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1. 发明授权

US4549982A 1-Oxoalkyl-2-isopropylnorbornane derivatives, uses thereof in augmenting or enhancing the aroma of consumable materials and processes for preparing same 失效
标题翻译： 1-氧代烷基-2-异丙基降冰片烷衍生物，其用于增强或增强消耗材料的香气及其制备方法
公开(公告)号：US4549982A
公开(公告)日：1985-10-29
申请号：US644058
申请日：1984-08-24
申请人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553 , C11B9/00 , C07C49/115 , A61K7/46
CPC分类号： C11B9/0046 , C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553
摘要： Described are 1-oxoalkyl-2-isopropylnorbornane derivatives defined according to the generic structure: ##STR1## wherein X represents a moiety selected from the group consisting of: ##STR2## wherein the dashed line represents a carbon-carbon double bond or a carbon-carbon single bond and wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that R.sub.1 and R.sub.2 are not both methyl, and uses thereof in augmenting or enhancing the aroma of consumable materials selected from the group consisting of perfume compositions, colognes and perfumed articles. Also described are processes for preparing said 1-oxoalkyl-2-isopropylnorbornane derivatives by means of a low temperature catalytic Diels Alder reaction or high temperature thermal Diels Alder reaction between a bicyclopentadiene derivative and 2-methyl-3- buten-5-one according to the reaction: ##STR3## wherein R represents methyl or hydrogen.
摘要翻译：描述根据以下通用结构定义的1-氧代烷基-2-异丙基降冰片烷衍生物：其中X表示选自以下的部分：其中虚线表示碳 - 碳双键或碳 - 碳单键，其中R 1和R 2表示氢或甲基，条件是R 1和R 2不是甲基，以及其用于增强或增强从由香料组合物，古龙水和香料制品组成的组中选择的可消耗材料的香气的用途。还描述了通过低温催化Diels Alder反应或双环戊二烯衍生物与2-甲基-3-丁烯-5-酮之间的高温热狄尔斯阿尔德反应制备所述1-氧代烷基-2-异丙基降冰片烷衍生物的方法，根据反应：其中R表示甲基或氢。

2. 发明授权

US4524020A Isopropyl substituted cyclohexenyl methyl ketones and perfumery uses thereof 失效
标题翻译：异丙基取代的环己烯基甲基酮及其香料用途
公开(公告)号：US4524020A
公开(公告)日：1985-06-18
申请号：US643827
申请日：1984-08-24
申请人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C45/69 , C07C49/543 , C11B9/00 , A61K7/46 , C07C49/21
CPC分类号： C11B9/0034 , C07C45/69 , C07C49/543
摘要： Described are isopropyl substituted cyclohexenyl methyl ketones defined according to the structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.11 and R.sub.21 each represents hydrogen or methyl with the provisos that:(a) at least two of R.sub.1, R.sub.21, R.sub.2 and R.sub.11 represent hydrogen;(b) either R.sub.2 is methyl and R.sub.21 is hydrogen or R.sub.21 is methyl and R.sub.2 is hydrogen; and(c) R.sub.1 is methyl only when R.sub.2 is methyl and R.sub.11 is methyl only when R.sub.21 is methyl,as well as uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers.
摘要翻译：描述了根据以下结构定义的异丙基取代的环己烯基甲基酮：其中R 1，R 2，R 11和R 21各自表示氢或甲基，条件是：（a）R 1，R 21，R 2和R 11中的至少两个表示氢 ; （b）R2是甲基，R21是氢或R21是甲基，R2是氢; 和（c）仅当R 2为甲基时，R 1为甲基，R 21为甲基时，R 21为甲基时，R 11为甲基，以及其用于增强或增强香料组合物，古龙水和香料的芳香物质的用途，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂和加香聚合物。

3. 发明授权

US4572796A 1,1,4,7-Tetramethyl-3-indanone, product produced thereby and organoleptic uses thereof 失效
标题翻译： 1,1,4,7-四甲基-3-二氢茚酮，由此生产的产品及其感官用途
公开(公告)号：US4572796A
公开(公告)日：1986-02-25
申请号：US671407
申请日：1984-11-14
申请人： Augustinus G. van Loveren , Mark A. Sprecker , Patrick Whelan , Marie R. Hanna
发明人： Augustinus G. van Loveren , Mark A. Sprecker , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/36 , C07C49/67 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0049 , C07C45/36 , C07C49/67 , C07C2102/08
摘要： Described is a process for producing 1,1,4,7-tetramethyl-3-indanone defined according to the structure: ##STR1## the 1,1,4,7-tetramethyl-3-indanone per se and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles and colognes.
摘要翻译：描述了根据以下结构限定的1,1,4,7-四甲基-3-二氢茚酮的方法：本文所述的1,1,4,7-四甲基-3-二氢茚酮及其增感的感官用途或增强香水组合物，香水制品和古龙水的香气。

4. 发明授权

US4532357A Process for producing 1,1-dimethyl-3-indanones, products produced thereby and organoleptic uses thereof 失效
标题翻译：制备1,1-二甲基-3-茚满酮的方法，由此生产的产品及其感官用途
公开(公告)号：US4532357A
公开(公告)日：1985-07-30
申请号：US613570
申请日：1984-05-24
申请人： Augustinus G. van Loveren , Mark A. Sprecker , Patrick Whelan , Marie R. Hanna
发明人： Augustinus G. van Loveren , Mark A. Sprecker , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C2/72 , C07C45/36 , C07C49/67 , C11B9/00 , C07C49/15 , A61K7/46
CPC分类号： C11B9/0049 , C07C2/72 , C07C45/36 , C07C49/67 , C07C2102/08
摘要： Described is a process for producing 1,1-dimethyl-3-indanones defined according to the structure: ##STR1## wherein R.sub.1 and R.sub.2 are the same or different and each represents hydrogen or methyl with the proviso that at least one of R.sub.1 and R.sub.2 methyl, products produced thereby and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles and colognes.
摘要翻译：描述了根据以下结构定义的1,1-二甲基-3-茚满酮的方法：其中R 1和R 2相同或不同，并且各自表示氢或甲基，条件是R 1和R 2中的至少一个甲基，由此产生的产品及其感官用途，以增强或增强香水组合物，香料制品和古龙水的香味。

5. 发明授权

US5023352A Alkyl-substituted tetra- or hexahydrobenzopyran derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：烷基取代的四或六氢苯并吡喃衍生物，其感官用途及其制备方法
公开(公告)号：US5023352A
公开(公告)日：1991-06-11
申请号：US546356
申请日：1990-06-29
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
IPC分类号： C07D311/74 , C07D311/94 , C11B9/00 , C11D3/50
CPC分类号： C07D311/74 , C07D311/94 , C11B9/008 , C11D3/50
摘要： Described are alkyl-substituted tetra- or hexahydrobenzopyran derivatives defined according to one of the generic structures: ##STR1## wherein Z is a moiety in the alternative either ##STR2## wherein in the moiety having the structure: ##STR3## R' is methyl or ethyl and in the moiety having the structure: ##STR4## one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represent carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 taken separately represent hydrogen or C.sub.1 -C.sub.3 lower alkyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) or R.sub.1 and R.sub.2 taken together complete a C.sub.5 or C.sub.6 cycloalkyl moiety; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, cosmetic powder and perfumed polymers. Also described are synthesis processes for preparing such alkyl-substituted tetra- or hexahydrobenzopyran derivatives by means of reacting isopulegol or an isomer thereof with an acetal or ketal.
摘要翻译：描述了根据以下通用结构之一定义的烷基取代的四或六氢苯并吡喃衍生物：其中Z是可选择的部分或其中的“IMAGE”或“IMAGE”，其中在具有以下结构的部分中： R'是甲基或乙基，并且在具有以下结构的部分中：虚线之一是碳 - 碳双键，虚线中的每一个代表碳 - 碳单键; 其中R1和R2分别代表氢或C1-C3低级烷基（前提是R1和R2不同时为氢）或R1和R2一起形成C5或C6环烷基部分; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，毛发制剂，化妆品粉末和加香聚合物的香料组合物，古龙水和香料制品的香气。。还描述了通过异丙醇或其异构体与缩醛或缩酮反应制备这种烷基取代的四或六氢苯并吡喃衍生物的合成方法。

6. 发明授权

US4772583A Beta-alkylidene phenethyl alcohol esters and ethers, organoleptic uses thereof and processes for preparing same 失效
标题翻译： β-亚烷基苯乙醇酯和醚，其感官用途及其制备方法
公开(公告)号：US4772583A
公开(公告)日：1988-09-20
申请号：US134817
申请日：1987-12-18
申请人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0061
摘要： Described is the novel compound genus the beta-alkylidene phenethyl alcohol esters and ethers of our invention defined according to the generic structure: ##STR1## wherein R.sub.5 represents hydrogen or methyl; wherein R.sub.6 represents one of the moieties: ##STR2## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 each represents the same or different hydrogen or methyl; wherein R.sub.7 represents methyl or ethyl; and wherein R.sub.8 represents hydrogen or methyl; useful in augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener articles, fabric softener compositions, cosmetic powders and hair preparations.
摘要翻译：描述了根据通用结构定义的本发明的β-亚烷基苯乙醇酯和醚的新化合物：其中R 5表示氢或甲基; 其中R 6表示以下部分之一：其中R 1，R 2，R 3和R 4各自表示相同或不同的氢或甲基; 其中R 7表示甲基或乙基; 并且其中R8表示氢或甲基; 可用于增强或增强消耗材料的香气，包括香料，古龙水和加香制品，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂制品，织物柔软剂组合物，化妆粉和头发制剂。

7. 发明授权

US4460795A Process for preparing mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4460795A
公开(公告)日：1984-07-17
申请号：US478355
申请日：1983-03-24
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C93/16
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "', R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "', R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "' and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

8. 发明授权

US4999439A Alkyl-substituted tetra- or hexahydrobenzopyran derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：烷基取代的四或六氢苯并吡喃衍生物，其感官用途及其制备方法
公开(公告)号：US4999439A
公开(公告)日：1991-03-12
申请号：US497693
申请日：1990-03-22
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
IPC分类号： C07D311/74 , C07D311/94 , C11B9/00 , C11D3/50
CPC分类号： C07D311/94 , C07D311/74 , C11B9/008 , C11D3/50
摘要： Described are alkyl-substituted tetra- or hexahydrobenzopyran derivatives defined according to one of the generic structures: ##STR1## wherein Z is a moiety in the alternative either ##STR2## wherein in the moiety having the structure: ##STR3## R' is methyl or ethyl and in the moiety having the structure: ##STR4## one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represent carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 taken separately represent hydrogen or C.sub.1 -C.sub.3 lower alkyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) or R.sub.1 and R.sub.2 taken together complete a C.sub.5 or C.sub.6 cycloalkyl moiety; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, cosmetic powders and perfumed polymers. Also described are synthesis processes for preparing such alkyl-substituted tetra- or hexahydrobenzopyran derivatives by means of reacting isopulegol or an isomer thereof with an acetal or ketal.
摘要翻译：描述了根据以下通用结构之一定义的烷基取代的四或六氢苯并吡喃衍生物：其中Z是可选择的部分或其中的“IMAGE”或“IMAGE”，其中在具有以下结构的部分中： R'是甲基或乙基，并且在具有以下结构的部分中：虚线之一是碳 - 碳双键，虚线中的每一个代表碳 - 碳单键; 其中R1和R2分别代表氢或C1-C3低级烷基（条件是R1和R2不同时为氢）或R1和R2一起形成C5或C6环烷基部分; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，毛发制品，化妆粉和加香聚合物的香料组合物，古龙水和香料制品的香气。。还描述了通过异丙醇或其异构体与缩醛或缩酮反应制备这种烷基取代的四或六氢苯并吡喃衍生物的合成方法。

9. 发明授权

US4962090A 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers, process for preparing same and perfumery uses thereof 失效
标题翻译： 2,4-二取代和2,2,4-三取代的四氢吡喃基-4-醚，其制备方法和香料用途
公开(公告)号：US4962090A
公开(公告)日：1990-10-09
申请号：US497593
申请日：1990-03-22
申请人： Mark A. Sprecker , Robert P. Belko , Salvatore M. Brucato , Charles E. J. Beck , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Salvatore M. Brucato , Charles E. J. Beck , Marie R. Hanna
IPC分类号： C07D309/10 , C07D311/96 , C11B9/00
CPC分类号： C07D311/96 , C07D309/10 , C11B9/008
摘要： Described are 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers defined according to the generic structure: ##STR1## wherein R' represents methyl or ethyl; R.sub.1 and R.sub.2 taken alone are the same or different hydrogen, phenyl, C.sub.1 -C.sub.8 alkyl or C.sub.2 -C.sub.8 alkenyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) and R.sub.1 and R.sub.2 taken together represent C.sub.5 -C.sub.12 cycloalkyl or alkyl cycloalkyl, and reaction products containing said 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers taken alone or taken further together in admixture with compounds defined according to the generic structure: ##STR2## wherein in the compounds defined according to the structure: ##STR3## one of the dashed lines in the moiety: ##STR4## represents a carbon-carbon double bond and each of the other dashed lines represent carbon-carbon single bonds; and R.sub.1 ' and R.sub.2 ' taken alone or taken together are defined in the same manner that R.sub.1 and R.sub.2 are defined, supra; and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to bleach compositions, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfume polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述根据通用结构定义的2,4-二取代的和2,2,4-三取代的四氢吡喃基-4-醚：其中R'表示甲基或乙基; 单独使用的R1和R2是相同或不同的氢，苯基，C1-C8烷基或C2-C8烯基（前提是R1和R2不同时为氢），R1和R2一起代表C5-C12环烷基或烷基环烷基，以及含有所述2,4-二取代的和2,2,4-三取代的四氢吡喃基-4-醚的反应产物，其独立地取代或进一步进一步与根据一般结构定义的化合物混合：其中在根据结构：部分中的虚线之一：表示碳 - 碳双键，并且每个其它虚线表示碳 - 碳单键; 单独或一起取代的R 1'和R 2'以与上述定义R 1和R 2相同的方式定义; 包括但不限于漂白组合物，固体或液体阴离子型，阳离子型，非离子型或两性离子型洗涤剂，香料聚合物，织物柔软剂组合物，织物柔软剂制品，化妆品的香料，以及增强或增强香水组合物，古龙水和香料制品的香气的感官用途粉末和头发制剂。

10. 发明授权

US4924026A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4924026A
公开(公告)日：1990-05-08
申请号：US392423
申请日：1989-08-11
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0015 , C07C33/025 , C07C67/11 , C11D3/50
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4--4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen, and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢，R1“和R2”不是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

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