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1. 发明申请

US20130068256A1 Longitudinal Solid-Liquid Countercurrent Contact Method, Method of Washing Solid Particles, Method of Manufacturing Poly(Arylene Sulfide) and Apparatus 审中-公开
标题翻译：纵向固液反向接触法，固体颗粒洗涤方法，聚（亚硫酰基）制备方法及装置
公开(公告)号：US20130068256A1
公开(公告)日：2013-03-21
申请号：US13699143
申请日：2011-04-20
申请人： Masanori Kobayashi , Hirohito Kawama , Koichi Suzuki , Mitsuhiro Matsuzaki
发明人： Masanori Kobayashi , Hirohito Kawama , Koichi Suzuki , Mitsuhiro Matsuzaki
IPC分类号： B08B3/04
CPC分类号： B08B3/041 , B01J8/10 , B01J19/0066 , B01J19/18 , B01J2219/00765 , B01J2219/00779 , C08G75/025
摘要： A longitudinal solid-liquid countercurrent contact method and apparatus are provided in which an aqueous slurry containing solid particles is supplied from an upper part and is caused to pass through a plurality of contact-processing chambers connected in a vertical direction while being caused to proceed downward, a contacting liquid is supplied from a lower part and is caused to pass through the plurality of contact-processing chambers connected in the vertical direction while being caused to proceed upward, and the aqueous slurry and the contacting liquid are caused to be continuously subjected to countercurrent contact, wherein the viscosity of a liquid phase in at least one of the contact-processing chambers is controlled, and especially the viscosity η1 of a liquid phase in a contact-processing chamber positioned at an uppermost part is controlled to fall within a range of 0.9≦η1/η0≦2.0 with respect to the reference viscosity η0 as the viscosity of a predetermined reference composition of a liquid phase at a predetermined temperature.
摘要翻译：提供了一种纵向固液逆流接触方法和装置，其中含有固体颗粒的含水浆料从上部供应并使其通过在垂直方向上连接的多个接触处理室，同时使其向下从下部供给接触液体，使其在垂直方向上连续通过的多个接触处理室通过，同时使上述水性浆料和接触液体连续地进行逆流接触，其中控制至少一个接触处理室中的液相的粘度，特别是控制位于最上部的接触处理室中的液相的粘度等于1 相对于参考粘度＆eegr; 0作为p的粘度，范围为0.9＆nlE;＆eegr; 1 / eegr; 0＆nlE; 2.0 在预定温度下液相的重新确定的参考组合物。

2. 发明授权

US08211997B2 Process for producing polyarylene sulfide 有权
标题翻译：生产聚芳硫醚的方法
公开(公告)号：US08211997B2
公开(公告)日：2012-07-03
申请号：US11661753
申请日：2005-08-31
申请人： Mitsuhiro Matsuzaki , Katsumi Horikoshi , Masanori Kobayashi
发明人： Mitsuhiro Matsuzaki , Katsumi Horikoshi , Masanori Kobayashi
IPC分类号： C08G75/00
CPC分类号： C08G75/0254 , C08G75/02
摘要： In a process for producing polyarylene sulfide, comprising: reacting an alkali sulfide source and an aromatic dihalide compound in a polar organic solvent to obtain a polymerizate slurry containing polyarylene sulfide particles, by-produced alkali metal salt fine particles and the polar organic solvent, and recovering the polyarylene sulfide particles washed from the polymerizate slurry; the polymerizate slurry is separated by sieving into the polyarylene sulfide particles and a slurry containing the alkali metal salt fine particles, and the separated polyarylene sulfide particles are subjected to a washing step wherein the polyarylene sulfides are introduced into a countercurrent washing apparatus enclosing a movable part and subjected therein to continuous countercurrent contact with a washing liquid. As a result, polyarylene sulfide particles of good quality are produced at a good yield, while pursuing process rationalization.
摘要翻译：在制备聚芳硫醚的方法中，包括：将碱金属硫化物源和芳族二卤化物在极性有机溶剂中反应，得到含有聚芳硫醚颗粒，副产的碱金属盐微粒和极性有机溶剂的聚合物淤浆，以及回收从聚合物浆料洗涤的聚芳硫醚颗粒; 将聚合物浆料通过筛分分离成聚芳硫醚颗粒和含有碱金属盐微粒的浆料，并将分离的聚芳硫醚颗粒进行洗涤步骤，其中将聚亚芳基硫化物引入到包围可动部分的逆流洗涤装置中并与其进行与洗涤液的连续逆流接触。结果，在追求工艺合理化的同时，以良好的产率生产质量好的聚芳硫醚颗粒。

3. 发明申请

US20080097075A1 Process for Producing Polyarylene Sulfide 有权
标题翻译：生产聚亚芳基硫化物的方法
公开(公告)号：US20080097075A1
公开(公告)日：2008-04-24
申请号：US11661753
申请日：2005-08-31
申请人： Mitsuhiro Matsuzaki , Katsumi Horikoshi , Masanori Kobayashi
发明人： Mitsuhiro Matsuzaki , Katsumi Horikoshi , Masanori Kobayashi
IPC分类号： C08G75/14
CPC分类号： C08G75/0254 , C08G75/02
摘要： In a process for producing polyarylene sulfide, comprising: reacting an alkali sulfide source and an aromatic dihalide compound in a polar organic solvent to obtain a polymerizate slurry containing polyarylene sulfide particles, by-produced alkali metal salt fine particles and the polar organic solvent, and recovering the polyarylene sulfide particles washed from the polymerizate slurry; the polymerizate slurry is separated by sieving into the polyarylene sulfide particles and a slurry containing the alkali metal salt fine particles, and the separated polyarylene sulfide particles are subjected to a washing step wherein the polyarylene sulfides are introduced into a countercurrent washing apparatus enclosing a movable part and subjected therein to continuous countercurrent contact with a washing liquid. As a result, polyarylene sulfide particles of good quality are produced at a good yield, while pursuing process rationalization.
摘要翻译：在制备聚芳硫醚的方法中，包括：将碱金属硫化物源和芳族二卤化物在极性有机溶剂中反应，得到含有聚芳硫醚颗粒，副产的碱金属盐微粒和极性有机溶剂的聚合物淤浆，以及回收从聚合物浆料洗涤的聚芳硫醚颗粒; 将聚合物浆料通过筛分分离成聚芳硫醚颗粒和含有碱金属盐微粒的浆料，并将分离的聚芳硫醚颗粒进行洗涤步骤，其中将聚亚芳基硫化物引入到包围可动部分的逆流洗涤装置中并与其进行与洗涤液的连续逆流接触。结果，在追求工艺合理化的同时，以良好的产率生产质量好的聚芳硫醚颗粒。

4. 发明授权

US09068047B2 Process for producing poly(arylene sulfide), and poly(arylene sulfide) comprising contacting a wash liquid with an alkaline compound 有权
标题翻译：包括使洗涤液与碱性化合物接触的制备聚（亚芳基硫醚）和聚（亚芳基硫醚）的方法
公开(公告)号：US09068047B2
公开(公告)日：2015-06-30
申请号：US13698600
申请日：2011-04-21
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/02 , C08G75/14
CPC分类号： C08G75/0254 , C08G75/0213 , C08G75/0259 , C08G75/0281 , Y10T428/2982
摘要： Disclosed is a process for producing poly(arylene sulfide) which includes: a polymerization step of polymerizing a dihalogenated aromatic compound and at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrogen sulfides in an organic amide solvent, preferably in the presence of a phase separating agent; a separation step of separating a polymer from a reaction liquid containing a produced polymer after the polymerization step; a washing step of washing the polymer with a washing liquid that consists of water and/or an organic solvent; and a separated liquid treatment step of bringing both a separated liquid that has been recovered after the separation of the polymer in the separation step and a separated liquid containing a wash waste liquid that has been recovered after the separation of the polymer in the washing step into contact with an alkaline compound. Also disclosed is poly(arylene sulfide).
摘要翻译：公开了一种生产聚（亚芳基硫醚）的方法，其包括：在有机酰胺溶剂中聚合二卤代芳族化合物和至少一种选自碱金属硫化物和碱金属硫化氢的硫源的聚合步骤，优选在相分离剂的存在下; 在聚合步骤之后从含有生成的聚合物的反应液中分离聚合物的分离步骤; 用由水和/或有机溶剂组成的洗涤液洗涤聚合物的洗涤步骤; 以及分离液体处理步骤，在分离步骤中分离聚合物之后已经回收的分离液体和在洗涤步骤中分离聚合物之后已经回收的含有洗涤废液的分离液体进入与碱性化合物接触。还公开了聚（亚芳基硫醚）。

5. 发明申请

US20130065054A1 Process for Producing Poly(Arylene Sulfide), and Poly(Arylene Sulfide) 有权
标题翻译：生产聚（亚硫酰亚胺）和聚（亚硫酰亚胺）的方法
公开(公告)号：US20130065054A1
公开(公告)日：2013-03-14
申请号：US13698600
申请日：2011-04-21
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/16
CPC分类号： C08G75/0254 , C08G75/0213 , C08G75/0259 , C08G75/0281 , Y10T428/2982
摘要： Disclosed is a process for producing poly(arylene sulfide) which includes: a polymerization step of polymerizing a dihalogenated aromatic compound and at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrogen sulfides in an organic amide solvent, preferably in the presence of a phase separating agent; a separation step of separating a polymer from a reaction liquid containing a produced polymer after the polymerization step; a washing step of washing the polymer with a washing liquid that consists of water and/or an organic solvent; and a separated liquid treatment step of bringing both a separated liquid that has been recovered after the separation of the polymer in the separation step and a separated liquid containing a wash waste liquid that has been recovered after the separation of the polymer in the washing step into contact with an alkaline compound. Also disclosed is poly(arylene sulfide).
摘要翻译：公开了一种生产聚（亚芳基硫醚）的方法，其包括：在有机酰胺溶剂中聚合二卤代芳族化合物和至少一种选自碱金属硫化物和碱金属硫化氢的硫源的聚合步骤，优选在相分离剂的存在下; 在聚合步骤之后从含有生成的聚合物的反应液中分离聚合物的分离步骤; 用由水和/或有机溶剂组成的洗涤液洗涤聚合物的洗涤步骤; 以及分离液体处理步骤，在分离步骤中分离聚合物之后已经回收的分离液体和在洗涤步骤中分离聚合物之后已经回收的含有洗涤废液的分离液体进入与碱性化合物接触。还公开了聚（亚芳基硫醚）。

6. 发明授权

US09096723B2 Production process of poly(arylene sulfide) and poly(arylene sulfide) 有权
标题翻译：聚（亚芳基硫醚）和聚（亚芳基硫醚）的生产工艺
公开(公告)号：US09096723B2
公开(公告)日：2015-08-04
申请号：US13989714
申请日：2011-10-18
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Takayuki Kimura , Koichi Suzuki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Takayuki Kimura , Koichi Suzuki
IPC分类号： C08G75/16 , C08G75/02
CPC分类号： C08G75/16 , C08G75/02
摘要： A production process of a poly(arylene sulfide), including (a) a polymerization step of polymerizing at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrosulfides and a dihalo-aromatic compound in an organic amide solvent to form a polymer; (b) a separation step of separating the polymer from a liquid reaction mixture containing the polymer formed after the polymerization step; (c) a washing step of washing the polymer with at least one washing liquid selected from the group consisting of water, an organic solvent and a mixed solution of water and an organic solvent as desired; and (d) an aqueous oxidizing solution treatment step of treating the polymer by bringing the polymer into contact with an aqueous oxidizing solution.
摘要翻译：一种聚（亚芳基硫醚）的制造方法，包括（a）聚合步骤，将选自碱金属硫化物和碱金属氢硫化物中的至少一种硫源和二卤代芳族化合物在有机酰胺溶剂中聚合，形成聚合物; （b）从含有聚合步骤后形成的聚合物的液体反应混合物分离聚合物的分离步骤; （c）洗涤步骤，根据需要用至少一种选自水，有机溶剂和水与有机溶剂的混合溶液的洗涤液洗涤聚合物; 和（d）通过使聚合物与氧化水溶液接触来处理聚合物的水性氧化溶液处理步骤。

7. 发明申请

US20130253147A1 Production Process of Poly(Arylene Sulfide) and Poly(Arylene Sulfide) 有权
标题翻译：聚（亚硫酰基）和聚（亚硫酰基）的生产工艺
公开(公告)号：US20130253147A1
公开(公告)日：2013-09-26
申请号：US13989714
申请日：2011-10-18
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Takayuki Kimura , Koichi Suzuki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Takayuki Kimura , Koichi Suzuki
IPC分类号： C08G75/16
CPC分类号： C08G75/16 , C08G75/02
摘要： A production process of a poly(arylene sulfide), including (a) a polymerization step of polymerizing at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrosulfides and a dihalo-aromatic compound in an organic amide solvent to form a polymer; (b) a separation step of separating the polymer from a liquid reaction mixture containing the polymer formed after the polymerization step; (c) a washing step of washing the polymer with at least one washing liquid selected from the group consisting of water, an organic solvent and a mixed solution of water and an organic solvent as desired; and (d) an aqueous oxidizing solution treatment step of treating the polymer by bringing the polymer into contact with an aqueous oxidizing solution.
摘要翻译：一种聚（亚芳基硫醚）的制造方法，包括（a）聚合步骤，将选自碱金属硫化物和碱金属氢硫化物中的至少一种硫源和二卤代芳族化合物在有机酰胺溶剂中聚合，形成聚合物; （b）从含有聚合步骤后形成的聚合物的液体反应混合物分离聚合物的分离步骤; （c）洗涤步骤，根据需要用至少一种选自水，有机溶剂和水与有机溶剂的混合溶液的洗涤液洗涤聚合物; 和（d）通过使聚合物与氧化水溶液接触来处理聚合物的水性氧化溶液处理步骤。

8. 发明授权

US08846574B2 Granular fertilizer containing herbicidal agrochemical 有权
标题翻译：含有除草农药的颗粒肥料
公开(公告)号：US08846574B2
公开(公告)日：2014-09-30
申请号：US13264591
申请日：2010-04-06
申请人： Masanori Kobayashi , Taiji Kikuchi , Toshihiro Ikeuchi
发明人： Masanori Kobayashi , Taiji Kikuchi , Toshihiro Ikeuchi
IPC分类号： A01N25/12 , A01P13/00 , C05G3/02 , A01N43/80 , C05G3/00
CPC分类号： A01N43/80 , C05G3/0041 , C05G3/02 , A01N25/02 , A01N25/12 , A01N25/14
摘要： Disclosed is a technique for achieving a required herbicidal effect using a small amount of a herbicide. Specifically disclosed are: a granular fertilizer containing a herbicidal agrochemical, which is characterized in that the granular fertilizer has been impregnated or coated with pyroxasulfone; and a weed eradication method which is characterized by applying the granular fertilizer to fields.
摘要翻译：公开了一种使用少量除草剂实现所需除草效果的技术。具体公开的是：含有除草农药的颗粒肥料，其特征在于，颗粒肥料已经用pyroxasulfone浸渍或涂覆; 其特征在于将颗粒肥施用于田地。

9. 发明申请

US20140084668A1 EXCAVATION MACHINE 有权
标题翻译：挖掘机
公开(公告)号：US20140084668A1
公开(公告)日：2014-03-27
申请号：US14112793
申请日：2012-06-27
申请人： Masanori Kobayashi , Kazuya Kokai , Yasuharu Hanaoka
发明人： Masanori Kobayashi , Kazuya Kokai , Yasuharu Hanaoka
IPC分类号： E21D9/11
CPC分类号： E21D9/112
摘要： An excavation machine having a cutter head with a large diameter while making it possible to excavate excavation objects such as hard bedrock etc. with high efficiency is provided. The excavation machine comprises an outer circumference cutter head 20 having a circular opening and being rotated and contacted to excavation objects and a small diameter cutter head 23 disposed in the opening and rotatable independently from the outer circumference cutter head. Rotation centers of the rotation disk and the rotation plate are gapped and the gap is shorter than a rotation radius of the small diameter cutter head.
摘要翻译：提供了具有大直径的切割头的挖掘机，同时能够高效率地挖掘诸如硬质基岩等挖掘对象。挖掘机包括具有圆形开口并与挖掘物体旋转接触的外圆周切割头20和设置在开口中并与外周切割头独立旋转的小直径刀头23。旋转盘和旋转板的旋转中心被间隙并且间隙比小直径刀头的旋转半径短。

10. 发明授权

US08593631B2 Spectral image acquiring apparatus 有权
标题翻译：光谱图像采集装置
公开(公告)号：US08593631B2
公开(公告)日：2013-11-26
申请号：US13275572
申请日：2011-10-18
申请人： Hideaki Hirai , Masanori Kobayashi
发明人： Hideaki Hirai , Masanori Kobayashi
IPC分类号： G01J3/40 , G01J3/45 , G01B9/02
CPC分类号： G01J3/2823 , G01J3/02 , G01J3/0208 , G01J3/0224 , G01J3/0229 , G01J3/0259 , G02B5/1814 , G02B5/20
摘要： A spectral image acquiring apparatus includes an optical filter on which light is incident; an image sensor including a two-dimensionally disposed pixel array for detecting the light via the optical filter; and a signal processing unit generating a difference-value image based on a detection signal from the image sensor. The optical filter includes a diffraction grating having a lattice pattern corresponding to one or more pixels on the image sensor. The signal processing unit calculates a difference value in an amount of received light between two adjacent pixels based on the detection signal from the image sensor, and generates the difference-value image based on the difference value. The difference value between the two adjacent pixels is varied depending on a difference in an interference point on the image sensor corresponding to a diffraction angle of the light that has passed through the diffraction grating.
摘要翻译：光谱图像获取装置包括光入射的滤光器; 图像传感器，包括用于经由滤光器检测光的二维布置的像素阵列; 以及信号处理单元，其基于来自图像传感器的检测信号生成差值图像。光学滤波器包括具有对应于图像传感器上的一个或多个像素的格子图案的衍射光栅。信号处理单元基于来自图像传感器的检测信号计算两个相邻像素之间的接收光量的差值，并基于差值生成差值图像。两个相邻像素之间的差值取决于对应于已经通过衍射光栅的光的衍射角的图像传感器上的干涉点的差异。

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