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1. 发明授权

US06635729B1 Process for the preparation of water-soluble &pgr;-conjugated polymers 有权
标题翻译：制备水溶性π-共轭聚合物的方法
公开(公告)号：US06635729B1
公开(公告)日：2003-10-21
申请号：US09767474
申请日：2001-01-23
申请人： Lambertus Groenendaal , Friedrich Jonas , Tom Cloots , Frank Louwet
发明人： Lambertus Groenendaal , Friedrich Jonas , Tom Cloots , Frank Louwet
IPC分类号： C08F12806
CPC分类号： C08G61/126 , H01B1/127 , H01G9/028 , H01G11/48 , H01G11/56 , Y02E60/13
摘要： The invention relates to a process for preparing water-soluble &pgr;-conjugated polymers by polymerizing, in aqueous solution using an oxidant, monomeric thiophene derivatives of formula (I) wherein X and Y are identical or different and are O, S, or N—R′, Z is —(CH2)m—CR2R3—(CH2)n—, R1 is aryl, C1-C18-alkyl, or hydrogen, R2 is hydrogen or —CH2)s—O—(CH2)p—SO3−M+, R3 is —(CH2)s—O—(CH2)p—SO3−M+, M+ is a cation, m and n are identical or different and are an integer from 0 to 3, s is an integer from 0 to 10, and p is an integer from 1 to 1.
摘要翻译：本发明涉及通过在水溶液中使用氧化剂，其中X和Y相同或不同且为O，S或N-R的式（I）的单体噻吩衍生物进行聚合来制备水溶性π-共轭聚合物的方法 '，Z是 - （CH 2）m-CR 2 R 3 - （CH 2）n - ，R 1是芳基，C 1 -C 18烷基或氢，R 2是氢或-CH 2 ）sO-（CH 2）p -SO 3 - ，M +，R 3是 - （CH 2）s O-（CH 2）p -SO 3 M +，M +是阳离子， m和n相同或不同，为0〜3的整数，s为0〜10的整数，p为1〜1的整数。

2. 发明授权

US06197418B1 Electroconductive glass laminate 有权
标题翻译：导电玻璃层压板
公开(公告)号：US06197418B1
公开(公告)日：2001-03-06
申请号：US09458829
申请日：1999-12-13
申请人： Tom Cloots , Frank Louwet , Hieronymus Andriessen , Bart Verlinden , Jean-Pierre Tahon , Leo Vermeulen , Luc Leenders , Rudi Goedeweeck
发明人： Tom Cloots , Frank Louwet , Hieronymus Andriessen , Bart Verlinden , Jean-Pierre Tahon , Leo Vermeulen , Luc Leenders , Rudi Goedeweeck
IPC分类号： B32B1710
CPC分类号： H05B33/28 , H01L51/5203 , Y10T428/26 , Y10T428/265 , Y10T428/266 , Y10T428/31507 , Y10T428/31616 , Y10T428/31627 , Y10T428/3163 , Y10T428/31645 , Y10T428/31649
摘要： A material is disclosed which comprises a substrate and an organic electroconductive layer provided on said substrate, characterised in that the substrate is a laminate comprising a glass layer and a support. The glass layer is preferably a flexible glass layer having a thickness from 10 to 500 &mgr;m. The material can be used as an electrode in electric or semiconductor devices thereby providing an improved lifetime, e.g. displays, photovoltaic cells or light-emitting diodes.
摘要翻译：公开了一种材料，其包括基板和设置在所述基板上的有机导电层，其特征在于，所述基板是包括玻璃层和支撑体的层压体。玻璃层优选为厚度为10〜500μm的柔性玻璃层。该材料可以用作电或半导体器件中的电极，从而提供改善的寿命，例如，显示器，光伏电池或发光二极管。

3. 发明授权

US06333145B1 Method for preparing a conductive polythiophene layer at low temperature 有权
标题翻译：在低温下制备导电聚噻吩层的方法
公开(公告)号：US06333145B1
公开(公告)日：2001-12-25
申请号：US09433971
申请日：1999-11-04
申请人： Tom Cloots , Johan Loccufier , Frank Louwet , Hieronymus Andriessen
发明人： Tom Cloots , Johan Loccufier , Frank Louwet , Hieronymus Andriessen
IPC分类号： G03C185
CPC分类号： H01B1/127 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/5203 , Y02E60/13
摘要： A method for producing a polymeric conductive layer on an object comprising the steps of: providing an aqueous composition containing a polythiophene, a polyanion compound and an aprotic compound with a dielectric constant, &egr;, ≧15, applying said composition to said object forming a layer and drying said layer to form a conductive polymeric layer on said object, characterised in that during said production said object and said layer are kept at a temperature below 100° C. and said conductive polymeric layer has a resistivity of at most 2 k&OHgr;/square.
摘要翻译：一种用于在物体上制备聚合物导电层的方法，包括以下步骤：提供含有聚噻吩，聚阴离子化合物和介质常数εi= 15的非质子化合物的水性组合物，将所述组合物施加到所述物体上形成层和干燥所述层以在所述物体上形成导电聚合物层，其特征在于，在所述生产期间，所述物体和所述层保持在低于100℃的温度，并且所述导电聚合物层具有至多2kOMEGA /平方的电阻率。

4. 发明授权

US06887556B2 Material for making a conductive pattern 失效
标题翻译：制作导电图案的材料
公开(公告)号：US06887556B2
公开(公告)日：2005-05-03
申请号：US10316274
申请日：2002-12-11
申请人： Johan Lamotte , Frank Louwet , Tom Cloots , Huub Van Aert
发明人： Johan Lamotte , Frank Louwet , Tom Cloots , Huub Van Aert
IPC分类号： H01B1/12 , H01L51/00 , H01L51/30 , H01L51/40 , H05K3/02 , H05K3/10 , D06N7/04
CPC分类号： H05K3/105 , H01B1/127 , H01L51/0021 , H01L51/0036 , H05K3/02 , Y10T428/24355 , Y10T428/24802 , Y10T428/269 , Y10T428/2933 , Y10T428/2971 , Y10T428/31855
摘要： A material for making a conductive pattern, the material comprising a support and a heat-differentiable element, the heat-differentiable element comprising an outermost layer containing a polyanion and an intrinsically conductive polymer and optionally a second layer contiguous with the outermost layer, characterized in that the outermost layer and/or the optional second layer contains hydrophobic thermocoagulable latex particles in a weight ratio range with respect to the intrinsically conductive polymer in the range of 20:1 to 1:5, the hydrophobic thermocoagulable latex particles are capable upon heating of increasing the conductivity of the heated parts of the outermost layer relative to the unheated parts of the outermost layer and/or changing the removability of the heated parts of the outermost layer relative to the unheated parts of the outermost layer and the heat-differentiable element does not comprise a di- or polyhydroxy organic compound or an aprotic compound with a dielectric constant, ∈, ≧15; a method of making a conductive pattern on a support therewith; and a use of the material for making a conductive pattern in making an electronic circuit in the production of an electric or semiconductor device such as a printed circuit board, an integrated circuit, a display or touch screen, an electroluminescent device or a photovoltaic cell.
摘要翻译：一种用于制造导电图案的材料，该材料包括支撑体和可热分解的元件，该热可分离元件包括含有聚阴离子和本征导电聚合物的最外层，以及任选地与最外层邻接的第二层，其特征在于最外层和/或任选的第二层含有相对于本征导电聚合物的重量比范围为20:1至1:5的疏水性热凝胶乳胶颗粒，疏水性热凝胶乳颗粒能够加热增加最外层的加热部分相对于最外层的未加热部分的导电性和/或改变最外层的加热部分相对于最外层和可热分散元件的未加热部分的可去除性不包含二 - 或多羟基有机化合物或具有夹层的非质子化合物三次常数∈，> = 15; 在其上的支撑件上形成导电图案的方法; 以及在制造诸如印刷电路板，集成电路，显示器或触摸屏，电致发光器件或光伏电池的电气或半导体器件中的电子电路中制造导电图案的材料的用途。

5. 发明申请

US20050042556A1 Process for preparing a substantially transparent conductive layer configuration 失效
标题翻译：制备基本上透明的导电层构型的方法
公开(公告)号：US20050042556A1
公开(公告)日：2005-02-24
申请号：US10645160
申请日：2003-08-21
申请人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
发明人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
IPC分类号： H01B1/12 , H01B1/22 , H01L51/00 , H01L51/30 , H01L51/52 , H05K3/10 , G03C1/46
CPC分类号： H05K3/106 , H01B1/127 , H01B1/22 , H01L51/0021 , H01L51/0037 , H01L51/445 , H01L51/5203 , H05K2201/0329 , Y02E10/549
摘要： A process for preparing a substantially transparent conductive layer configuration on a support, the layer configuration comprising in any order at least a first layer containing an intrinsically conductive polymer optionally containing structural units represented by formula (I): wherein n is larger than 1 and each of R1 and R2 independently represents hydrogen or an optionally substituted C1-4 alkyl group or together represent an optionally substituted C1-4 alkylene group or an optionally substituted cycloalkylene group, preferably an ethylene group, an optionally alkyl-substituted methylene group, an optionally C1-12 alkyl- or phenyl-substituted ethylene group, a 1,3-propylene group or a 1,2-cyclohexylene group; and a second layer consisting of a non-continuous layer of conductive silver, the process comprising the step of: preparing the second layer by a photographic process; and light emitting diodes, photovoltaic devices, transistors and electroluminescent devices comprising a layer configuration prepared according to this process.
摘要翻译：一种用于在载体上制备基本上透明的导电层构型的方法，所述层构型至少包含含有本发明的导电聚合物的第一层，所述固有导电聚合物任选含有由式（I）表示的结构单元：其中n大于1， R 1和R 2独立地表示氢或任选取代的C 1-4烷基或一起表示任选取代的C 1-4亚烷基或任选取代的亚环烷基，优选亚乙基，任选烷基取代的亚甲基，任选的C 1-12烷基或苯基取代的亚乙基，1,3-亚丙基或1,2-亚环己基; 以及由不连续的导电银层组成的第二层，该方法包括以下步骤：通过摄影法制备第二层; 以及发光二极管，光电器件，晶体管和电致发光器件，其包括根据该工艺制备的层构型。

6. 发明授权

US07026079B2 Process for preparing a substantially transparent conductive layer configuration 失效
标题翻译：制备基本上透明的导电层构型的方法
公开(公告)号：US07026079B2
公开(公告)日：2006-04-11
申请号：US10645160
申请日：2003-08-21
申请人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
发明人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
IPC分类号： G03C1/89 , G03C5/29 , G03C8/28 , G03C8/52 , G03C8/32
CPC分类号： H05K3/106 , H01B1/127 , H01B1/22 , H01L51/0021 , H01L51/0037 , H01L51/445 , H01L51/5203 , H05K2201/0329 , Y02E10/549
摘要： A process for preparing a substantially transparent conductive layer configuration on a support, the layer configuration comprising in any order at least a first layer containing an intrinsically conductive polymer optionally containing structural units represented by formula (I): wherein n is larger than 1 and each of R1 and R2 independently represents hydrogen or an optionally substituted C1-4 alkyl group or together represent an optionally substituted C1-4 alkylene group or an optionally substituted cycloalkylene group, preferably an ethylene group, an optionally alkyl-substituted methylene group, an optionally C1-12 alkyl- or phenyl-substituted ethylene group, a 1,3-propylene group or a 1,2-cyclohexylene group; and a second layer consisting of a non-continuous layer of conductive silver, the process comprising the step of: preparing the second layer by a photographic process; and light emitting diodes, photovoltaic devices, transistors and electroluminescent devices comprising a layer configuration prepared according to this process.
摘要翻译：一种用于在载体上制备基本上透明的导电层构型的方法，所述层构型至少包含含有本发明的导电聚合物的第一层，所述第一层含有任选含有由式（I）表示的结构单元的固有导电聚合物：其中n大于1， R 1和R 2独立地表示氢或任选取代的C 1-4烷基，或者一起表示任选取代的C 1 -C 4烷基， 1-4个亚烷基或任选取代的亚环烷基，优选亚乙基，任选烷基取代的亚甲基，任选的C 1-12烷基或苯基取代的亚乙基，1,3-亚丙基或1,2-亚环己基; 以及由不连续的导电银层组成的第二层，该方法包括以下步骤：通过摄影法制备第二层; 以及发光二极管，光电器件，晶体管和电致发光器件，其包括根据该工艺制备的层构型。

7. 发明授权

US06444400B1 Method of making an electroconductive pattern on a support 失效
标题翻译：在支撑体上制作导电图案的方法
公开(公告)号：US06444400B1
公开(公告)日：2002-09-03
申请号：US09635707
申请日：2000-08-09
申请人： Tom Cloots , Frank Louwet , Ronn Andriessen , Etienne Van Thillo
发明人： Tom Cloots , Frank Louwet , Ronn Andriessen , Etienne Van Thillo
IPC分类号： H01B112
CPC分类号： H05K3/105 , H01L51/441 , H01L51/5088 , H01L51/5206 , H01L2251/5338 , Y02E10/549 , Y10S430/145 , Y10S430/146
摘要： A method of making an electroconductive pattern on a support is disclosed. The support is provided with a polymer layer containing a polythiophene, a polyanion and a di- or polyhydroxy organic compound. Said layer is characterized by an initial surface resistivity (SRi) having a value which is higher than 104 &OHgr;/□, or more preferably higher than 106 &OHgr;/□. By heating selected areas of the polymer layer, the surface resistivity of these areas is reduced to SRi/&Dgr; wherein &Dgr; is at least 10, preferably at least 103 and more preferable at least 105. The electroconductive pattern thus obtained can be used as an electronic circuit for making an electric or semiconductor device such as a printed circuit board, an integrated circuit, a display, an electroluminescent device or a photovoltaic cell.
摘要翻译：公开了一种在载体上制造导电图案的方法。该支撑体设有含有聚噻吩，聚阴离子和二羟基或多羟基有机化合物的聚合物层。所述层的特征在于初始表面电阻率（SRi）具有高于104欧米亚/平方的值，或更优选高于106欧米亚/平方。通过加热聚合物层的选定区域，这些区域的表面电阻率降低到SRi / DELTA，其中DELTA为至少10，优选至少为103，更优选为至少105.由此获得的导电图案可以用作电子用于制造诸如印刷电路板，集成电路，显示器，电致发光器件或光伏电池的电或半导体器件的电路。

8. 发明授权

US06340496B1 Method for patterning a layer of conductive polymers 有权
标题翻译：图案化导电聚合物层的方法
公开(公告)号：US06340496B1
公开(公告)日：2002-01-22
申请号：US09573549
申请日：2000-05-19
申请人： Tom Cloots , Roger Van den Bogaert , Jean-Pierre Tahon , Frank Louwet
发明人： Tom Cloots , Roger Van den Bogaert , Jean-Pierre Tahon , Frank Louwet
IPC分类号： B05D512
CPC分类号： C08G61/126 , H01B1/127
摘要： A method for producing electrode pattern in a conductive polymer on a substrate comprising the steps of applying a layer containing between 10 and 5000 mg/m2 of a conductive polymer, so as to prepare a conductive layer and printing an electrode pattern on said layer using a printing solution containing of an oxidant selected from the group consisting of ClO−, BrO−, MnO4−, Cr2O7−−, S2O8−− and H2O2.
摘要翻译：一种用于在基板上的导电聚合物中制造电极图案的方法，包括以下步骤：施加含有10-5000mg / m 2导电聚合物的层，以便制备导电层，并使用印刷溶液在所述层上印刷电极图案含有选自ClO-，BrO-，MnO4-，Cr2O7--，S2O8--和H2O2的氧化剂。

9. 发明授权

US07214405B2 Method of making a liquid crystal alignment layer 失效
标题翻译：制造液晶取向层的方法
公开(公告)号：US07214405B2
公开(公告)日：2007-05-08
申请号：US10653068
申请日：2003-09-03
申请人： Jean-Pierre Tahon , Tom Cloots , Roger Bäuerle
发明人： Jean-Pierre Tahon , Tom Cloots , Roger Bäuerle
IPC分类号： B05D5/06
CPC分类号： G02F1/133784 , G02F1/133711 , G02F2001/133796 , H01L51/0037 , Y10T428/1005 , Y10T428/1055
摘要： A method of making a liquid crystal alignment layer comprising the steps of: (i) providing a layer on a substrate, the layer comprising a polythiophene according to formula (I): wherein R1 and R2 each independently represent hydrogen or a C1–C4 alkyl group or together represent a C1–C4 alkylene group or a cycloalkylene group; and (ii) mechanically rendering the layer liquid crystal aligning; a liquid crystal alignment layer obtainable by the above-mentioned method; a liquid crystal device incorporating the above-mentioned liquid crystal alignment layer; a liquid crystal display comprising the above-mentioned liquid crystal alignment layer or the above-mentioned liquid crystal device; and the use of the polythiophene according to formula (I) for aligning liquid crystals.
摘要翻译：一种制备液晶取向层的方法，包括以下步骤：（i）在基底上提供一层，该层包含根据式（I）的聚噻吩：其中R 1和R 2 > 2 各自独立地表示氢或C 1 -C 4烷基，或者一起表示C 1 -C 3 > 4个亚烷基或亚环烷基; 和（ii）机械渲染层液晶取向; 通过上述方法得到的液晶取向层; 包含上述液晶取向层的液晶装置; 包括上述液晶取向层或上述液晶装置的液晶显示器; 以及使用根据式（I）的聚噻吩来取向液晶。

10. 发明授权

US07247342B2 Stable electroluminescent devices 失效
标题翻译：稳定的电致发光器件
公开(公告)号：US07247342B2
公开(公告)日：2007-07-24
申请号：US10614148
申请日：2003-07-07
申请人： Peter Willaert , Tom Cloots , Roger Van den Bogaert
发明人： Peter Willaert , Tom Cloots , Roger Van den Bogaert
IPC分类号： B05D5/06 , C09K11/06 , H01L51/54
CPC分类号： H01B1/128 , C08G61/126 , C09D11/106 , C09D11/52 , C09D165/00 , C09K11/06 , H01L51/0037 , H01L51/5206 , H01L51/5221 , Y10S428/917
摘要： An electroluminescent device comprising a transparent or translucent support, a transparent or translucent first electrode, a second conductive electrode and an electroluminescent phosphor layer sandwiched between the transparent or translucent first electrode and the second conductive electrode, wherein the first and second electrodes each comprises a polymer or copolymer of a 3,4-dialkoxythiophene, which may be the same or different, in which the two alkoxy groups may be the same or different or together represent an optionally substituted oxy-alkylene-oxy bridge; a display comprising the above-mentioned electroluminescent device; a lamp comprising the above-mentioned electroluminescent device; manufacturing processes for the above-mentioned electroluminescent devices; and the use of such devices for the integrated backlighting of static and dynamic posters and signage.
摘要翻译：一种电致发光器件，包括透明或半透明的支撑体，透明或半透明的第一电极，第二导电电极和夹在透明或半透明的第一电极和第二导电电极之间的电致发光磷光体层，其中第一和第二电极各自包含聚合物或可以相同或不同的3,4-二烷氧基噻吩的共聚物，其中两个烷氧基可以相同或不同，或一起代表任选取代的氧 - 亚烷基 - 氧桥; 包括上述电致发光器件的显示器; 一种包括上述电致发光器件的灯; 上述电致发光器件的制造工艺; 以及使用这种设备进行静态和动态海报和标牌的集成背光。

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