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    • 8. 发明授权
    • Method and apparatus for producing metal powder
    • 金属粉末的制造方法和装置
    • US07449044B2
    • 2008-11-11
    • US10528372
    • 2003-09-12
    • Tsuyoshi AsaiTakuya Miyagi
    • Tsuyoshi AsaiTakuya Miyagi
    • B22F9/28
    • B22F9/28
    • An object of the present invention is to provide a method for production of metallic powder in which aggregation of particles and growth to secondary particle after reducing process of the metallic powder particle can be prevented, to reliably obtain metallic particles containing few coarse particles and to meet requirements of thinner layer and greater number of layers in recent capacitors, and a production device therefor. The present invention includes a reducing process in which metal chloride gas and reducing gas are contacted to continuously reduce the metal chloride, and a cooling process in which a gas containing metallic powder generated in the reducing process is continuously cooled by inert gas. In the cooling process, a vortex flow is generated by blowing out the inert gas from at least one part around the flowing passage of the metallic powder. Furthermore, during the production of the metallic powder, inert gas flow is generated in the vertical direction along the inner wall of the production device (reducing process and cooling process) continuously. Aggregation of the metallic powder and growth of secondary particles can be reduced to reliably obtain metallic powder having uniform particle size containing few coarse particles.
    • 本发明的目的是提供一种金属粉末的制造方法,其中可以防止金属粉末颗粒的还原过程后的颗粒和生长到二次颗粒的聚集,以可靠地获得含有少量粗颗粒的金属颗粒并满足 最近电容器中较薄层和更多层数的要求及其制造装置。 本发明包括使金属氯化物气体和还原气体接触以连续地还原金属氯化物的还原过程,并且在还原过程中产生的含有金属粉末的气体通过惰性气体连续冷却的冷却过程。 在冷却过程中,通过从金属粉末的流动通道周围的至少一部分吹出惰性气体而产生涡流。 此外,在制造金属粉末的过程中,沿着生产装置的内壁(还原过程和冷却过程)在垂直方向上产生惰性气体流。 可以减少金属粉末的聚集和二次粒子的生长,以可靠地获得具有少量粗粒子的均匀粒径的金属粉末。