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1. 发明申请

US20130005960A1 METHOD FOR PRODUCING AMIDE COMPOUND 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：US20130005960A1
公开(公告)日：2013-01-03
申请号：US13635092
申请日：2011-03-15
申请人： Junichi Kugimoto , Joji Kawai , Kazuo Yamato , Masahide Okada , Tsunemi Sugimoto , Hiroshi Matsumoto
发明人： Junichi Kugimoto , Joji Kawai , Kazuo Yamato , Masahide Okada , Tsunemi Sugimoto , Hiroshi Matsumoto
IPC分类号： C07D225/02
CPC分类号： C07D201/06 , C07D201/04 , C07D225/02
摘要： The present invention relates to a method for producing a high purity, high quality amide compound, particularly, lactam. A first embodiment of the present invention is characterized in that an amount of each of a halide, an aldehyde compound, an alcohol compound and a nitrile compound contained in a solution recycled into an oxime-forming step is controlled to an amount of 0.4 mol % or less based on the ketone as a starting material. A second embodiment of the present invention is characterized in that one or more compounds selected from the group consisting of a ketone, an oxime and an amide compound are purified by hydrogenation and/or crystallization for eliminating impurities containing a double bond. A third embodiment of the present invention is characterized in that a content of impurities having a cyclic bridge structure is controlled by using a cycloalkanone purified by recrystallization.
摘要翻译：本发明涉及一种生产高纯度，优质酰胺化合物，特别是内酰胺的方法。本发明的第一实施方案的特征在于，将再循环到肟形成步骤的溶液中所含的卤化物，醛化合物，醇化合物和腈化合物中的每一种的量控制为0.4mol％基于酮作为原料。本发明的第二个实施方案的特征在于，通过氢化和/或结晶纯化一种或多种选自酮，肟和酰胺化合物的化合物，以消除含有双键的杂质。本发明的第三实施方案的特征在于通过使用通过重结晶纯化的环烷酮来控制具有环状桥结构的杂质的含量。

2. 发明授权

US08530645B2 Method for producing amide compound 有权
标题翻译：酰胺化合物的制备方法
公开(公告)号：US08530645B2
公开(公告)日：2013-09-10
申请号：US13254217
申请日：2010-03-04
申请人： Junichi Kugimoto , Tsunemi Sugimoto
发明人： Junichi Kugimoto , Tsunemi Sugimoto
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D225/02 , C07D201/04
摘要： This invention relates to a process for producing an amide compound by Beckmann rearrangement of an oxime compound using a compound having at least two electron-withdrawing leaving groups as a rearrangement catalyst, the process comprising a pre-preparation step in which the rearrangement catalyst and at least a part of the oxime compound are mixed and reacted; and a rearrangement reaction step in which the oxime compound is rearranged at a temperature higher than that in the pre-preparation step.
摘要翻译：本发明涉及通过使用具有至少两个吸电子离去基团的化合物作为重排催化剂的肟化合物的贝克曼重排制备酰胺化合物的方法，该方法包括预制备步骤，其中重排催化剂和将至少一部分肟化合物混合并反应; 和重排反应步骤，其中肟化合物在比预制备步骤中高的温度下重新排列。

3. 发明申请

US20110313149A1 METHOD FOR PRODUCING AMIDE COMPOUND 有权
标题翻译：生产酰胺化合物的方法
公开(公告)号：US20110313149A1
公开(公告)日：2011-12-22
申请号：US13254217
申请日：2010-03-04
申请人： Junichi Kugimoto , Tsunemi Sugimoto
发明人： Junichi Kugimoto , Tsunemi Sugimoto
IPC分类号： C07D225/02
CPC分类号： C07D225/02 , C07D201/04
摘要： This invention relates to a process for producing an amide compound by Beckmann rearrangement of an oxime compound using a compound having at least two electron-withdrawing leaving groups as a rearrangement catalyst, the process comprising a pre-preparation step in which the rearrangement catalyst and at least a part of the oxime compound are mixed and reacted; and a rearrangement reaction step in which the oxime compound is rearranged at a temperature higher than that in the pre-preparation step.
摘要翻译：本发明涉及通过使用具有至少两个吸电子离去基团的化合物作为重排催化剂的肟化合物的贝克曼重排制备酰胺化合物的方法，该方法包括预制备步骤，其中重排催化剂和将至少一部分肟化合物混合并反应; 和重排反应步骤，其中肟化合物在比预制备步骤中高的温度下重新排列。

4. 发明授权

US06420575B1 Refining treatment method of liquid reaction mixture obtained from epoxidation reaction of 1,5,9-cyclododecatriene 有权
公开(公告)号：US06420575B1
公开(公告)日：2002-07-16
申请号：US09895192
申请日：2001-07-02
申请人： Kouhei Ninomiya , Tsunemi Sugimoto , Junichi Kugimoto , Mitsuo Yamanaka , Kohji Kaiso
发明人： Kouhei Ninomiya , Tsunemi Sugimoto , Junichi Kugimoto , Mitsuo Yamanaka , Kohji Kaiso
IPC分类号： C07D30112
CPC分类号： C07D301/12
摘要： After 1,5,9-cyclododecatriene is epoxidized with hydrogen peroxide in the presence of a catalyst containing a tungsten compound, a quaternary onium salt and a mineral acid, to obtain a liquid reaction mixture containing the resultant 1,2-epoxy-5,9-cyclododecadiene, the catalyst, non-reacted hydrogen peroxide and non-reacted 1,5,9-cyclododecatriene and being phase-separated into an oil phase fraction and an aqueous phase fraction, at least the oil phase fraction of the liquid reaction mixture is treated with an aqueous alkali solution to deactivate and remove the non-reacted hydrogen peroxide and the catalyst contained in at least the oil phase fraction.

5. 发明授权

US08624021B2 Compound and process for producing amide compound therewith 有权
标题翻译：用于生产酰胺化合物的化合物和方法
公开(公告)号：US08624021B2
公开(公告)日：2014-01-07
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02 , C07D201/04
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供了新的环十二烷酮-O-氮杂环十二烯-2-基肟和环十二酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

6. 发明申请

US20130005961A1 NOVEL COMPOUND AND PROCESS FOR PRODUCING AMIDE COMPOUND THEREWITH 有权
标题翻译：新型化合物及其生产方法
公开(公告)号：US20130005961A1
公开(公告)日：2013-01-03
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供新的环十二烷酮-O-氮杂环十二烷-2-基肟和环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

7. 发明授权

US5977416A Dehydration catalyst and process for producing a monoalkylether of a dihydric phenolic compound using same 失效
标题翻译：脱水催化剂和使用其制备二羟基酚类化合物的单烷基醚的方法
公开(公告)号：US5977416A
公开(公告)日：1999-11-02
申请号：US58327
申请日：1998-04-09
申请人： Tokuo Matsuzaki , Tsunemi Sugimoto , Yasuo Nakamura , Takumi Manabe
发明人： Tokuo Matsuzaki , Tsunemi Sugimoto , Yasuo Nakamura , Takumi Manabe
IPC分类号： B01J23/18 , B01J27/02 , B01J27/16 , B01J27/18 , C07C41/00 , C07C45/00 , C07C27/26 , C07C213/00
CPC分类号： B01J27/16 , B01J23/18 , B01J27/02 , B01J27/1815
摘要： A dehydration catalyst useful for producing a monoalkylether of dihydric phenolic compound by a dehydration reaction of a dihydric phenolic compound with a lower alkyl alcohol with a high conversion at a high selectivity, comprises at least one inorganic substance of the empirical formula (I):Al.sub.a P.sub.b Ti.sub.c Si.sub.d X.sub.e O.sub.f (I)wherein X represents a member selected from the group consisting of (1) an antimony and/or a bismuth atom, and (2) a sulfur atom, a, b, c, d, e and f respectively represent the numbers of Al, P, Ti, Si, X and 0 atoms, the atomic ratio a:b is 1:1.0 to 1.9, the atomic ratio a:c is 1:0.05 to 0.5, the atomic ratio a:d is 1:0.05 to 0.2, the atomic ratio a:e is 1:0.01 to 0.3 when X represents antimony and/or bismuth atom and 1:0.004 to 0.015 when X represents a sulfur atom, and the atomic ratio a:f is 1:4.1 to 8.4.
摘要翻译：通过二羟基酚类化合物与高级选择性的高转化率的低级烷基醇的脱水反应生产二羟基酚类化合物的单烷基醚的脱水催化剂包含至少一种经验式（I）的无机物质：Ala （I）其中X表示选自（1）锑和/或铋原子的成员，（2）硫原子，a，b，c，d，e和f 分别表示Al，P，Ti，Si，X和0原子的数量，原子比a:b为1：1.0〜1.9，原子比a：c为1:0.05〜0.5，原子比a：d 为1:0.05〜0.2，当X表示锑和/或铋原子时，原子比a:e为1:0.01〜0.3，当X表示硫原子时为1：0.004〜0.015，原子比a:f为1 ：4.1〜8.4。

8. 发明申请

US20120149937A1 METHOD FOR PRODUCING HYDROXYCARBOXYLIC ACID DERIVATIVE 有权
标题翻译：生产羟基羧酸衍生物的方法
公开(公告)号：US20120149937A1
公开(公告)日：2012-06-14
申请号：US13387943
申请日：2010-07-12
申请人： Akio Kamimura , Kouji Kaiso , Tsunemi Sugimoto
发明人： Akio Kamimura , Kouji Kaiso , Tsunemi Sugimoto
IPC分类号： C07C67/31 , C07C51/06
CPC分类号： C07C67/20 , Y02P20/544 , C07C69/675
摘要： To provide a method for the production of a hydroxycarboxylic acid derivative, by which a hydroxycarboxylic acid derivative, which can be reused in various applications, can be obtained from a polyamide at a high yield without consuming a large amount of energy. A method for the production of a hydroxycarboxylic acid derivative, which is characterized by including allowing an alcohol in a supercritical state to act on a polyamide in the presence of a carboxylic acid derivative to depolymerize the polyamide to obtain the hydroxycarboxylic acid derivative.
摘要翻译：为了提供一种生产羟基羧酸衍生物的方法，通过该方法可以从聚酰胺中以高产率获得可以在各种应用中重复使用的羟基羧酸衍生物，而不消耗大量的能量。一种羟基羧酸衍生物的制造方法，其特征在于，使含有超临界状态的醇在羧酸衍生物的存在下作用于聚酰胺，使聚酰胺解聚而获得羟基羧酸衍生物。

9. 发明申请

US20110311821A1 POLYAMIDE PARTICLES AND PROCESS FOR PRODUCING SAME 有权
标题翻译：聚酰胺颗粒及其生产方法
公开(公告)号：US20110311821A1
公开(公告)日：2011-12-22
申请号：US13254026
申请日：2010-03-02
申请人： Koji Kaiso , Masanori Abe , Tsunemi Sugimoto
发明人： Koji Kaiso , Masanori Abe , Tsunemi Sugimoto
IPC分类号： C08J9/36 , C08G69/02 , C08J9/00
CPC分类号： C08G69/02 , C08G69/14 , C08G69/26 , C08J3/14 , C08J2377/00 , Y10T428/2982
摘要： There is provided a novel polyamide particles having an approximately spherical outer shape, which are spongy particles having through holes in an outer surface part and closed voids in an inside part. The polyamide particles can be produced by dissolving a polyamide in a cyclic amide with heating to obtain a homogeneous solution and then cooling the solution.
摘要翻译：提供了具有近似球形外形的新型聚酰胺颗粒，其是在外表面部分具有通孔的海绵状颗粒和内部部分中的封闭空隙。聚酰胺颗粒可以通过将聚酰胺溶解在环状酰胺中而加热得到均匀的溶液，然后冷却溶液来制备。

10. 发明授权

US5342826A Bi-Sr-Ca-Cu-O superconducting thin film 失效
标题翻译： Bi-Sr-Ca-Cu-O超导薄膜
公开(公告)号：US5342826A
公开(公告)日：1994-08-30
申请号：US950127
申请日：1992-09-24
申请人： Nobuhiko Kubota , Tsunemi Sugimoto , Kazushi Sugawara , Yuh Shiohara
发明人： Nobuhiko Kubota , Tsunemi Sugimoto , Kazushi Sugawara , Yuh Shiohara
IPC分类号： H01L39/24 , B32B9/00
CPC分类号： H01L39/2458 , Y10S505/701
摘要： A Bi-Sr-Ca-Cu-O system superconducting thin film formed on a substrate comprising [110] single crystals of an ABO.sub.3 type oxide having a perovskite structure, in which a (119) face is selectively grown relative to a substrate surface. The film is formed on the substrate by chemical vapor deposition process. A method of manufacturing a BiSrCaCuO system superconducting film in which an a-axis is oriented preferentially relative to the surface of a substrate comprising MgO (100) single crystals, wherein the chemical composition ratio (Sr+Ca+Cu)/Bi of the BiSrCaCuO system superconducting film is made not less than 3.5. A Bi-Sr-Ca-Cu-O system superconducting thin film formed on a substrate comprising MgO [110] single crystals, in which a (110) face is selectively grown to the substrate surface. The film is formed on the substrate by a chemical vapor deposition process.
摘要翻译：在包含[110]具有钙钛矿结构的ABO 3型氧化物的单晶的衬底上形成的Bi-Sr-Ca-Cu-O系超导薄膜，其中（119）面相对于衬底表面选择性地生长。该薄膜通过化学气相沉积工艺在基板上形成。制造BiSrCaCuO系超导膜的方法，其中a轴相对于包含MgO（100）单晶的衬底的表面优先取向，其中BiSrCaCuO的化学组成比（Sr + Ca + Cu）/ Bi 系统超导薄膜不低于3.5。在包含MgO [110]单晶的基板上形成的Bi-Sr-Ca-Cu-O系超导薄膜，其中（110）面选择性地生长到基板表面。通过化学气相沉积工艺在基板上形成膜。

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