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1. 发明申请

US20130206579A1 SELECTIVE DEHYDROHALOGENATION OF TERTIARY HALOGENATED HYDROCARBONS AND REMOVAL OF TERTIARY HALOGENATED HYDROCARBON IMPURITIES FROM A HALOGENATED HYDROCARBON PRODUCT 审中-公开
标题翻译：选择性脱氢氢化氢化石油烃，并从氢化氢产物中去除苛性氢化烃类污染物
公开(公告)号：US20130206579A1
公开(公告)日：2013-08-15
申请号：US13837276
申请日：2013-03-15
申请人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
发明人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
IPC分类号： C07C17/395
CPC分类号： C07C17/395 , B01D3/00 , B01D3/009 , B01D3/34 , C07B2200/09 , C07C17/383 , C07C21/073
摘要： A process for converting a tertiary halogenated hydrocarbons in a tertiary halogenated hydrocarbon-containing stream to a corresponding unhalogenated or less-halogenated unsaturated hydrocarbon product with the release of hydrogen halide involves contacting the tertiary halogenated hydrocarbon with a sorbent-type dehydrohalogenation catalyst in a reaction zone and optionally passing a stripping gas through the reaction zone to remove vapor phase reaction products from the reaction zone. A process for removing a tertiary chlorinated hydrocarbon impurity from 1,3-dichloro-1-propene involves contacting a mixture containing the 1,3-dichloro-1-propene and the tertiary chlorinated hydrocarbon impurity with a dehydrochlorination catalyst effective to catalyze a conversion of the tertiary chlorinated hydrocarbon impurity to a corresponding unchlorinated or less-chlorinated unsaturated hydrocarbon and hydrogen chloride and distilling the 1,3-dichloro-1-propene to produce a purified cis-1,3-dichloro-1-propene fraction and a purified trans-1,3-dichloro-1-propene fraction.
摘要翻译：在含卤代烃的物流中将叔卤代烃转化为相应的未卤化或低卤化的不饱和烃产物的方法，其中卤化氢的释放包括使叔卤代烃与吸附剂型脱卤化氢催化剂在反应区并且可选地使汽提气体通过反应区以从反应区除去气相反应产物。从1,3-二氯-1-丙烯中除去叔氯化烃杂质的方法包括将含有1,3-二氯-1-丙烯和叔氯化烃杂质的混合物与脱氯化氢催化剂接触，该催化剂有效催化转化率叔氯化烃杂质转化成相应的未氯化或较少氯化的不饱和烃和氯化氢并蒸馏1,3-二氯-1-丙烯以产生纯化的顺式-1,3-二氯-1-丙烯馏分和纯化的反式 -1,3-二氯-1-丙烯馏分。

2. 发明申请

US20130206578A1 SELECTIVE DEHYDROHALOGENATION OF TERTIARY HALOGENATED HYDROCARBONS AND REMOVAL OF TERTIARY HALOGENATED HYDROCARBON IMPURITIES FROM A HALOGENATED HYDROCARBON PRODUCT 审中-公开
标题翻译：选择性脱氢化氢化石油烃，并从氢化氢产物中去除苛性氢化烃类污染物
公开(公告)号：US20130206578A1
公开(公告)日：2013-08-15
申请号：US13835951
申请日：2013-03-15
申请人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
发明人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
IPC分类号： C07C17/395
CPC分类号： C07C17/395 , B01D3/00 , B01D3/009 , B01D3/34 , C07B2200/09 , C07C17/383 , C07C21/073
摘要： A process for converting a tertiary halogenated hydrocarbons in a tertiary halogenated hydrocarbon-containing stream to a corresponding unhalogenated or less-halogenated unsaturated hydrocarbon product with the release of hydrogen halide involves contacting the tertiary halogenated hydrocarbon with a sorbent-type dehydrohalogenation catalyst in a reaction zone and optionally passing a stripping gas through the reaction zone to remove vapor phase reaction products from the reaction zone. A process for removing a tertiary chlorinated hydrocarbon impurity from 1,3-dichloro-1-propene involves contacting a mixture containing the 1,3-dichloro--propene and the tertiary chlorinated hydrocarbon impurity with a dehydrochlorination catalyst effective to catalyze a conversion of the tertiary chlorinated hydrocarbon impurity to a corresponding unchlorinated or less-chlorinated unsaturated hydrocarbon and hydrogen chloride and distilling the 1,3-dichloro-1-propene to produce a purified cis-1,3-dichloro- 1-propene fraction and a purified trans-1,3-dichloro-1-propene fraction.
摘要翻译：在含卤代烃的物流中将叔卤代烃转化为相应的未卤化或低卤化的不饱和烃产物的方法，其中卤化氢的释放包括使叔卤代烃与吸附剂型脱卤化氢催化剂在反应区并且可选地使汽提气体通过反应区以从反应区除去气相反应产物。从1,3-二氯-1-丙烯中除去叔氯化烃杂质的方法包括使含有1,3-二氯丙烯和叔氯代烃杂质的混合物与脱氯化氢催化剂接触，该催化剂有效地催化将叔氯化烃杂质加入到相应的未氯化或较少氯化的不饱和烃和氯化氢中并蒸馏1,3-二氯-1-丙烯以产生纯化的顺式-1,3-二氯-1-丙烯级分和纯化的反式 - 1,3-二氯-1-丙烯馏分。

3. 发明授权

US08449729B2 Selective dehydrohalogenation of tertiary halogenated hydrocarbons and removal of tertiary halogenated hydrocarbon impurities from a halogenated hydrocarbon product 有权
公开(公告)号：US08449729B2
公开(公告)日：2013-05-28
申请号：US12803345
申请日：2010-06-24
申请人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
发明人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
IPC分类号： B01D3/00 , B01D3/34
CPC分类号： C07C17/395 , B01D3/00 , B01D3/009 , B01D3/34 , C07B2200/09 , C07C17/383 , C07C21/073
摘要： A process for converting a tertiary halogenated hydrocarbons in a tertiary halogenated hydrocarbon-containing stream to a corresponding unhalogenated or less-halogenated unsaturated hydrocarbon product with the release of hydrogen halide involves contacting the tertiary halogenated hydrocarbon with a sorbent-type dehydrohalogenation catalyst in a reaction zone and optionally passing a stripping gas through the reaction zone to remove vapor phase reaction products from the reaction zone. A process for removing a tertiary chlorinated hydrocarbon impurity from 1,3-dichloro-1-propene involves contacting a mixture containing the 1,3-dichloro-1-propene and the tertiary chlorinated hydrocarbon impurity with a dehydrochlorination catalyst effective to catalyze a conversion of the tertiary chlorinated hydrocarbon impurity to a corresponding unchlorinated or less-chlorinated unsaturated hydrocarbon and hydrogen chloride and distilling the 1,3-dichloro-1-propene to produce a purified cis-1,3-dichloro-1-propene fraction and a purified trans-1,3-dichloro-1-propene fraction.

4. 发明申请

US20110005914A1 Selective dehydrohalogenation of tertiary halogenated hydrocarbons and removal of tertiary halogenated hydrocarbon impurities from a halogenated hydrocarbon product 有权
标题翻译：叔卤代烃的选择性脱卤化氢和从卤代烃产物中除去叔卤代烃杂质
公开(公告)号：US20110005914A1
公开(公告)日：2011-01-13
申请号：US12803345
申请日：2010-06-24
申请人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
发明人： Michael L. Trippeer , Timothy C. Frank , Patrick H. Au-Yeung , Jason L. Bronkema , Robin K. Johnston , Mukund R. Patel , Bruce S. Holden , Terrence McCabe , Daniel A. Hickman
IPC分类号： B01D3/34
CPC分类号： C07C17/395 , B01D3/00 , B01D3/009 , B01D3/34 , C07B2200/09 , C07C17/383 , C07C21/073
摘要： A process for converting a tertiary halogenated hydrocarbons in a tertiary halogenated hydrocarbon-containing stream to a corresponding unhalogenated or less-halogenated unsaturated hydrocarbon product with the release of hydrogen halide involves contacting the tertiary halogenated hydrocarbon with a sorbent-type dehydrohalogenation catalyst in a reaction zone and optionally passing a stripping gas through the reaction zone to remove vapor phase reaction products from the reaction zone. A process for removing a tertiary chlorinated hydrocarbon impurity from 1,3-dichloro-1-propene involves contacting a mixture containing the 1,3-dichloro-1-propene and the tertiary chlorinated hydrocarbon impurity with a dehydrochlorination catalyst effective to catalyze a conversion of the tertiary chlorinated hydrocarbon impurity to a corresponding unchlorinated or less-chlorinated unsaturated hydrocarbon and hydrogen chloride and distilling the 1,3-dichloro-1-propene to produce a purified cis-1,3-dichloro-1-propene fraction and a purified trans-1,3-dichloro-1-propene fraction.
摘要翻译：在含卤代烃的物流中将叔卤代烃转化为相应的未卤化或低卤化的不饱和烃产物的方法，其中卤化氢的释放包括使叔卤代烃与吸附剂型脱卤化氢催化剂在反应区并且可选地使汽提气体通过反应区以从反应区除去气相反应产物。从1,3-二氯-1-丙烯中除去叔氯化烃杂质的方法包括将含有1,3-二氯-1-丙烯和叔氯化烃杂质的混合物与脱氯化氢催化剂接触，该催化剂有效催化转化率叔氯化烃杂质转化成相应的未氯化或较少氯化的不饱和烃和氯化氢并蒸馏1,3-二氯-1-丙烯以产生纯化的顺式-1,3-二氯-1-丙烯馏分和纯化的反式 -1,3-二氯-1-丙烯馏分。

5. 发明申请

US20100099155A1 RECOVERY OF VOLATILE PRODUCTS FROM FERMENTATION BROTH 审中-公开
标题翻译：从发酵豆中回收挥发性产品
公开(公告)号：US20100099155A1
公开(公告)日：2010-04-22
申请号：US12516981
申请日：2007-12-12
申请人： Timothy C. Frank , Jeff A. Ferrio , Paul E. Swanson , Juergen Lueske
发明人： Timothy C. Frank , Jeff A. Ferrio , Paul E. Swanson , Juergen Lueske
IPC分类号： C12M1/12 , C12P7/62 , C12P7/26 , C12P7/28 , C12P7/04 , C12P7/16 , C12P7/06
CPC分类号： C12P7/16 , B01D3/343 , C12M21/04 , C12M21/12 , C12M27/20 , C12M29/02 , C12M47/10 , Y02E50/10 , Y02E50/17
摘要： Provided are apparatuses and processes for the removal and purification of fermentation prepared one or more volatile organic compounds. The apparatuses comprise a fermentor unit, a vacuum side stripper unit (10), and, optionally, one or more of a pressure-swing adsorption unit, a dual-function column, a dividing wall distillation column unit, and a means for inducing phase separation of a mixture of a volatile organic compound and water.
摘要翻译：提供了制备一种或多种挥发性有机化合物的用于去除和纯化发酵的装置和方法。这些装置包括发酵罐单元，真空侧剥离器单元（10），以及任选的一个或多个变压吸附单元，双功能柱，分隔壁蒸馏塔单元和用于诱导相的装置分离挥发性有机化合物和水的混合物。

6. 发明申请

US20090321352A1 LIQUID-LIQUID EXTRACTION 失效
标题翻译：液体萃取
公开(公告)号：US20090321352A1
公开(公告)日：2009-12-31
申请号：US12375275
申请日：2007-07-26
申请人： Timothy C. Frank , John J. Anderson
发明人： Timothy C. Frank , John J. Anderson
IPC分类号： B01D11/04
CPC分类号： B01D11/0434 , B01D11/0438
摘要： A liquid-liquid extraction process that uses counterflowing liquid phases, especially in conjunction with a reciprocating plate extraction column, wherein one of the liquid phases has a lower density than the other and is at least partially saturated with a dispersible gas, requires less plate stack height or a smaller column diameter when plate-to-plate spacing is non-uniform rather than uniform and such non-uniform plate-to-plate spacing includes greater plate-to-plate spacing proximate to raffinate liquid discharge than proximate to feed of the lower density liquid phase.
摘要翻译：一种液 - 液萃取方法，其特别是与往复式板萃取塔结合使用逆流液相，其中液相之一具有比另一液相低的密度，并且至少部分地被可分散的气体饱和，需要较少的板堆高度或较小的柱直径，当板对板间距不均匀而不是均匀，并且这种不均匀的板对板间距包括靠近萃余液液体排放的较大的板对板间距，低密度液相。

7. 发明授权

US5301934A Twin screw vise 失效
标题翻译：双螺纹虎钳
公开(公告)号：US5301934A
公开(公告)日：1994-04-12
申请号：US927326
申请日：1992-08-10
申请人： John S. Lynn , Francis A. McLean , Edwin C. Tucker , Lloyd Sevack , Gary W. Lacoste , Timothy C. Frank , Michel Perrier , Leonard G. Lee
发明人： John S. Lynn , Francis A. McLean , Edwin C. Tucker , Lloyd Sevack , Gary W. Lacoste , Timothy C. Frank , Michel Perrier , Leonard G. Lee
IPC分类号： B25B1/10 , B23Q1/04
CPC分类号： B25B1/103
摘要： A twin screw vise utilizing two threaded vise screw rods that are journaled through flanged nuts fixed to a workbench top or to a rear, fixed bench jaw. The vise screws pass through a movable front jaw and into tee-castings and handles that may be turned to rotate the screws. Sprockets are located on each screw between the tee castings and the front jaw and are coupled by a chain. One of the sprockets is fixed in position on its screw during a calibration procedure. The other sprocket remains free to rotate on its screw, except when a spring loaded pin in the corresponding tee-casting engages a depression in the face of the sprocket, thereby coupling that sprocket to the tee casting and associated screw.
摘要翻译：一种双螺纹虎钳，采用两根螺纹虎钳螺丝杆，通过法兰螺母固定在工作台顶部或后部固定的台钳上。虎钳螺丝穿过可移动的前颚，并穿过T形铸件和手柄，可以转动以旋转螺丝。链轮位于三通铸件和前颚之间的每个螺钉上，并通过链条连接。其中一个链轮在校准过程中固定在其螺钉上的位置上。另一个链轮在其螺钉上保持自由旋转，除非相应的三通铸件中的弹簧加载销接合链轮表面的凹陷，从而将该链轮联接到三通铸件和相关螺钉。

8. 发明申请

US20110031102A1 PURIFICATION OF HYDROFORMYLATED AND HYDROGENATED FATTY ALKYL ESTER COMPOSITIONS 有权
标题翻译：氢化和加氢脂肪酸酯组合物的纯化
公开(公告)号：US20110031102A1
公开(公告)日：2011-02-10
申请号：US12667884
申请日：2008-06-20
申请人： George J. Frycek , Shawn D. Feist , Timothy C. Frank , Zenon Lysenko , Joe D. Phillips , Bruce W. Pynnonen
发明人： George J. Frycek , Shawn D. Feist , Timothy C. Frank , Zenon Lysenko , Joe D. Phillips , Bruce W. Pynnonen
IPC分类号： B01D3/10 , B01D1/22 , B01D15/08 , B01D15/18
CPC分类号： B01D1/22 , B01D3/10 , B01D15/1821 , C07C67/56 , C11C3/00 , C11C3/12 , C07C69/675 , C07C69/24
摘要： Effect separation of a composition of matter that includes at least two seed or plant oil derivatives into at least one desired product stream using at least two separation operations, which are independently selected from among several potential separation operations, in conjunction with at least one recycle stream from a separation operation.
摘要翻译：使用至少两个分离操作将包含至少两种种子或植物油衍生物的物质组合物分离成至少一种所需的产物流，所述至少两种分离操作独立地选自几种潜在的分离操作，连同至少一种循环流从分离操作。

9. 发明授权

US07713418B2 Process for recovering organic compounds from aqueous streams containing same 有权
标题翻译：从含有它们的水流中回收有机化合物的方法
公开(公告)号：US07713418B2
公开(公告)日：2010-05-11
申请号：US10590685
申请日：2005-02-18
申请人： Timothy C. Frank , Thomas C. Thyne , Felipe A. Donate
发明人： Timothy C. Frank , Thomas C. Thyne , Felipe A. Donate
IPC分类号： B01D15/00 , C02F1/44 , B01D11/04
CPC分类号： C07C227/40 , C07C29/86 , C07C51/48 , C07C55/10 , C07C59/08 , C07C55/14 , C07C59/265 , C07C53/08 , C07C31/225 , C07C31/205 , C07C31/22 , C07C31/26 , C07C229/24
摘要： A method for a liquid-liquid extraction of hydrophilic organic compounds from aqueous solutions thereof is described. The method generally includes intermixing a sufficient quantity of a specified glycol ether with the aqueous liquor at a first temperature to form a suspension comprising an aqueous raffinate phase and a glycol ether extract phase; separating the glycol ether extract phase from the aqueous raffinate phase; heating the glycol ether extract phase to a second, higher temperature to form a suspension comprising an aqueous extract phase containing a portion of the hydrophilic organic compound and a glycol ether raffinate phase; and separating this glycol ether raffinate phase from the aqueous extract phase. The selected glycol ether has an inverse solubility in water and the partition ratio, value K, for the hydrophilic organic compound is greater than 0.1. This method is useful for recovering valuable hydrophilic organic acids produced via fermentation or produced or used in various manufacturing processes.
摘要翻译：描述了从其水溶液中液 - 液萃取亲水性有机化合物的方法。该方法通常包括在第一温度下将足够量的特定二醇醚与含水液体混合以形成包含残液相和二醇醚萃取相的悬浮液; 从萃余水相中分离出乙二醇醚萃取相; 将乙二醇醚提取相加热至第二较高温度以形成包含含有一部分亲水性有机化合物和二醇醚萃余相的含水萃取相的悬浮液; 并从水相萃取相中分离出该二醇醚萃余相。所选择的二醇醚在水中具有相反的溶解度，并且亲水性有机化合物的分配比值K大于0.1。该方法可用于回收通过发酵生产或生产或用于各种制造工艺中的有价值的亲水性有机酸。

10. 发明授权

US08883472B2 Process for removing water from aqueous solutions of proteins 有权
标题翻译：从蛋白质水溶液中除去水分的方法
公开(公告)号：US08883472B2
公开(公告)日：2014-11-11
申请号：US10590095
申请日：2005-02-18
申请人： Felipe A. Donate , Timothy C. Frank , Barbara J. Grabowski
发明人： Felipe A. Donate , Timothy C. Frank , Barbara J. Grabowski
IPC分类号： C07K1/00 , C07K1/14
CPC分类号： C07K1/145
摘要： A method for extracting water from an aqueous solution of a protein comprising the steps of: (a) intermixing the aqueous solution of the protein with a sufficient quantity of at least one glycol ether at a temperature at least 30 centigrade degrees above the lower critical solution temperature (LCST), preferably at least 20 centigrade degrees above the LCST, and most preferably at least 10 degrees above the LCST, to form a suspension comprising a concentrated aqueous protein phase and a liquid organic phase comprising said at least one glycol ether and at least 10 percent water extracted from the aqueous solution of the protein, wherein the glycol ether has an inverse solubility in water, with the proviso that the solubility of the glycol ether in water is significantly less than the solubility of water in the glycol ether, and the glycol ether does not significantly deactivate the protein, and (b) separating the concentrated aqueous protein phase formed in step (a) from at least a portion of the liquid organic phase.
摘要翻译：一种从蛋白质水溶液中提取水的方法，包括以下步骤：（a）将蛋白质水溶液与足够量的至少一种二醇醚在比较低临界溶液高至少30摄氏度的温度下混合温度（LCST），优选高于LCST至少20摄氏度，最优选高于LCST至少10度，以形成包含浓缩的蛋白质水相和包含所述至少一种二醇醚的液体有机相的悬浮液，并且在从蛋白质水溶液中提取的最少10％的水，其中乙二醇醚在水中具有相反的溶解度，条件是二醇醚在水中的溶解度显着小于水在乙二醇醚中的溶解度，以及乙二醇醚不会使蛋白质显着失活，和（b）将步骤（a）中形成的浓缩水性蛋白质相从至少一个孔液体有机相。

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