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1. 发明授权

US08624021B2 Compound and process for producing amide compound therewith 有权
标题翻译：用于生产酰胺化合物的化合物和方法
公开(公告)号：US08624021B2
公开(公告)日：2014-01-07
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02 , C07D201/04
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供了新的环十二烷酮-O-氮杂环十二烯-2-基肟和环十二酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

2. 发明申请

US20130005961A1 NOVEL COMPOUND AND PROCESS FOR PRODUCING AMIDE COMPOUND THEREWITH 有权
标题翻译：新型化合物及其生产方法
公开(公告)号：US20130005961A1
公开(公告)日：2013-01-03
申请号：US13497687
申请日：2010-09-24
申请人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
发明人： Tsunemi Sugimoto , Mitsuru Kishishita , Junichi Kugimoto , Kazunori Kurosawa , Hideo Shimomura , Ryouta Yasumatsu
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention provides novel cyclododecanone-O-azacyclotridecen-2-yloxime and cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride. The invention also provides a process for producing an amide compound wherein cyclododecanone-O-azacyclotridecen-2-yloxime, hydrogen chloride and/or Lewis acid or cyclododecanone-O-azacyclotridecen-2-yloxime hydrochloride are used as a rearrangement catalyst and/or a reaction starting material in a reaction step.
摘要翻译：本发明提供新的环十二烷酮-O-氮杂环十二烷-2-基肟和环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐。本发明还提供一种制备酰胺化合物的方法，其中使用环十二酮-O-氮杂环十二碳-2-肟，氯化氢和/或路易斯酸或环十二烷酮-O-氮杂环十二烯-2-基肟酸盐酸盐作为重排催化剂和/或反应步骤中的反应原料。

3. 发明申请

US20110065913A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20110065913A1
公开(公告)日：2011-03-17
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

4. 发明授权

US08309714B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08309714B2
公开(公告)日：2012-11-13
申请号：US12744675
申请日：2008-11-19
申请人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro Ii
发明人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro Ii
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Provided is a process for efficiently producing laurolactam by simple steps from cyclododecanone and hydroxylamine. This production process comprises the steps of: (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an oxime-formation solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase; (c) removing a part or all of the oxime-formation solvent and dissolved water from the solution of cyclododecanone oxime which is collected as an oil phase in the oil/aqueous phase separation step, whereby preparing a solution containing a rearrangement solvent to be used in a rearrangement reaction in a later step and the cyclododecanone oxime; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating and removing the rearrangement solvent and the rearrangement catalyst from the reaction mixture after the rearrangement step, and purifying the laurolactam.
摘要翻译：提供一种通过简单的步骤从环十二酮和羟胺有效地生产十二内酰胺的方法。该制备方法包括以下步骤：（a）在肟形成溶剂存在下，使环十二酮与羟胺在水溶液中反应，生成环十二烷酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油相和水相，并收集油相的环十二烷酮肟溶液; （c）从油/水相分离步骤中以油相收集的环十二烷酮肟溶液中除去部分或全部肟形成溶剂和溶解的水，由此制备含有使用的重排溶剂的溶液在后续步骤中的重排反应和环十二酮肟; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后从反应混合物中分离和除去重排溶剂和重排催化剂，并纯化月桂内酰胺。

5. 发明授权

US08338589B2 Process for producing laurolactam 有权
标题翻译：生产月桂内酰胺的方法
公开(公告)号：US08338589B2
公开(公告)日：2012-12-25
申请号：US12993451
申请日：2009-05-19
申请人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
发明人： Junichi Kugimoto , Nobuhiro Ii , Takashi Doi , Satoru Fujitsu , Tadashi Gotou , Hideo Shimomura , Ryouta Yasumatsu , Joji Kawai
IPC分类号： C07D201/04 , C07D225/02
CPC分类号： C07D201/04 , C07D225/02
摘要： The present invention relates to a process for producing laurolactam from cyclododecanone oxime by liquid-phase rearrangement reaction using trichlorotriazine as a rearrangement catalyst. The present invention can provide a process which can solve the problem of termination of the reaction at a certain conversion, can prevent an inactive precipitate generated from trichlorotriazine from precipitating in the course of the reaction process, and can remove an inactive precipitate, an active intermediate and a residual catalyst.
摘要翻译：本发明涉及使用三氯三嗪作为重排催化剂通过液相重排反应从环十二酮肟生产十二内酰胺的方法。本发明可以提供能够解决在一定转化时终止反应的问题的方法，可以防止三氯三嗪在反应过程中产生的不活泼的沉淀物沉淀，并且可以除去无活性的沉淀物，活性中间体和残留催化剂。

6. 发明申请

US20100267944A1 PROCESS FOR PRODUCING LAUROLACTAM 有权
标题翻译：生产乳酸菌的方法
公开(公告)号：US20100267944A1
公开(公告)日：2010-10-21
申请号：US12744675
申请日：2008-11-19
申请人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
发明人： Junichi Kugimoto , Joji Kawai , Hideo Shimomura , Ryouta Yasumatsu , Nobuhiro II
IPC分类号： C07D225/02
CPC分类号： C07D201/04 , C07D225/02 , Y02P20/582
摘要： Provided is a process for efficiently producing laurolactam by simple steps from cyclododecanone and hydroxylamine. This production process comprises the steps of: (a) reacting cyclododecanone with hydroxylamine in an aqueous solution in the presence of an oxime-formation solvent to produce cyclododecanone oxime; (b) separating the reaction mixture obtained after the oxime-forming step into an oil and an aqueous phases and collecting a solution of cyclododecanone oxime of the oil phase; (c) removing a part or all of the oxime-formation solvent and dissolved water from the solution of cyclododecanone oxime which is collected as an oil phase in the oil/aqueous phase separation step, whereby preparing a solution containing a rearrangement solvent to be used in a rearrangement reaction in a later step and the cyclododecanone oxime; (d) producing laurolactam from cyclododecanone oxime by rearrangement reaction using an aromatic-ring containing compound as a rearrangement catalyst; and (e) separating and removing the rearrangement solvent and the rearrangement catalyst from the reaction mixture after the rearrangement step, and purifying the laurolactam.
摘要翻译：提供一种通过简单的步骤从环十二酮和羟胺有效地生产十二内酰胺的方法。该制备方法包括以下步骤：（a）在肟形成溶剂存在下，使环十二酮与羟胺在水溶液中反应，生成环十二酮肟; （b）将在肟形成步骤后获得的反应混合物分离成油相和水相，并收集油相的环十二烷酮肟溶液; （c）从油/水相分离步骤中以油相收集的环十二酮肟溶液中除去部分或全部肟形成溶剂和溶解的水，由此制备含有使用的重排溶剂的溶液在后续步骤中的重排反应和环十二酮肟; （d）使用含芳环的化合物作为重排催化剂，通过重排反应从环十二酮肟生产月桂内酰胺; 和（e）在重排步骤之后从反应混合物中分离和除去重排溶剂和重排催化剂，并纯化月桂内酰胺。

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