铝化物具有完全不含奥氏体的铁素体组织，并且可以以重量％计含有4至32％的Al和任选的添加物，例如<= 1％Cr，> = 0.05％Zr <= 2％Ti， = 2％Mo，<= 1％Ni，≤= 0.75％C，<= 0.1％B，≤1％亚微米级氧化物颗粒和/或电绝缘或导电共价陶瓷颗粒，≤1％稀土金属，和/或<= 3％Cu。该方法包括通过将具有金属间化合物组合物的粉末如通过辊压，带铸或等离子体喷涂固结形成非致密金属片，通过冷轧非致密金属片形成冷轧板，以增加密度并减小其厚度并退火冷轧板。粉末可以是在固结步骤之前与粘合剂进行筛分和/或共混的水，聚合物或气体雾化粉末。在固结步骤之后，片材可以部分烧结。可以重复冷轧和/或退火步骤以实现所需的板厚度和性能。退火可以在真空或惰性气氛的真空炉中进行。在最终退火期间，冷轧板再结晶至平均粒径约为10〜30μm。最终的应力消除退火可以在B2相温度范围内进行。

8. 发明授权

US5620651A Iron aluminide useful as electrical resistance heating elements 失效
标题翻译：铁铝化物可用作电阻加热元件
公开(公告)号：US5620651A
公开(公告)日：1997-04-15
申请号：US426006
申请日：1995-04-20
申请人： Vinod K. Sikka , Seetharama C. Deevi , Grier S. Fleischhauer , Mohammad R. Hajaligol , A. Clifton Lilly, Jr.
发明人： Vinod K. Sikka , Seetharama C. Deevi , Grier S. Fleischhauer , Mohammad R. Hajaligol , A. Clifton Lilly, Jr.
IPC分类号： C22C38/00 , B22F3/23 , C22C1/04 , C22C33/02 , C22C38/06 , C22C38/14 , C22C38/54 , H01C7/00 , H01C13/00 , H05B3/12
CPC分类号： C22C33/0278 , B22F3/23 , C22C1/0491 , C22C38/06 , B22F2998/00 , B22F2998/10 , B22F2999/00
摘要： The invention relates generally to aluminum containing iron-base alloys useful as electrical resistance heating elements. The aluminum containing iron-base alloys have improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The alloy has an entirely ferritic microstructure which is free of austenite and includes, in weight %, over 4% Al, .ltoreq.1% Cr and either .gtoreq.0.05% Zr or ZrO.sub.2 stringers extending perpendicular to an exposed surface of the heating element or .gtoreq.0.1% oxide dispersoid particles. The alloy can contain 14-32% Al, .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Zr, .ltoreq.1% C, .ltoreq.0.1% B, .ltoreq.30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, .ltoreq.1% oxygen, .ltoreq.3% Cu, balance Fe.
摘要翻译：本发明一般涉及可用作电阻加热元件的含铝铁基合金。含铝铁基合金具有改善的室温延展性，电阻率，循环耐疲劳性，耐高温氧化性，低，高温强度和/或耐高温下垂的能力。该合金具有完全不含奥氏体的铁素体组织，其重量百分比包括超过4％的Al，≤1％的Cr和> / = 0.05％的Zr或ZrO2桁条，垂直于加热的暴露表面延伸元素或> / = 0.1％氧化物分散质颗粒。该合金可以含有14-32％的Al，2％Ti，2％Mo，1％Zr，1％C，0.1％B，30％氧化物分散质和/或电绝缘或导电共价陶瓷颗粒，1％稀土金属，1％氧，3％Cu，余量为Fe。

9. 发明授权

US06607576B1 Oxidation, carburization and/or sulfidation resistant iron aluminide alloy 有权
标题翻译：氧化，渗碳和/或耐硫化铁铝合金
公开(公告)号：US06607576B1
公开(公告)日：2003-08-19
申请号：US09172375
申请日：1998-10-14
申请人： Vinod K. Sikka , Seetharama C. Deevi , Grier S. Fleischhauer , Mohammad R. Hajaligol , A. Clifton Lilly, Jr.
发明人： Vinod K. Sikka , Seetharama C. Deevi , Grier S. Fleischhauer , Mohammad R. Hajaligol , A. Clifton Lilly, Jr.
IPC分类号： C22C3302
CPC分类号： C22C33/0278 , B22F3/23 , B22F2998/00 , B22F2998/10 , B22F2999/00 , C22C1/0491 , C22C38/06 , B22F3/04 , B22F3/20 , B22F3/1208 , B22F3/18 , B22F3/10 , B22F9/082 , B22F3/15 , B22F2201/05
摘要： The invention relates generally to aluminum containing iron-base alloys useful as electrical resistance heating elements. The aluminum containing iron-base alloys have improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The alloy has an entirely ferritic microstructure which is free of austenite and includes, in weight %, over 4% Al, ≦1% Cr and either ≧0.05% Zr or Zro2 stringers extending perpendicular to an exposed surface of the heating element or ≧0.1% oxide dispersoid particles. The alloy can contain 14-32% Al, ≦2% Ti, ≦2% Mo, ≦1% Zr, ≦1% C, ≦0.1% B. ≦30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, ≦1% oxygen, ≦3% Cu, balance Fe.
摘要翻译：本发明一般涉及可用作电阻加热元件的含铝铁基合金。含铝铁基合金具有改善的室温延展性，电阻率，循环耐疲劳性，耐高温氧化性，低，高温强度和/或耐高温下垂的能力。该合金具有完全不含奥氏体的铁素体组织，其重量％包括超过4％的Al，≤1％的Cr和> = 0.05％的Zr或Zro2桁条，垂直于加热元件的暴露表面延伸，或 > = 0.1％氧化物分散质颗粒。该合金可以含有14-32％的Al，<= 2％Ti，<= 2％Mo，≤1％Zr，≤1％C，<= 0.1％B. <= 30％氧化物分散质和/或电绝缘或导电共价陶瓷颗粒，<= 1％稀土金属，<= 1％氧，<= 3％Cu，余量为Fe。

10. 发明授权

US06332936B1 Thermomechanical processing of plasma sprayed intermetallic sheets 有权
标题翻译：等离子喷涂金属间板的热机械加工
公开(公告)号：US06332936B1
公开(公告)日：2001-12-25
申请号：US09399364
申请日：1999-09-20
申请人： Mohammad R. Hajaligol , Clive Scorey , Vinod K. Sikka , Seetharama C. Deevi , Grier Fleischhauer , A. Clifton Lilly, Jr. , Randall M. German
发明人： Mohammad R. Hajaligol , Clive Scorey , Vinod K. Sikka , Seetharama C. Deevi , Grier Fleischhauer , A. Clifton Lilly, Jr. , Randall M. German
IPC分类号： B22F500
CPC分类号： C22C33/0278 , B22F3/18 , B22F5/006 , B22F9/082 , B22F2003/248 , B22F2009/0824 , B22F2009/088 , B22F2998/10 , C21D8/0205 , C21D8/0236 , C21D8/0273 , C22C1/0491 , B22F3/115 , B22F3/16 , B22F3/24
摘要： A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu. The process includes forming a non-densified metal sheet by consolidating a powder having an intermetallic alloy composition such as by roll compaction, tape casting or plasma spraying, forming a cold rolled sheet by cold rolling the non-densified metal sheet so as to increase the density and reduce the thickness thereof and annealing the cold rolled sheet. The powder can be a water, polymer or gas atomized powder which is subjecting to sieving and/or blending with a binder prior to the consolidation step. After the consolidation step, the sheet can be partially sintered. The cold rolling and/or annealing steps can be repeated to achieve the desired sheet thickness and properties. The annealing can be carried out in a vacuum furnace with a vacuum or inert atmosphere. During final annealing, the cold rolled sheet recrystallizes to an average grain size of about 10 to 30 &mgr;m. Final stress relief annealing can be carried out in the B2 phase temperature range.
摘要翻译：从具有金属间合金组成如粉末铁，镍或钛铝化物的粉末制备片材的粉末冶金方法。可以将片材制造成具有改善的室温延展性，电阻率，耐循环疲劳性，耐高温氧化性，低和高温强度和/或耐高温下垂的电阻加热元件。铁铝化物具有完全不含奥氏体的铁素体组织，并且可以以重量％计含有4至32％的Al和任选的添加物，例如<= 1％Cr，> = 0.05％Zr <= 2％Ti， = 2％Mo，<= 1％Ni，≤= 0.75％C，<= 0.1％B，≤1％亚微米级氧化物颗粒和/或电绝缘或导电共价陶瓷颗粒，≤1％稀土金属，和/或<= 3％Cu。该方法包括通过将具有金属间化合物组合物的粉末如通过辊压，带铸或等离子体喷涂固结形成非致密金属片，通过冷轧非致密金属片形成冷轧板，以增加密度并减小其厚度并退火冷轧板。粉末可以是在固结步骤之前与粘合剂进行筛分和/或共混的水，聚合物或气体雾化粉末。在固结步骤之后，片材可以部分烧结。可以重复冷轧和/或退火步骤以实现所需的板厚度和性能。退火可以在真空或惰性气氛的真空炉中进行。在最终退火期间，冷轧板再结晶至平均粒径约为10〜30μm。最终的应力消除退火可以在B2相温度范围内进行。

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