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1. 发明授权

US5731458A Process for thermally cracking carbamic acid esters 失效
标题翻译：热裂解氨基甲酸酯的方法
公开(公告)号：US5731458A
公开(公告)日：1998-03-24
申请号：US811801
申请日：1997-03-06
申请人： Jurgen Dahmer , Dieter Schleenstein , Heinrich Steude , Oswald Wilmes , Christian Rasp , Georg Ronge , Klaus Nachtkamp , Wilfried Litz , Stephan Kabelac
发明人： Jurgen Dahmer , Dieter Schleenstein , Heinrich Steude , Oswald Wilmes , Christian Rasp , Georg Ronge , Klaus Nachtkamp , Wilfried Litz , Stephan Kabelac
IPC分类号： C07C263/04 , C07C265/04 , C07C265/14 , C07C269/06 , C07C271/20
CPC分类号： C07C263/04 , Y02P20/127 , Y02P20/582
摘要： This present invention relates to a process for thermally cracking carbamic acid esters into the corresponding isocyanate and hydroxyl compounds in the liquid phase, wherein the reaction proceeds as a reactive rectification in the stripping zone of a column and in an inert, high-boiling solvent, which acts as a buffer to keep the reaction away from the evaporator region of the column.
摘要翻译：本发明涉及一种将氨基甲酸酯热裂解成液相中相应的异氰酸酯和羟基化合物的方法，其中反应在塔的汽提区和惰性高沸点溶剂中作为反应性精馏进行，其用作缓冲剂以使反应远离柱的蒸发器区域。

2. 发明授权

US5981653A Process for the production of aqueous stoving coating compositions 失效
标题翻译：用于生产水性烘烤涂料组合物的方法
公开(公告)号：US5981653A
公开(公告)日：1999-11-09
申请号：US844815
申请日：1997-04-22
申请人： Oswald Wilmes , Lothar Kahl , Bernd Klinksiek , Christian Wamprecht , Manfred Bock , Klaus Nachtkamp
发明人： Oswald Wilmes , Lothar Kahl , Bernd Klinksiek , Christian Wamprecht , Manfred Bock , Klaus Nachtkamp
IPC分类号： C08J3/02 , B01J13/04 , C08G18/08 , C08G18/63 , C08G18/79 , C08G18/80 , C08J3/03 , C08J3/12 , C09D5/46 , C09D175/04 , C08G18/40 , C08L75/04
CPC分类号： C08J3/03 , C08G18/0866 , C08G18/631 , C08G18/792 , C08G18/8061 , C08G2150/20 , C08J2375/04
摘要： The present invention relates to a process for the production of aqueous dispersions which form powder coatings at room temperature, have an average particle size of 0.1 to 10 .mu.m, contain polyols and blocked polyisocyanate crosslinking agents, and, after stoving, yield coatings with improved water and solvent resistance, in particular on metallic substrates.
摘要翻译：本发明涉及一种在室温下形成粉末涂料的水性分散体的制备方法，平均粒径为0.1-10μm，含有多元醇和封端的多异氰酸酯交联剂，并且在烘烤后，产率增加了耐水和耐溶剂性，特别是在金属基材上。

3. 发明授权

US5852106A Coating compositions for glass substrates 失效
标题翻译：玻璃基材用涂料组合物
公开(公告)号：US5852106A
公开(公告)日：1998-12-22
申请号：US848948
申请日：1997-05-01
申请人： Oswald Wilmes , Beate Baumbach , Klaus Nachtkamp , Eberhard Konig , Randall Dearth , Manfred Bock , Wolfhart Wieczorrek
发明人： Oswald Wilmes , Beate Baumbach , Klaus Nachtkamp , Eberhard Konig , Randall Dearth , Manfred Bock , Wolfhart Wieczorrek
IPC分类号： C03C17/32 , C08G18/08 , C08G18/12 , C08G18/64 , C08G18/75 , C08G18/79 , C08G18/80 , C09D175/04 , C08J3/00 , B32B27/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/807 , C03C17/322 , C08G18/0819 , C08G18/12 , C08G18/758 , C08G18/8058 , Y10T428/31551
摘要： The present invention relates to aqueous polyurethane coating compositions wherein the binder contains a) a polyol component, which is soluble or dispersible in water and is the reaction product of a polyisocyanate component containing 50 to 100 wt. % of 4,4'-diisocyanatodicyclohexylmethane, a polyol component containing one or more polyether polyols and having an OH number of 25 to 350 mg KOH/g solids and an isocyanate-reactive component containing at least one group capable of salt formation and b) a polyisocyanate component, which is soluble or dispersible in water, has blocked isocyanate groups and is the reaction product of a polyisocyanate having an isocyanurate group content of 2 to 30 wt. %, a reversible, monofunctional blocking agent for isocyanate groups, a nonionic hydrophilic component and a stabilizing component which has 1 to 2 hydrazide groups and a molecular weight of 70 to 300, wherein the equivalent ratio of blocked isocyanate groups of component b) to hydroxyl groups of component a) is at least 0.8:1. The present invention also relates to the use of the binders for coating any glass surfaces, especially glass bottles.
摘要翻译：本发明涉及水性聚氨酯涂料组合物，其中粘合剂包含a）多元醇组分，其可溶于或分散于水中，并且是含有50-100重量份的多异氰酸酯组分的反应产物。％的4,4'-二异氰酸根合二环己基甲烷，含有一种或多种聚醚多元醇并且OH数为25至350mg KOH / g固体的多元醇组分和含有至少一个能够形成盐的基团的异氰酸酯反应性组分，以及b）可溶于或分散于水中的多异氰酸酯组分具有封闭的异氰酸酯基团，并且是异氰脲酸酯基团含量为2-30重量％的多异氰酸酯的反应产物。％，用于异氰酸酯基团的可逆的单官能封端剂，非离子亲水组分和具有1至2个酰肼基和分子量为70至300的稳定组分，其中组分b）的封端异氰酸酯基团与羟基的当量比组分a）的组分至少为0.8:1。本发明还涉及粘合剂用于涂覆任何玻璃表面，特别是玻璃瓶的用途。

4. 发明授权

US5804647A Aqueous polyurethane-ureas, a process for their production and their use in coating compositions 失效
标题翻译：水性聚氨酯 - 尿素，其制备方法及其在涂料组合物中的应用
公开(公告)号：US5804647A
公开(公告)日：1998-09-08
申请号：US804462
申请日：1997-02-21
申请人： Klaus Nachtkamp , Oswald Wilmes , Eberhard Arning , Rolf Roschu
发明人： Klaus Nachtkamp , Oswald Wilmes , Eberhard Arning , Rolf Roschu
IPC分类号： C08L75/04 , C08G18/00 , C08G18/08 , C08G18/12 , C08G18/28 , C08G18/42 , C08G18/48 , C08G18/50 , C08G18/65 , C08G18/66 , C08G18/72 , C08G18/75 , C09D175/00 , C09D175/02 , C09D175/04 , C08J3/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/664 , C08G18/0819 , C08G18/0823 , C08G18/12 , C08G18/283 , C08G18/4202 , C08G18/4833 , C08G18/5024 , C08G18/6692 , C08G18/751 , C09D175/02
摘要： The present invention relates to aqueous polyurethane-urea dispersions which are film forming at temperatures of .ltoreq.20.degree. C. in the absence of film forming additives, dry at room temperature to yield films having a hardness according to DIN 53 157 (Konig pendulum hardness) of .gtoreq.100 seconds, in which the polyurethane-ureas have a urethane group content (calculated as --NH--CO--O--, molecular weight 59) of 7 to 20 wt. %, and a urea group content (calculated as -NH-CO-N, molecular weight 57) of 5 to 18 wt. %, and contain 15-70 wt. %, based on resin solids, of structural units prepared by incorporating 1-methyl-2,4- and/or -2,6-diisocyanatocyclohexane in the form of urethane and/or urea groups. The present invention also relates to a process for the production of these aqueous polyurethane-urea dispersions and to their use in coating compositions.
摘要翻译：本发明涉及在不存在成膜添加剂的情况下在-20℃的温度下成膜的水性聚氨酯 - 尿素分散体，在室温下干燥，得到具有根据DIN 53 157（K + 其中聚氨酯 - 脲的氨基甲酸酯基含量（以-NH-CO-O-计算，分子量59）为7〜20重量％。％，尿素基含量（以-NH-CO-N计算，分子量57）为5〜18重量％。％，含有15-70wt。基于树脂固体的通过以氨基甲酸酯和/或脲基团的形式并入1-甲基-2,4-和/或-2,6-二异氰酸酯基环己烷制备的结构单元的％。本发明还涉及这些水性聚氨酯 - 尿素分散体的制备方法及其在涂料组合物中的用途。

5. 发明授权

US5744633A Process for the production of diurethanes and their use for the production of diisocyanates 失效
标题翻译：用于生产二氨基甲酸酯的方法及其用于生产二异氰酸酯的方法
公开(公告)号：US5744633A
公开(公告)日：1998-04-28
申请号：US348704
申请日：1994-12-02
申请人： Oswald Wilmes , Eberhard Konig , Klaus Nachtkamp , Ernst Kysela
发明人： Oswald Wilmes , Eberhard Konig , Klaus Nachtkamp , Ernst Kysela
IPC分类号： C07C263/04 , C07C265/14 , C07C269/04 , C07C271/20 , C07C261/00
CPC分类号： C07C269/04
摘要： A new process for the production of high purity (cyclo)aliphatic diurethanes from (cyclo)aliphatic diamines, alcohols and urea in a multistep reaction in which (1) urea is reacted with alcohol with elimination of ammonia, (2) diamine is then introduced into the reaction mixture, optionally in the form of a solution in alcohol, and reacted with continuous release of ammonia and (3) the reaction mixture is freed from volatile components by distillation. The diurethanes produced by this process are useful as starting materials for the production of the corresponding diisocyanates by thermal urethane cleavage.
摘要翻译：然后引入（1）尿素与醇与氨反应脱除（2）二胺时，在多步反应中从（环）脂族二胺，醇和尿素生产高纯度（环）脂族二氨基甲酸酯的新方法进入反应混合物中，任选地呈醇的溶液形式，并与氨的连续释放反应，和（3）通过蒸馏除去挥发性组分。通过该方法制备的二氨基甲酸酯可用作通过热氨基甲酸酯切割生产相应的二异氰酸酯的起始原料。

6. 发明授权

US5789620A Process for the preparation of 1,4-bis(aminomethyl) cyclohexane 失效
标题翻译：制备1,4-双（氨基甲基）环己烷的方法
公开(公告)号：US5789620A
公开(公告)日：1998-08-04
申请号：US962072
申请日：1997-10-31
申请人： Helmut Waldmann , Jurgen Dahmer , Klaus Nachtkamp , Anatoly Bazanov , Alexandre Timofeev , Natalja Zubritskaya , Gennady Terechtchenko
发明人： Helmut Waldmann , Jurgen Dahmer , Klaus Nachtkamp , Anatoly Bazanov , Alexandre Timofeev , Natalja Zubritskaya , Gennady Terechtchenko
IPC分类号： C07C209/16 , C07C211/18
CPC分类号： C07C209/16 , C07C2101/14
摘要： The present invention relates to a process for preparing 1,4-bis(aminomethyl)cyclohexane by reacting a 40 to 80 wt. % aqueous solution of 1,4-bis(hydroxymethyl)cyclohexane with a mixture of hydrogen and ammonia in the presence of a nickel/copper/chromium catalyst at a pressure of 100 to 250 bar and a temperature of 150.degree. to 250.degree. C.
摘要翻译：本发明涉及一种制备1,4-双（氨基甲基）环己烷的方法，该方法是使40至80wt。％的镍/铜/铬催化剂存在下，在氢气和氨的混合物下，在100-250巴的压力和150-250℃的温度下，1,4-双（羟甲基）环己烷的％水溶液。

7. 发明授权

US07071326B2 Anionic cellulose nitrate derivatives and aqueous dispersions thereof 失效
标题翻译：阴离子硝酸纤维素衍生物及其水分散体
公开(公告)号：US07071326B2
公开(公告)日：2006-07-04
申请号：US11290193
申请日：2005-11-30
申请人： Carsten Hüttermann , Thomas Wagner , Klaus Nachtkamp
发明人： Carsten Hüttermann , Thomas Wagner , Klaus Nachtkamp
IPC分类号： C08B7/00 , C09D101/20
CPC分类号： C08J3/05 , C08B7/00 , C08J2301/18 , C08L1/20
摘要： An anionic cellulose nitrate derivative is described, which has: (i) a degree of acid group substitution (DS (acid)) in the range of 0.01 to 0.2; and (ii) a nitrogen content of 10.7 wt. % to 12.3 wt. %, based on the weight of cellulose nitrate derivative. The anionic cellulose nitrate derivative is prepared by a process which includes esterifying cellulose nitrate feed material with at least one dicarboxylic acid anhydride (e.g., maleic anhydride). Aqueous dispersions according to the present invention include: (a) at least on anionic cellulose nitrate derivative according to the present invention; and (b) at least one base.
摘要翻译：描述了一种阴离子硝酸纤维素衍生物，其具有：（i）酸基置换度（DS（酸））在0.01至0.2的范围内; 和（ii）10.7重量％的氮含量。％〜12.3重量％％，基于硝酸纤维素衍生物的重量。通过包括用至少一种二羧酸酐（例如马来酸酐）将硝酸纤维素原料酯化的方法制备阴离子硝酸纤维素衍生物。根据本发明的水分散体包括：（a）至少一种根据本发明的阴离子硝酸纤维素衍生物; 和（b）至少一个碱基。

8. 发明申请

US20060041117A1 Process for the preparation of cellulose derivatives containing amino groups 审中-公开
标题翻译：制备含氨基的纤维素衍生物的方法
公开(公告)号：US20060041117A1
公开(公告)日：2006-02-23
申请号：US11184093
申请日：2005-07-19
申请人： Jurgen Engelhardt , Meinolf Brackhagen , Klaus Nachtkamp , Wolfgang Koch , Thomas Schulze , Frank Meister
发明人： Jurgen Engelhardt , Meinolf Brackhagen , Klaus Nachtkamp , Wolfgang Koch , Thomas Schulze , Frank Meister
IPC分类号： C08B11/00
CPC分类号： C08B11/145 , A61K8/731 , A61Q19/00 , C02F1/56 , D21H17/07 , D21H17/25
摘要： A process is described for the preparation of cellulose derivatives containing amino groups that involves reacting, in the presents of water as a reaction medium, alkali cellulose or alkali cellulose derivatives with reagents represented by the following formula, X—(CH2)n—NR1R2 in which: X is selected from the group consisting of chlorine, bromine, iodine and a sulfonic acid radical R′SO3, in which R′ is an aromatic radical or an aliphatic radical; n is at least 2; and R1 and R2 independently of each other are selected from the group consisting of aliphatic substituents, branched alkyl substituents, cyclic alkyl substituents, aryl substituents, aryl substituents substituted by heteroatoms, H, and R1 and R2 together form a ring with the nitrogen. In the process, the mole ratio of cellulose to water, of said reaction medium, is 1:5 to 1:40 mol water per mol of anhydroglucose unit (AGU). Amino functional cellulose derivatives prepared in accordance with the method of the present invention are useful in cosmetic formulations and aqueous paper treatment compositions.
摘要翻译：描述了制备含有氨基的纤维素衍生物的方法，该方法包括在作为反应介质的水的存在下，将碱纤维素或碱性纤维素衍生物与下式表示的试剂反应：<？在线配方说明= “In-line Formulas”end =“lead”？> X-（CH 2）n - NR 1 R 2 - 其中：X选自氯，溴，碘和磺酸基R'SO 2，其中：X选自氯，溴，碘，磺酸根R' 其中R'是芳族基团或脂族基团; n至少为2; R 1和R 2彼此独立地选自脂族取代基，支链烷基取代基，环烷基取代基，芳基取代基，被杂原子取代的芳基取代基，H和R 1和R 2一起与氮一起形成环。在该过程中，所述反应介质的纤维素与水的摩尔比为每摩尔脱水葡萄糖单元（AGU）为1:5至1:40摩尔水。根据本发明的方法制备的氨基官能纤维素衍生物可用于化妆品制剂和水性纸处理组合物中。

9. 发明授权

US5889106A Polyisocyanates blocked with 3,5-dimethyl-1,2,4-triazole 失效
公开(公告)号：US5889106A
公开(公告)日：1999-03-30
申请号：US899951
申请日：1997-07-24
申请人： Gerald Kurek , Eberhard Konig , Klaus Nachtkamp , Theodor Engbert
发明人： Gerald Kurek , Eberhard Konig , Klaus Nachtkamp , Theodor Engbert
IPC分类号： C07D249/08 , C08G18/79 , C08G18/80 , C09D175/12 , C08J3/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/807 , C08G18/792 , C08G18/808
摘要： This invention relates to polyisocyanates which are partially or completely blocked with 3,5-dimethyl-1,2,4-triazole, to heat curable, one-component coating compositions containing these blocked polyisocyanates and to the resulting coatings.

10. 发明授权

US5141987A Aqueous coating compositions containing water dispersible polyurethane polyureas as binders and the coatings produced therefrom 失效
标题翻译：含有水分散聚氨酯聚氨酯作为粘合剂的水性涂料组合物及其生产的涂料
公开(公告)号：US5141987A
公开(公告)日：1992-08-25
申请号：US604718
申请日：1990-10-26
申请人： Klaus Nachtkamp , Jurgen Mosbach , Klaus Noll , Hans G. Schmitz , Armin Sickert
发明人： Klaus Nachtkamp , Jurgen Mosbach , Klaus Noll , Hans G. Schmitz , Armin Sickert
IPC分类号： C09D5/00 , C08G18/08 , C08G18/44 , C08G18/50 , C08G18/78 , C09D5/38 , C09D175/00 , C09D175/04
CPC分类号： C08G18/7818 , C08G18/0804 , C08G18/44 , C08G18/5042 , C09D175/04
摘要： This invention relates to an aqueous coating composition containing aluminum pigments and a water dispersible polyurethane polyurea binder which contains(i) at least 200 milliequivalents per 100 g of solids of chemically incorporated carbonate groups --O--CO--O-- and(ii) a combined total of up to 320 milliequivalents per 100 g of solids of chemically incorporated urethane groups --NH--CO--O-- and chemically incorporated urea groups --NH--CO--NH--.The invention further relates to coatings prepared from the aqueous coating composition.
摘要翻译：本发明涉及包含铝颜料和水分散性聚氨酯聚脲粘合剂的水性涂料组合物，其含有（i）每100g固体化学掺入的碳酸酯基团-O-CO-O-至少200毫当量，和（ii）组合每100g固体的化学引入的氨基甲酸酯基团-NH-CO-O-和化学引入的脲基团-NH-CO-NH-的总计可达320毫当量。本发明还涉及由水性涂料组合物制备的涂料。

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