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1. 发明授权

US06887556B2 Material for making a conductive pattern 失效
标题翻译：制作导电图案的材料
公开(公告)号：US06887556B2
公开(公告)日：2005-05-03
申请号：US10316274
申请日：2002-12-11
申请人： Johan Lamotte , Frank Louwet , Tom Cloots , Huub Van Aert
发明人： Johan Lamotte , Frank Louwet , Tom Cloots , Huub Van Aert
IPC分类号： H01B1/12 , H01L51/00 , H01L51/30 , H01L51/40 , H05K3/02 , H05K3/10 , D06N7/04
CPC分类号： H05K3/105 , H01B1/127 , H01L51/0021 , H01L51/0036 , H05K3/02 , Y10T428/24355 , Y10T428/24802 , Y10T428/269 , Y10T428/2933 , Y10T428/2971 , Y10T428/31855
摘要： A material for making a conductive pattern, the material comprising a support and a heat-differentiable element, the heat-differentiable element comprising an outermost layer containing a polyanion and an intrinsically conductive polymer and optionally a second layer contiguous with the outermost layer, characterized in that the outermost layer and/or the optional second layer contains hydrophobic thermocoagulable latex particles in a weight ratio range with respect to the intrinsically conductive polymer in the range of 20:1 to 1:5, the hydrophobic thermocoagulable latex particles are capable upon heating of increasing the conductivity of the heated parts of the outermost layer relative to the unheated parts of the outermost layer and/or changing the removability of the heated parts of the outermost layer relative to the unheated parts of the outermost layer and the heat-differentiable element does not comprise a di- or polyhydroxy organic compound or an aprotic compound with a dielectric constant, ∈, ≧15; a method of making a conductive pattern on a support therewith; and a use of the material for making a conductive pattern in making an electronic circuit in the production of an electric or semiconductor device such as a printed circuit board, an integrated circuit, a display or touch screen, an electroluminescent device or a photovoltaic cell.
摘要翻译：一种用于制造导电图案的材料，该材料包括支撑体和可热分解的元件，该热可分离元件包括含有聚阴离子和本征导电聚合物的最外层，以及任选地与最外层邻接的第二层，其特征在于最外层和/或任选的第二层含有相对于本征导电聚合物的重量比范围为20:1至1:5的疏水性热凝胶乳胶颗粒，疏水性热凝胶乳颗粒能够加热增加最外层的加热部分相对于最外层的未加热部分的导电性和/或改变最外层的加热部分相对于最外层和可热分散元件的未加热部分的可去除性不包含二 - 或多羟基有机化合物或具有夹层的非质子化合物三次常数∈，> = 15; 在其上的支撑件上形成导电图案的方法; 以及在制造诸如印刷电路板，集成电路，显示器或触摸屏，电致发光器件或光伏电池的电气或半导体器件中的电子电路中制造导电图案的材料的用途。

2. 发明申请

US20050003315A1 Binders for use in the thermosensitive elements of substantially light-insensitive thermographic recording materials 审中-公开
标题翻译：用于基本上不透光的热敏记录材料的热敏元件的粘合剂
公开(公告)号：US20050003315A1
公开(公告)日：2005-01-06
申请号：US10859528
申请日：2004-06-02
申请人： Carlo Uyttendaele , Ivan Hoogmartens , Huub Van Aert , Frank Louwet
发明人： Carlo Uyttendaele , Ivan Hoogmartens , Huub Van Aert , Frank Louwet
IPC分类号： B41M5/40 , B41M5/44 , G03C1/00 , G03C1/498
CPC分类号： G03C1/4989 , B41M5/3372 , B41M5/44 , B41M5/443 , B41M2205/40 , G03C1/04
摘要： A substantially light-insensitive monosheet thermographic recording material comprising a support and on one side of the support a thermosensitive element, the thermosensitive element comprising at least one substantially light-insensitive silver salt of a carboxylic acid, at least one reducing agent therefor in thermal working relationship therewith and at least one binder, the at least one binder comprising at least one first polymer consisting of vinyl aceto-acetal monomer units, vinyl butyral monomer units and monomer units selected from the group consisting of, vinyl alcohol, vinyl acetate and itaconic acid monomer units, wherein the weight ratio of the at least one binder to the light-insensitive silver salt(s) of a carboxylic acid in the thermosensitive element is greater than 1.5; and the at least one binder optionally contains less than 40% by weight of a second polymer consisting of vinyl butyral monomer units and optionally vinyl alcohol and/or vinyl acetate monomer units.
摘要翻译：一种基本上不光敏的单片热成像记录材料，其包含支撑体，并且在支撑体的一侧上具有热敏元件，所述热敏元件包含至少一种基本上不受光敏的羧酸银盐，至少一种用于热加工的还原剂与至少一种粘合剂，所述至少一种粘合剂包含至少一种由乙烯基乙酰 - 缩醛单体单元，乙烯基缩丁醛单体单元和选自由乙烯醇，乙酸乙烯酯和衣康酸组成的组的单体单元组成的第一聚合物单体单元，其中所述热敏元件中所述至少一种粘合剂与所述不敏感的羧酸的银盐的重量比大于1.5; 并且所述至少一种粘合剂任选地包含小于40重量％的由乙烯醇缩丁醛单体单元和任选的乙烯醇和/或乙酸乙烯酯单体单元组成的第二聚合物。

3. 发明授权

US06300052B1 Binders for thermographic materials 失效
标题翻译：用于热成像材料的粘合剂
公开(公告)号：US06300052B1
公开(公告)日：2001-10-09
申请号：US09138048
申请日：1998-08-21
申请人： Frank Louwet , Huub Van Aert , Frank Ruttens , Ivan Hoogmartens
发明人： Frank Louwet , Huub Van Aert , Frank Ruttens , Ivan Hoogmartens
IPC分类号： G03C1498
CPC分类号： G03C1/49863 , G03C1/4989
摘要： A substantially light-insensitive black and white thermographic material comprising a support and a thermosensitive element containing a substantially light-insensitive organic silver salt, a reducing agent therefor in thermal working relationship therewith and a binder, wherein the binder is a water-dispersible film-forming polymer having covalently bonded ionic groups and the thermographic material is thermally developable under substantially water-free conditions; and a process for producing the substantially light-insensitive black and white thermographic material comprising the steps of: producing an aqueous dispersion of the substantially light-insensitive organic silver salt; producing one or more aqueous coating compositions containing together the aqueous dispersion of the substantially light-insensitive organic silver salt, the reducing agent and the binder; and applying the one or more aqueous coating compositions to the support, thereby forming after drying the thermosensitive element.
摘要翻译：一种基本上不透光的黑色和白色热成像材料，其包括载体和含有基本上不光敏的有机银盐的热敏元件，与其热加工关系的还原剂和粘合剂，其中所述粘合剂是水分散性膜 - 具有共价键离子基团的成型聚合物，并且热成像材料在基本上无水条件下是可热显影的; 以及用于生产基本上不透光的黑白热成像材料的方法，包括以下步骤：制备基本上不光敏的有机银盐的水分散体; 制备一种或多种含有基本上不光敏的有机银盐，还原剂和粘合剂的水性分散体的水性涂料组合物; 并将一种或多种水性涂料组合物施加到载体上，从而在干燥热敏元件之后形成。

4. 发明授权

US06306572B1 Binders for thermographic materials 失效
标题翻译：用于热成像材料的粘合剂
公开(公告)号：US06306572B1
公开(公告)日：2001-10-23
申请号：US09135637
申请日：1998-08-17
申请人： Carlo Uyttendaele , Huub Van Aert , Frank Louwet , Ivan Hoogmartens
发明人： Carlo Uyttendaele , Huub Van Aert , Frank Louwet , Ivan Hoogmartens
IPC分类号： G03C1498
CPC分类号： G03C1/4989 , G03C1/04 , G03C1/49863 , G03C2200/36
摘要： A substantially light-insensitive black and white thermographic material including a support and a thermosensitive element, containing a substantially light-insensitive organic silver salt, a reducing agent therefor in thermal working relationship therewith and a binder, wherein the binder is a water-dispersible film-forming polymer with covalently bonded moieties with one or more acid groups or anhydrides thereof and the thermographic material is thermally developable under substantially water-free conditions; and a process for producing the substantially light-insensitive black and white thermographic material comprising the steps of: producing an aqueous dispersion of the substantially light-insensitive organic silver salt; producing one or more aqueous coating compositions containing together the aqueous dispersion of the substantially light-insensitive organic silver salt, the reducing agent and the binder; and applying the one or more aqueous coating compositions to the support thereby forming after drying the thermosensitive element.
摘要翻译：一种基本上不透光的黑色和白色热成像材料，包括支撑体和热敏元件，其含有基本上不受光敏的有机银盐，与其热加工关系的还原剂和粘合剂，其中粘合剂是水分散性膜具有共价键合的部分与一个或多个酸基团或其酸酐并且热成像材料在基本上无水条件下可热显影; 以及用于生产基本上不透光的黑白热成像材料的方法，包括以下步骤：制备基本上不光敏的有机银盐的水分散体; 制备一种或多种含有基本上不光敏的有机银盐，还原剂和粘合剂的水性分散体的水性涂料组合物; 并且将一种或多种水性涂料组合物施加到载体上，从而在干燥热敏元件之后形成。

5. 发明授权

US06197418B1 Electroconductive glass laminate 有权
标题翻译：导电玻璃层压板
公开(公告)号：US06197418B1
公开(公告)日：2001-03-06
申请号：US09458829
申请日：1999-12-13
申请人： Tom Cloots , Frank Louwet , Hieronymus Andriessen , Bart Verlinden , Jean-Pierre Tahon , Leo Vermeulen , Luc Leenders , Rudi Goedeweeck
发明人： Tom Cloots , Frank Louwet , Hieronymus Andriessen , Bart Verlinden , Jean-Pierre Tahon , Leo Vermeulen , Luc Leenders , Rudi Goedeweeck
IPC分类号： B32B1710
CPC分类号： H05B33/28 , H01L51/5203 , Y10T428/26 , Y10T428/265 , Y10T428/266 , Y10T428/31507 , Y10T428/31616 , Y10T428/31627 , Y10T428/3163 , Y10T428/31645 , Y10T428/31649
摘要： A material is disclosed which comprises a substrate and an organic electroconductive layer provided on said substrate, characterised in that the substrate is a laminate comprising a glass layer and a support. The glass layer is preferably a flexible glass layer having a thickness from 10 to 500 &mgr;m. The material can be used as an electrode in electric or semiconductor devices thereby providing an improved lifetime, e.g. displays, photovoltaic cells or light-emitting diodes.
摘要翻译：公开了一种材料，其包括基板和设置在所述基板上的有机导电层，其特征在于，所述基板是包括玻璃层和支撑体的层压体。玻璃层优选为厚度为10〜500μm的柔性玻璃层。该材料可以用作电或半导体器件中的电极，从而提供改善的寿命，例如，显示器，光伏电池或发光二极管。

6. 发明授权

US06333145B1 Method for preparing a conductive polythiophene layer at low temperature 有权
标题翻译：在低温下制备导电聚噻吩层的方法
公开(公告)号：US06333145B1
公开(公告)日：2001-12-25
申请号：US09433971
申请日：1999-11-04
申请人： Tom Cloots , Johan Loccufier , Frank Louwet , Hieronymus Andriessen
发明人： Tom Cloots , Johan Loccufier , Frank Louwet , Hieronymus Andriessen
IPC分类号： G03C185
CPC分类号： H01B1/127 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/5203 , Y02E60/13
摘要： A method for producing a polymeric conductive layer on an object comprising the steps of: providing an aqueous composition containing a polythiophene, a polyanion compound and an aprotic compound with a dielectric constant, &egr;, ≧15, applying said composition to said object forming a layer and drying said layer to form a conductive polymeric layer on said object, characterised in that during said production said object and said layer are kept at a temperature below 100° C. and said conductive polymeric layer has a resistivity of at most 2 k&OHgr;/square.
摘要翻译：一种用于在物体上制备聚合物导电层的方法，包括以下步骤：提供含有聚噻吩，聚阴离子化合物和介质常数εi= 15的非质子化合物的水性组合物，将所述组合物施加到所述物体上形成层和干燥所述层以在所述物体上形成导电聚合物层，其特征在于，在所述生产期间，所述物体和所述层保持在低于100℃的温度，并且所述导电聚合物层具有至多2kOMEGA /平方的电阻率。

7. 发明申请

US20050042556A1 Process for preparing a substantially transparent conductive layer configuration 失效
标题翻译：制备基本上透明的导电层构型的方法
公开(公告)号：US20050042556A1
公开(公告)日：2005-02-24
申请号：US10645160
申请日：2003-08-21
申请人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
发明人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
IPC分类号： H01B1/12 , H01B1/22 , H01L51/00 , H01L51/30 , H01L51/52 , H05K3/10 , G03C1/46
CPC分类号： H05K3/106 , H01B1/127 , H01B1/22 , H01L51/0021 , H01L51/0037 , H01L51/445 , H01L51/5203 , H05K2201/0329 , Y02E10/549
摘要： A process for preparing a substantially transparent conductive layer configuration on a support, the layer configuration comprising in any order at least a first layer containing an intrinsically conductive polymer optionally containing structural units represented by formula (I): wherein n is larger than 1 and each of R1 and R2 independently represents hydrogen or an optionally substituted C1-4 alkyl group or together represent an optionally substituted C1-4 alkylene group or an optionally substituted cycloalkylene group, preferably an ethylene group, an optionally alkyl-substituted methylene group, an optionally C1-12 alkyl- or phenyl-substituted ethylene group, a 1,3-propylene group or a 1,2-cyclohexylene group; and a second layer consisting of a non-continuous layer of conductive silver, the process comprising the step of: preparing the second layer by a photographic process; and light emitting diodes, photovoltaic devices, transistors and electroluminescent devices comprising a layer configuration prepared according to this process.
摘要翻译：一种用于在载体上制备基本上透明的导电层构型的方法，所述层构型至少包含含有本发明的导电聚合物的第一层，所述固有导电聚合物任选含有由式（I）表示的结构单元：其中n大于1， R 1和R 2独立地表示氢或任选取代的C 1-4烷基或一起表示任选取代的C 1-4亚烷基或任选取代的亚环烷基，优选亚乙基，任选烷基取代的亚甲基，任选的C 1-12烷基或苯基取代的亚乙基，1,3-亚丙基或1,2-亚环己基; 以及由不连续的导电银层组成的第二层，该方法包括以下步骤：通过摄影法制备第二层; 以及发光二极管，光电器件，晶体管和电致发光器件，其包括根据该工艺制备的层构型。

8. 发明授权

US07026079B2 Process for preparing a substantially transparent conductive layer configuration 失效
标题翻译：制备基本上透明的导电层构型的方法
公开(公告)号：US07026079B2
公开(公告)日：2006-04-11
申请号：US10645160
申请日：2003-08-21
申请人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
发明人： Frank Louwet , Tom Cloots , Hieronymus Andriessen
IPC分类号： G03C1/89 , G03C5/29 , G03C8/28 , G03C8/52 , G03C8/32
CPC分类号： H05K3/106 , H01B1/127 , H01B1/22 , H01L51/0021 , H01L51/0037 , H01L51/445 , H01L51/5203 , H05K2201/0329 , Y02E10/549
摘要： A process for preparing a substantially transparent conductive layer configuration on a support, the layer configuration comprising in any order at least a first layer containing an intrinsically conductive polymer optionally containing structural units represented by formula (I): wherein n is larger than 1 and each of R1 and R2 independently represents hydrogen or an optionally substituted C1-4 alkyl group or together represent an optionally substituted C1-4 alkylene group or an optionally substituted cycloalkylene group, preferably an ethylene group, an optionally alkyl-substituted methylene group, an optionally C1-12 alkyl- or phenyl-substituted ethylene group, a 1,3-propylene group or a 1,2-cyclohexylene group; and a second layer consisting of a non-continuous layer of conductive silver, the process comprising the step of: preparing the second layer by a photographic process; and light emitting diodes, photovoltaic devices, transistors and electroluminescent devices comprising a layer configuration prepared according to this process.
摘要翻译：一种用于在载体上制备基本上透明的导电层构型的方法，所述层构型至少包含含有本发明的导电聚合物的第一层，所述第一层含有任选含有由式（I）表示的结构单元的固有导电聚合物：其中n大于1， R 1和R 2独立地表示氢或任选取代的C 1-4烷基，或者一起表示任选取代的C 1 -C 4烷基， 1-4个亚烷基或任选取代的亚环烷基，优选亚乙基，任选烷基取代的亚甲基，任选的C 1-12烷基或苯基取代的亚乙基，1,3-亚丙基或1,2-亚环己基; 以及由不连续的导电银层组成的第二层，该方法包括以下步骤：通过摄影法制备第二层; 以及发光二极管，光电器件，晶体管和电致发光器件，其包括根据该工艺制备的层构型。

9. 发明授权

US06635729B1 Process for the preparation of water-soluble &pgr;-conjugated polymers 有权
标题翻译：制备水溶性π-共轭聚合物的方法
公开(公告)号：US06635729B1
公开(公告)日：2003-10-21
申请号：US09767474
申请日：2001-01-23
申请人： Lambertus Groenendaal , Friedrich Jonas , Tom Cloots , Frank Louwet
发明人： Lambertus Groenendaal , Friedrich Jonas , Tom Cloots , Frank Louwet
IPC分类号： C08F12806
CPC分类号： C08G61/126 , H01B1/127 , H01G9/028 , H01G11/48 , H01G11/56 , Y02E60/13
摘要： The invention relates to a process for preparing water-soluble &pgr;-conjugated polymers by polymerizing, in aqueous solution using an oxidant, monomeric thiophene derivatives of formula (I) wherein X and Y are identical or different and are O, S, or N—R′, Z is —(CH2)m—CR2R3—(CH2)n—, R1 is aryl, C1-C18-alkyl, or hydrogen, R2 is hydrogen or —CH2)s—O—(CH2)p—SO3−M+, R3 is —(CH2)s—O—(CH2)p—SO3−M+, M+ is a cation, m and n are identical or different and are an integer from 0 to 3, s is an integer from 0 to 10, and p is an integer from 1 to 1.
摘要翻译：本发明涉及通过在水溶液中使用氧化剂，其中X和Y相同或不同且为O，S或N-R的式（I）的单体噻吩衍生物进行聚合来制备水溶性π-共轭聚合物的方法 '，Z是 - （CH 2）m-CR 2 R 3 - （CH 2）n - ，R 1是芳基，C 1 -C 18烷基或氢，R 2是氢或-CH 2 ）sO-（CH 2）p -SO 3 - ，M +，R 3是 - （CH 2）s O-（CH 2）p -SO 3 M +，M +是阳离子， m和n相同或不同，为0〜3的整数，s为0〜10的整数，p为1〜1的整数。

10. 发明授权

US06444400B1 Method of making an electroconductive pattern on a support 失效
标题翻译：在支撑体上制作导电图案的方法
公开(公告)号：US06444400B1
公开(公告)日：2002-09-03
申请号：US09635707
申请日：2000-08-09
申请人： Tom Cloots , Frank Louwet , Ronn Andriessen , Etienne Van Thillo
发明人： Tom Cloots , Frank Louwet , Ronn Andriessen , Etienne Van Thillo
IPC分类号： H01B112
CPC分类号： H05K3/105 , H01L51/441 , H01L51/5088 , H01L51/5206 , H01L2251/5338 , Y02E10/549 , Y10S430/145 , Y10S430/146
摘要： A method of making an electroconductive pattern on a support is disclosed. The support is provided with a polymer layer containing a polythiophene, a polyanion and a di- or polyhydroxy organic compound. Said layer is characterized by an initial surface resistivity (SRi) having a value which is higher than 104 &OHgr;/□, or more preferably higher than 106 &OHgr;/□. By heating selected areas of the polymer layer, the surface resistivity of these areas is reduced to SRi/&Dgr; wherein &Dgr; is at least 10, preferably at least 103 and more preferable at least 105. The electroconductive pattern thus obtained can be used as an electronic circuit for making an electric or semiconductor device such as a printed circuit board, an integrated circuit, a display, an electroluminescent device or a photovoltaic cell.
摘要翻译：公开了一种在载体上制造导电图案的方法。该支撑体设有含有聚噻吩，聚阴离子和二羟基或多羟基有机化合物的聚合物层。所述层的特征在于初始表面电阻率（SRi）具有高于104欧米亚/平方的值，或更优选高于106欧米亚/平方。通过加热聚合物层的选定区域，这些区域的表面电阻率降低到SRi / DELTA，其中DELTA为至少10，优选至少为103，更优选为至少105.由此获得的导电图案可以用作电子用于制造诸如印刷电路板，集成电路，显示器，电致发光器件或光伏电池的电或半导体器件的电路。

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