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1. 发明授权

US5618898A Weather-resistant solvent-based coating obtained by polymerization with thioether bond converted to sulfone bond 失效
标题翻译：通过用硫醚键聚合得到的耐候溶剂型涂料转化成砜键
公开(公告)号：US5618898A
公开(公告)日：1997-04-08
申请号：US318523
申请日：1994-10-05
申请人： Mitsuru Nagasawa , Kazuyuki Kuwano , Takeshi Kawakami , Mamoru Sugiura , Hiroshi Hibino , Shiro Kojima , Kishiro Azuma
发明人： Mitsuru Nagasawa , Kazuyuki Kuwano , Takeshi Kawakami , Mamoru Sugiura , Hiroshi Hibino , Shiro Kojima , Kishiro Azuma
IPC分类号： C08F8/06 , C08F20/24 , C08F20/26
CPC分类号： C08F290/046 , C08F8/06 , C08F8/14 , C08F2810/20 , C08F2810/30 , C08F2810/40 , Y10T428/31504
摘要： A process for producing a polymer of excellent weatherability, which comprises reacting a polymer having a thioether bond, with a peroxide to oxidize the sulfur atom in the bond to convert it into a sulfone.
摘要翻译：一种制备具有优异耐候性的聚合物的方法，其包括使具有硫醚键的聚合物与过氧化物反应以氧化该键中的硫原子以将其转化为砜。

2. 发明授权

US5310813A Thermosetting coating resin and process for producing the same 失效
标题翻译：热固性涂料树脂及其制备方法
公开(公告)号：US5310813A
公开(公告)日：1994-05-10
申请号：US43585
申请日：1993-04-05
申请人： Mitsuru Nagasawa , Kazuyuki Kuwano , Masataka Muramatsu , Kishiro Azuma , Hiroshi Hibino , Kazuko Nakanishi
发明人： Mitsuru Nagasawa , Kazuyuki Kuwano , Masataka Muramatsu , Kishiro Azuma , Hiroshi Hibino , Kazuko Nakanishi
IPC分类号： C08F290/04 , C09D4/06 , C08F265/06 , C08F265/02 , C08F265/04 , C08F267/02
CPC分类号： C08F290/04 , C09D4/06
摘要： The present invention provides a thermosetting coating resin consisting of a branched polymer, which branched polymer is obtained by copolymerizing a macromolecular monomer having a radical-polymerizable group at one end in the molecule and having a weight-average molecular weight of 1,000-10,000, with another radical-polymerizable monomer, which branched polymer contains the unit of said macromolecular monomer in a proportion of 40-99.5% by weight based on the amount of total constitutional units, which branched polymer has a cross-linkable functional group, and which branched polymer has a weight-average molecular weight of 5,000-30,000. The present invention further provides a process for producing such a thermosetting coating resin.
摘要翻译：本发明提供一种由支化聚合物组成的热固性涂料树脂，该支化聚合物通过使分子中一端具有自由基聚合性基团的高分子单体与重均分子量为1,000〜10,000的共聚而得到，另一种可自由基聚合的单体，其支化聚合物含有所述大分子单体的单元，其比例为总配合量为40-99.5重量％，该支化聚合物具有可交联官能团，并且该支化聚合物重均分子量为5,000〜30,000。本发明还提供一种制备这种热固性涂料树脂的方法。

3. 发明授权

US5164454A Ethylene graft copolymer and molding resin composition containing the same 失效
标题翻译：乙烯共聚物和含有它的成型树脂组合物
公开(公告)号：US5164454A
公开(公告)日：1992-11-17
申请号：US549995
申请日：1990-07-09
申请人： Katsufumi Suga , Yoshihiro Yoshinaga , Hiroaki Yoshitomi , Takashi Tsuda , Shiro Kojima , Kishiro Azuma
发明人： Katsufumi Suga , Yoshihiro Yoshinaga , Hiroaki Yoshitomi , Takashi Tsuda , Shiro Kojima , Kishiro Azuma
IPC分类号： C08F290/04 , C08L51/00
CPC分类号： C08F290/04 , C08L51/00
摘要： An ethylene graft copolymer is disclosed, which is obtained by radical polymerizing a monomer composition comprising (A) from 50 to 99.95% by weight of ethylene, (B) from 0.05 to 50% by weight of a macromonomer having a number average molecular weight of from 2,000 to 20,000 and having a (meth)acryloyl group only at one terminal of the molecular chain thereof, and (C) 0 to 49.95% by weight of other radical polymerizable monomer(s). The ethylene graft copolymer is a modifier for improving impact resistance of engineering plastics or a compatibilizer for engineering plastics to provide a molding resin composition excellent in impact resistance and oil resistance. The ethylene graft copolymer is also useful as a hot-melt adhesive or a pressure-sensitive adhesive.

4. 发明授权

US5147952A Process for producing macromolecular monomer 失效
标题翻译：生产大分子单体的方法
公开(公告)号：US5147952A
公开(公告)日：1992-09-15
申请号：US750337
申请日：1991-08-27
申请人： Yoshio Mori , Makoto Watanabe , Kishiro Azuma , Shiro Kojima
发明人： Yoshio Mori , Makoto Watanabe , Kishiro Azuma , Shiro Kojima
IPC分类号： C08F4/00 , C08F4/42 , C08F20/10 , C08F20/12 , C08F20/18 , C08F299/00
CPC分类号： C08F20/12 , C08F299/00
摘要： A process for producing a macromolecular monomer, which comprises anionic polymerization of a (meth)acrylic acid ester monomer by using, as a polymerization initiator, a compound represented by the following general formula [I]: ##STR1## wherein M.sup.+ is a quaternary ammonium ion; .phi.is a phenylene group; R.sub.1 and R.sub.2 are each an electron withdrawing group stabilizing the carbanion C.sup.-, or one of them is said electron withdrawing group and the other is an alkyl group of 1-6 carbon atoms or a phenyl group; and n is an integer of 0-6.
摘要翻译：一种制备高分子单体的方法，其包括通过使用由以下通式[I]表示的化合物作为聚合引发剂使（甲基）丙烯酸酯单体的阴离子聚合：其中M +为季铵离子; phi是亚苯基; R 1和R 2各自是稳定碳负离子C的吸电子基团，或者它们中的一个是所述吸电子基团，另一个是1-6个碳原子的烷基或苯基; n为0-6的整数。

5. 发明授权

US4759991A Magnetic recording medium having a lubricating coating layer 失效
标题翻译：具有润滑涂层的磁记录介质
公开(公告)号：US4759991A
公开(公告)日：1988-07-26
申请号：US707046
申请日：1985-03-01
申请人： Toshiyuki Kanno , Hitoshi Watanabe , Yasutaro Yasuda , Shiro Kojima , Hiroyuki Kato , Takashi Tsuda , Kishiro Azuma
发明人： Toshiyuki Kanno , Hitoshi Watanabe , Yasutaro Yasuda , Shiro Kojima , Hiroyuki Kato , Takashi Tsuda , Kishiro Azuma
IPC分类号： G11B5/72
CPC分类号： G11B5/72 , Y10S428/90 , Y10T428/31663 , Y10T428/31935
摘要： A magnetic recording medium having a modified surface, consisting essentially of (a) a substrate, (b) a ferromagnetic metal thin film formed on one side of the substrate by a vacuum deposition method, an ion plating method, a sputtering method or a plating method and (c) a lubricating coating layer formed on the thin film or on the back of the substrate or on both of them. The recording medium has an improved running stability, durability and corrosion resistance.
摘要翻译：一种具有改性表面的磁记录介质，其基本上由（a）基底，（b）通过真空沉积法形成在基底的一侧上的强磁性金属薄膜，离子镀法，溅射法或电镀方法和（c）形成在薄膜上或基底背面或两者上的润滑涂层。记录介质具有改进的运行稳定性，耐久性和耐腐蚀性。

6. 发明授权

US4677225A Process for the production of acrylic acid or methacrylic acid 失效
标题翻译：制备丙烯酸或甲基丙烯酸的方法
公开(公告)号：US4677225A
公开(公告)日：1987-06-30
申请号：US736621
申请日：1985-05-21
申请人： Hiroshi Niizuma , Toshiro Miki , Shiro Kojima , Kishiro Azuma , Hiroyuki Kato , Yuichi Murakami , Tsutomu Ito
发明人： Hiroshi Niizuma , Toshiro Miki , Shiro Kojima , Kishiro Azuma , Hiroyuki Kato , Yuichi Murakami , Tsutomu Ito
IPC分类号： B01J27/18 , B01J27/186 , C07C51/353 , C07C57/05 , C07C57/04
CPC分类号： B01J27/186 , B01J27/18 , C07C51/353
摘要： A process for producing acrylic acid or methacrylic acid by reacting acetic acid or propionic acid with formaldehyde in a gas phase is described, characterized by carrying out the reaction in the presence of a solid catalyst containing at least one of boron oxide or phosphorus oxide and having an acid site of an acid strength, pKa.ltoreq.-3.0. The solid catalyst is of high activity and is satisfactory in both selectivity and conversion and, furthermore, its high selectivity can be maintained for long periods of time. Thus the desired product, acrylic acid or methacrylic acid, can be produced in high yield.
摘要翻译：描述了一种通过使乙酸或丙酸与甲醛在气相中反应生产丙烯酸或甲基丙烯酸的方法，其特征在于在含有氧化硼或氧化磷中的至少一种的固体催化剂存在下进行反应，并且具有酸强度的酸性位点，pKa <3.0。固体催化剂具有高活性，并且在选择性和转化率方面均令人满意，此外，其高选择性可以长时间保持。因此，可以高产率生产所需产物丙烯酸或甲基丙烯酸。

7. 发明授权

US5179158A Process for producing aqueous resin dispersion 失效
标题翻译：生产水性树脂分散体的方法
公开(公告)号：US5179158A
公开(公告)日：1993-01-12
申请号：US564479
申请日：1990-08-09
申请人： Kishiro Azuma , Yoshio Mori , Masayoshi Okubo
发明人： Kishiro Azuma , Yoshio Mori , Masayoshi Okubo
IPC分类号： C08F2/24 , C08F2/26 , C08F290/04
CPC分类号： C08F290/046 , C08F290/044
摘要： A process for producing an aqueous resin dispersion is disclosed, which comprises dissolving a macromonomer having a radical polymerizable group at the terminal thereof and an oil-soluble radical polymerization initiator in a hydrophobic vinyl monomer copolymerizable with the macromonomer to form a solution, emulsifying the solution in an aqueous medium in the presence of an emulsifying agent selected from (A) an alkali sulfosuccinate anionic surfactant and (B) a surfactant comprising from 2 to 98% by weight of (i) an alkali sulfonate anionic surfactant other than (A) or (ii) an alkali sulfuric ester anionic surfactant, and from 98 to 2% by weight of a nonionic surfactant having an HLB value of 10 or more, and copolymerizing the macromonomer and the vinyl monomer at an elevated temperature. The aqueous resin dispersion has a high content of a graft polymer with a reduced content of unreacted macromonomer.
摘要翻译：公开了一种水性树脂分散体的制造方法，其特征在于，将其末端具有自由基聚合性基团的大分子单体和油溶性自由基聚合引发剂溶解在与大分子单体共聚的疏水性乙烯基单体中，形成溶液，在（A）碱金属磺基琥珀酸盐阴离子表面活性剂和（B）包含2-98重量％的（ⅰ）除（A）之外的碱金属磺酸盐阴离子表面活性剂的表面活性剂的存在下，在水性介质中，（ii）碱硫酸酯阴离子表面活性剂和98〜2重量％HLB值为10以上的非离子表面活性剂，并在高温下共聚大分子单体和乙烯基单体。含水树脂分散体具有高含量的未反应的大分子单体含量降低的接枝聚合物。

8. 发明授权

US5073357A Process for producing hydroxylapatites 失效
标题翻译：生产羟基磷酸酯的方法
公开(公告)号：US5073357A
公开(公告)日：1991-12-17
申请号：US554709
申请日：1990-07-18
申请人： Osamu Takagi , Kishiro Azuma , Tatsuichi Iwamura
发明人： Osamu Takagi , Kishiro Azuma , Tatsuichi Iwamura
IPC分类号： B01J20/281 , B01J20/04 , C01B25/32 , G01N30/88
CPC分类号： C01B25/327 , B01J20/048 , B01J20/28014 , B01J20/281 , B01J2220/52
摘要： Provided is a process for producing hydroxylapatite suitable for chromatographic separation of biopolymers. The process comprises allowing hexagonal prismatic or acicular monetite to react with potassium hydroxide and/or lithium hydroxide under heating.
摘要翻译：提供了适用于生物聚合物色谱分离的羟基磷灰石的方法。该方法包括在加热下使六角棱柱形或针状六棱石与氢氧化钾和/或氢氧化锂反应。

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