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1. 发明申请

US20060217494A1 Basic silane coupling agent organic carboxylate composition, method for producing the same, and epoxy resin composition containing the same 有权
标题翻译：碱性硅烷偶联剂有机羧酸酯组合物，其制备方法和含有它们的环氧树脂组合物
公开(公告)号：US20060217494A1
公开(公告)日：2006-09-28
申请号：US11444728
申请日：2006-06-01
申请人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
发明人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
IPC分类号： C08G65/48 , C07F7/10
CPC分类号： C08G59/4238 , C07F7/1804
摘要： There are provided a composition for functioning as an effective additive for epoxy resin that is solid at room temperature and has high storage stability, and a method thereof. The composition of the present invention is a basic silane coupling agent organic carboxylate composition obtained by first synthesizing an organic carboxylate of a basic silane coupling agent by reacting a basic silane coupling agent and an organic carboxylic acid, and subsequently heating and mixing the organic carboxylate of the basic silane coupling agent with a compound exhibiting good affinity for the basic silane coupling agent or organic carboxylic acid and having a softening point or melting point of 40° C. or greater.
摘要翻译：提供了用作在室温下为固体并具有高储存稳定性的环氧树脂的有效添加剂的组合物及其方法。本发明的组合物是通过使碱性硅烷偶联剂与有机羧酸反应，首先合成碱性硅烷偶联剂的有机羧酸酯，然后将所述碱性硅烷偶联剂与对所述碱性硅烷偶联剂或有机羧酸具有良好亲和性且软化点或熔点为40℃以上的化合物。

2. 发明授权

US06605356B2 Metal surface treatment agent, and metal material coated with same 有权
标题翻译：金属表面处理剂，金属材料涂覆同样
公开(公告)号：US06605356B2
公开(公告)日：2003-08-12
申请号：US10009902
申请日：2001-12-10
申请人： Takashi Ouchi , Katsuyuki Tsuchida , Masashi Kumagai
发明人： Takashi Ouchi , Katsuyuki Tsuchida , Masashi Kumagai
IPC分类号： B32B2738
CPC分类号： C23C30/00 , Y10T428/31511 , Y10T428/31515 , Y10T428/31529 , Y10T428/31663
摘要： A metal surface treatment agent containing the following components (A) to (D), which securely adheres to a metal substrate such as aluminum, exhibits excellent corrosion preventive properties, even with a thin film thickness, and has excellent plasticity and adhesion to paints. (A) at least one organosilicon compound having three carbonyl groups and at least one alkoxysilyl group, the organosilicon compound being present in a weight ratio of 5 to 15, based on the total of the components (A) to (D) being 100; (B) at least one epoxy resin modified with an alkanolamine, the modified epoxy resin being present in a weight ratio of 10 to 30 relative to the above total; (C) at least one blocked polyisocyanate present in a weight ratio of 50 to 70 relative to the above total; and (D) at least one amino resin present in a weight ratio of ratio 5 to 15 relative to the above total.
摘要翻译：含有以下成分（A）〜（D）的金属表面处理剂即使在薄膜厚度上也能够牢固地附着于铝等金属基材，也具有优异的耐腐蚀性，且具有优异的塑性和对涂料的粘合性。（A）至少一种具有三个羰基和至少一个烷氧基甲硅烷基的有机硅化合物，以组分（A）至（D）的总和为100，有机硅化合物以重量比5至15存在; （B）至少一种用链烷醇胺改性的环氧树脂，所述改性环氧树脂以相对于上述总量为10至30的重量比存在;（C）至少一种以重量比为50至70的封端多异氰酸酯相对于上述总数; 和（D）至少一种氨基树脂以相对于上述总量的比例为5至15的重量比存在。

3. 发明授权

US07432335B2 Basic silane coupling agent organic carboxylate composition, method for producing the same, and epoxy resin composition containing the same 有权
标题翻译：碱性硅烷偶联剂有机羧酸酯组合物，其制备方法和含有它们的环氧树脂组合物
公开(公告)号：US07432335B2
公开(公告)日：2008-10-07
申请号：US11444728
申请日：2006-06-01
申请人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
发明人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
IPC分类号： C08L61/06 , C08L63/02
CPC分类号： C08G59/4238 , C07F7/1804
摘要： There are provided a composition for functioning as an effective additive for epoxy resin that is solid at room temperature and has high storage stability, and a method thereof. The composition of the present invention is a basic silane coupling agent organic carboxylate composition obtained by first synthesizing an organic carboxylate of a basic silane coupling agent by reacting a basic silane coupling agent and an organic carboxylic acid, and subsequently heating and mixing the organic carboxylate of the basic silane coupling agent with a compound exhibiting good affinity for the basic silane coupling agent or organic carboxylic acid and having a softening point or melting point of 40° C. or greater.
摘要翻译：提供了用作在室温下为固体并具有高储存稳定性的环氧树脂的有效添加剂的组合物及其方法。本发明的组合物是通过使碱性硅烷偶联剂与有机羧酸反应，首先合成碱性硅烷偶联剂的有机羧酸酯，然后将所述碱性硅烷偶联剂与对所述碱性硅烷偶联剂或有机羧酸具有良好亲和性且软化点或熔点为40℃以上的化合物。

4. 发明授权

US06916865B2 Organic carboxylic acid salt composition, process for preparation thereof and additives for epoxy resins 有权
标题翻译：有机羧酸盐组合物，其制备方法和环氧树脂添加剂
公开(公告)号：US06916865B2
公开(公告)日：2005-07-12
申请号：US10451977
申请日：2002-08-27
申请人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
发明人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
IPC分类号： C07B61/00 , C07F7/18 , C08G59/40 , C08G59/42 , C08G59/58 , C09D5/03 , C09D163/00 , H05K3/28 , C07D213/69 , C07D233/72 , C07D235/12 , C07F7/10 , C08K5/11
CPC分类号： C08G59/58 , C07F7/1804 , C08G59/4238 , H05K3/287
摘要： The present invention provides an organic carboxylate composition that has long working life, cures epoxy resins, and improves adhesive properties, and also provides a method for producing the same. An organic carboxylate composition, obtained by heating and mixing a basic silane coupling agent and an amine compound with a softening point or melting point of 40° C. or greater together with an organic carboxylic acid; a method for producing the same; an additive for epoxy resin that contains this as the active ingredient thereof; and an epoxy resin composition containing the same. The basic silane coupling agent should preferably be a specific imidazole-group containing silane coupling agent, amino group-containing silane coupling agent, dialkylamino group-containing silane coupling agent, monomethylamino group-containing silane coupling agent, benzimidazole group-containing silane coupling agent, benzotriazole group-containing silane coupling agent, and pyridine ring-containing silane coupling agent.
摘要翻译：本发明提供一种具有长的使用寿命，固化环氧树脂和改善粘合性能的有机羧酸盐组合物，并且还提供了一种制备该组合物的方法。通过将碱性硅烷偶联剂和软化点或熔点为40℃以上的胺化合物与有机羧酸一起加热混合而获得的有机羧酸盐组合物; 其制造方法; 含有作为其活性成分的环氧树脂添加剂; 和含有该环氧树脂组合物的环氧树脂组合物。碱性硅烷偶联剂优选为特定的含咪唑基的硅烷偶联剂，含氨基的硅烷偶联剂，含二烷基氨基的硅烷偶联剂，含单甲基氨基的硅烷偶联剂，含苯并咪唑基的硅烷偶联剂，含有苯并三唑基的硅烷偶联剂和含吡啶环的硅烷偶联剂。

5. 发明授权

US07094845B2 Basic silane coupling agent organic carboxylate composition, method for producing the same, and epoxy resin composition containing the same 有权
标题翻译：碱性硅烷偶联剂有机羧酸酯组合物，其制备方法和含有它们的环氧树脂组合物
公开(公告)号：US07094845B2
公开(公告)日：2006-08-22
申请号：US10450421
申请日：2002-08-27
申请人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
发明人： Masashi Kumagai , Takashi Ouchi , Katsuyuki Tsuchida
IPC分类号： C08L61/06 , C08L63/02
CPC分类号： C08G59/4238 , C07F7/1804
摘要： There is provided a composition for functioning as an effective additive for an epoxy resin that is a solid at room temperature and has a high storage stability, and a method thereof. The composition of the present invention is a basic silane coupling agent organic carboxylate composition obtained by first synthesizing an organic carboxylate of a basic silane coupling agent by reacting a basic silane coupling agent and an organic carboxylic acid, and subsequently heating and mixing the organic carboxylate of the basic silane coupling agent with a compound exhibiting a good affinity for the basic silane coupling agent or organic carboxylic acid and having a softening point or melting point of 40° C. or greater.
摘要翻译：提供了用作环氧树脂在室温下为固体并具有高储存稳定性的有效添加剂的组合物及其方法。本发明的组合物是通过使碱性硅烷偶联剂与有机羧酸反应，首先合成碱性硅烷偶联剂的有机羧酸酯，然后将碱性硅烷偶联剂与对碱性硅烷偶联剂或有机羧酸具有良好亲和性且软化点或熔点为40℃以上的化合物。

6. 发明授权

US06921577B2 Water-based metal surface treatment agent 有权
标题翻译：水性金属表面处理剂
公开(公告)号：US06921577B2
公开(公告)日：2005-07-26
申请号：US10169893
申请日：2002-02-19
申请人： Takashi Ouchi , Katsuyuki Tsuchida , Masashi Kumagai
发明人： Takashi Ouchi , Katsuyuki Tsuchida , Masashi Kumagai
IPC分类号： C08L33/14 , C08L63/00 , C09D133/14 , C09D163/00 , C23C26/00 , C23F11/173 , B32B15/08
CPC分类号： C23C26/00 , Y10T428/31511 , Y10T428/31529
摘要： A water-based metal surface treatment agent for the surface treatment of metals including aluminum products such as pre-coated aluminum sheets gives excellent coating film adhesion, flexibility and acid resistance.The water-based metal surface treatment agent contains the following components (1) to (3): (1) A copolymer, containing in a side chain, a diketene or ketoester capable of switching between keto and enol tautomeric forms, and containing at least one hydrophilic side chain containing a cationic group, an anionic group, or a nonionic group; (2) An epoxy resin modified with a phosphoric acid type compound; and (3) A water-soluble curing agent.
摘要翻译：用于表面处理金属的水性金属表面处理剂，包括铝制品如预涂铝片，提供了优异的涂膜粘附性，柔韧性和耐酸性。水性金属表面处理剂含有以下成分（1）〜（3）：（1）在侧链中含有能够在酮和烯醇互变异构体之间切换的双烯酮或酮酯的共聚物，至少含有一个含有阳离子基团，阴离子基团或非离子基团的亲水侧链; （2）用磷酸型化合物改性的环氧树脂; 和（3）水溶性固化剂。

7. 发明授权

US07824534B2 Copper electrolytic solution containing as additive compound having specific skeleton, and electrolytic copper foil manufactured therewith 有权
标题翻译：含有具有特定骨架的添加剂化合物的铜电解液和由其制造的电解铜箔
公开(公告)号：US07824534B2
公开(公告)日：2010-11-02
申请号：US10588686
申请日：2005-12-09
申请人： Katsuyuki Tsuchida , Hironori Kobayashi , Masashi Kumagai
发明人： Katsuyuki Tsuchida , Hironori Kobayashi , Masashi Kumagai
IPC分类号： C25D3/38
CPC分类号： C25D1/04 , C25D3/38
摘要： The object of the present invention is to obtain a low profile electrolytic copper foil with a low surface roughness at the rough surface side (opposite side from the glossy side) in the electrolytic copper foil manufacture using a cathode drum and, particularly, to obtain an electrolytic copper foil with excellent elongation and tensile strength that permits fine patterning. Another object is to obtain a copper electrolytic solution that allows uniform copper plating without pinholes on a 2-layer flexible substrate. This copper electrolytic solution contains, as an additive, a compound having the specific skeleton represented by General Formula (1) below which is obtained by an addition reaction in which water is added to a compound having in a molecule one or more epoxy groups: wherein A is an epoxy compound residue and n is an integer of 1 or more.
摘要翻译：本发明的目的是在使用阴极鼓的电解铜箔制造中，在粗糙表面侧（与光面相反的一侧）获得具有低表面粗糙度的薄型电解铜箔，特别是获得电解铜箔具有优异的伸长率和拉伸强度，可以进行精细图案化。另一个目的是获得一种铜电解溶液，其允许在2层柔性基板上均匀镀铜而没有针孔。该铜电解液含有作为添加剂的具有下述通式（1）表示的特定骨架的化合物，其通过加成反应获得，其中将水加入到分子中具有一个或多个环氧基的化合物：其中 A是环氧化合物残基，n是1以上的整数。

8. 发明申请

US20100224496A1 Copper electrolytic solution containing as additive compound having specific skeleton, and electrolytic copper foil manufactured therewith 审中-公开
标题翻译：含有具有特定骨架的添加剂化合物的铜电解液和由其制造的电解铜箔
公开(公告)号：US20100224496A1
公开(公告)日：2010-09-09
申请号：US12660199
申请日：2010-02-23
申请人： Katsuyuki Tsuchida , Hironori Kobayashi , Masashi Kumagai
发明人： Katsuyuki Tsuchida , Hironori Kobayashi , Masashi Kumagai
IPC分类号： B32B1/00 , B32B15/04
CPC分类号： C25D1/04 , C25D3/38
摘要： The object of the present invention is to obtain a low profile electrolytic copper foil with low surface roughness at the rough surface side (opposite side from the glossy side) in the electrolytic copper foil manufacture using a cathode drum, and particularly to obtain an electrolytic copper foil with excellent elongation and tensile strength that permits fine patterning. Another object is to obtain a copper electrolytic solution that allows uniform copper plating without pinholes on a 2-layer flexible substrate. This copper electrolytic solution comprises as an additive a compound having the specific skeleton represented by General Formula (1) below which is obtained by an addition reaction in which water is added to a compound having in a molecule one or more epoxy groups: wherein A is an epoxy compound residue and n is an integer of 1 or more.
摘要翻译：本发明的目的是在使用阴极鼓的电解铜箔制造中，在粗糙表面侧（与光泽面相反侧）获得具有低表面粗糙度的低剖面电解铜箔，特别是获得电解铜箔具有优异的伸长率和拉伸强度，允许精细图案化。另一个目的是获得一种铜电解溶液，其允许在2层柔性基板上均匀镀铜而没有针孔。该铜电解液包含作为添加剂的具有下述通式（1）表示的特定骨架的化合物，其通过加成反应获得，其中将水加入到分子中具有一个或多个环氧基的化合物：其中A为环氧化合物残基，n为1以上的整数。

9. 发明授权

US07651783B2 Surface treated copper film 有权
标题翻译：表面处理铜膜
公开(公告)号：US07651783B2
公开(公告)日：2010-01-26
申请号：US10486274
申请日：2002-07-17
申请人： Katsuyuki Tsuchida , Masashi Kumagai , Fumiaki Akase
发明人： Katsuyuki Tsuchida , Masashi Kumagai , Fumiaki Akase
IPC分类号： H05K1/03 , H05K3/38 , H05K3/46 , B32B15/08
CPC分类号： C23C28/00 , C23C30/00 , H05K3/384 , H05K3/389 , Y10T428/12438 , Y10T428/12569 , Y10T428/12611 , Y10T428/12792 , Y10T428/12882 , Y10T428/12903 , Y10T428/1291 , Y10T428/12993 , Y10T428/31663
摘要： A surface treated copper foil with improved adhesion to the insulating resin of a copper-clad laminate for higher frequency applications contains a copper foil provided with a heat-resistant layer and an olefin-based silane coupling agent layer sequentially on at least one side thereof. An anticorrosive treatment may be performed after the heat resistance treatment. The copper foil is preferably an electrolytic copper foil, and these layers can be provided on the S side and/or the M side thereof. The copper foil has an adequate adhesive strength, even without the roughening treatment that has been performed in the past. A film of zinc, zinc-tin, zinc-nickel, zinc-cobalt, copper-zinc, copper-nickel-cobalt, or nickel-cobalt can be used favorably as the heat-resistant layer, and a film that has undergone a zinc-chromate or a chromate treatment can be used favorably as the anticorrosive layer.
摘要翻译：与用于更高频率应用的覆铜层压板的绝缘树脂具有改善的粘合性的表面处理铜箔包含在其至少一侧上依次具有耐热层和烯烃基硅烷偶联剂层的铜箔。耐热处理后可以进行防锈处理。铜箔优选为电解铜箔，这些层可以设置在S侧和/或M侧。铜箔具有足够的粘合强度，即使没有在过去进行的粗糙化处理。可以有利地使用锌，锌 - 锡，锌 - 镍，锌 - 钴，铜 - 锌，铜 - 镍 - 钴或镍 - 钴的薄膜作为耐热层，并且已经经历了锌铬酸盐或铬酸盐处理可以有利地用作防腐层。

10. 发明申请

US20090092789A1 Two-Layer Flexible Substrate 有权
标题翻译：双层柔性基材
公开(公告)号：US20090092789A1
公开(公告)日：2009-04-09
申请号：US11992209
申请日：2006-08-22
申请人： Katsuyuki Tsuchida , Hironori Kobayashi , Ryu Murakami , Masashi Kumagai
发明人： Katsuyuki Tsuchida , Hironori Kobayashi , Ryu Murakami , Masashi Kumagai
IPC分类号： D06N7/04
CPC分类号： H05K1/09 , B32B15/08 , B32B15/20 , B32B27/281 , B32B2307/206 , H05K1/0346 , H05K1/0393 , H05K3/108 , H05K3/28 , H05K3/382 , H05K3/388 , H05K2201/0355 , H05K2201/098 , H05K2203/0723 , Y10T428/24355
摘要： The invention provides a two-layer flexible substrate free of surface defects and having excellent etching characteristics and adherence to resist.The two-layer flexible substrate has a copper layer provided on one or both faces of an insulator film without using an adhesive, wherein the surface roughness (Ra) of the copper layer is 0.10 to 0.25 μm, and wherein the average crystal grain size [of copper] is no greater than 0.8 μm at 1 μm from the insulator film in the cross section of the copper layer. Preferably, the insulator film is a polyimide film.
摘要翻译：本发明提供一种没有表面缺陷且具有优异的蚀刻特性和抗粘附性的双层柔性基材。双层柔性基板在不使用粘合剂的情况下，在绝缘膜的一面或两面上具有铜层，其中铜层的表面粗糙度（Ra）为0.10〜0.25μm，平均结晶粒径[ 的铜]在铜层的截面中距离绝缘膜1个1um时不大于0.8μm。优选地，绝缘膜是聚酰亚胺膜。

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