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1. 发明授权

US08394902B2 Pyridyldiamido transition metal complexes, production and use thereof 有权
标题翻译：吡啶基二氨基过渡金属络合物，其制备和应用
公开(公告)号：US08394902B2
公开(公告)日：2013-03-12
申请号：US13071738
申请日：2011-03-25
申请人： John R. Hagadorn , Renuka N. Ganesh , Dmitry V. Uborsky , Ilya S. Borisov , Ivan V. Pruss , Alexander Z. Voskoboynikov
发明人： John R. Hagadorn , Renuka N. Ganesh , Dmitry V. Uborsky , Ilya S. Borisov , Ivan V. Pruss , Alexander Z. Voskoboynikov
IPC分类号： C08F4/16 , C07F17/00
CPC分类号： C08F10/00 , B01J31/143 , B01J31/146 , B01J31/1815 , B01J31/183 , B01J2531/0241 , B01J2531/0297 , B01J2531/48 , B01J2531/49 , C07D213/38 , C07D213/48 , C07D213/53 , C07F7/00 , C07F7/003 , C08F110/06 , C08F210/16 , C08F2500/03 , C08F210/14 , C08F4/64148 , C08F4/64144
摘要： Pyridyldiamido transition metal complexes are disclosed for use in alkene polymerization.
摘要翻译：公开了用于烯烃聚合的吡啶基二酰氨基过渡金属络合物。

2. 发明申请

US20120071616A1 Pyridyldiamido Transition Metal Complexes, Production And Use Thereof 有权
标题翻译：吡啶二氨基过渡金属络合物，其生产和使用
公开(公告)号：US20120071616A1
公开(公告)日：2012-03-22
申请号：US13071738
申请日：2011-03-25
申请人： John R. Hagadorn , Renuka N. Ganesh , Dmitry V. Uborsky , Ilya S. Borisov , Ivan V. Pruss , Alexander Z. Voskoboynikov
发明人： John R. Hagadorn , Renuka N. Ganesh , Dmitry V. Uborsky , Ilya S. Borisov , Ivan V. Pruss , Alexander Z. Voskoboynikov
IPC分类号： C08F2/00 , C08F4/659 , C08F10/06 , C08F4/76 , C07F7/00 , C08F10/02
CPC分类号： C08F10/00 , B01J31/143 , B01J31/146 , B01J31/1815 , B01J31/183 , B01J2531/0241 , B01J2531/0297 , B01J2531/48 , B01J2531/49 , C07D213/38 , C07D213/48 , C07D213/53 , C07F7/00 , C07F7/003 , C08F110/06 , C08F210/16 , C08F2500/03 , C08F210/14 , C08F4/64148 , C08F4/64144
摘要： Pyridyldiamido transition metal complexes are disclosed for use in alkene polymerization.
摘要翻译：公开了用于烯烃聚合的吡啶基二酰氨基过渡金属络合物。

3. 发明授权

US08546595B2 Halogen substituted heteroatom-containing metallocene compounds for olefin polymerization 有权
标题翻译：用于烯烃聚合的卤素取代的含杂原子的茂金属化合物
公开(公告)号：US08546595B2
公开(公告)日：2013-10-01
申请号：US13424782
申请日：2012-03-20
申请人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
发明人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
IPC分类号： C07F17/00 , C08F4/6592
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65925 , C08F2420/02 , C08F2420/06 , Y10S526/943 , C08F4/65927 , C08F4/6592 , C08F110/06 , C08F2500/02 , C08F2500/03 , C08F210/16 , C08F210/14 , C08F110/02
摘要： Halogen substituted metallocene compounds are described and comprise one or more monocyclic or polycyclic ligands that are pi-bonded to the metal atom and include at least one halogen substituent directly bonded to an sp2 carbon atom at a bondable ring position of the ligand, wherein the or at least one ligand has one or more ring heteroatoms in its cyclic structure. When combined with a suitable activator, these compounds show activity in the polymerization of olefins, such as ethylene and propylene.
摘要翻译：描述了卤素取代的茂金属化合物，并且包含一个或多个单键或多环配体，其与金属原子π键合，并且包括至少一个与配体的可键合环位置上的sp2碳原子键合的卤素取代基，其中或至少一个配体在其环状结构中具有一个或多个环杂原子。当与合适的活化剂组合时，这些化合物在烯烃如乙烯和丙烯的聚合中显示出活性。

4. 发明授权

US07667064B2 Halogen substituted metallocene compounds for olefin polymerization 有权
标题翻译：用于烯烃聚合的卤素取代的金属茂化合物
公开(公告)号：US07667064B2
公开(公告)日：2010-02-23
申请号：US11302798
申请日：2005-12-14
申请人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Dmitry V. Uborsky , Alexander V. Lygin , Catalina L. Coker , Jo Ann M. Canich
发明人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Dmitry V. Uborsky , Alexander V. Lygin , Catalina L. Coker , Jo Ann M. Canich
IPC分类号： C07F17/00 , C07F7/00 , C08F4/6392 , C08F4/6592 , B01J31/22
CPC分类号： C07F17/00 , Y10S526/943
摘要： A metallocene compound is represented by the formula (1): AMXn-1 wherein M is a transition metal atom having a coordination number of n selected from Group 3, 4, 5 or 6 of the Periodic Table of Elements, or a lanthanide metal atom, or actinide metal atom; A is a substituted monocyclic or polycyclic arenyl ligand pi-bonded to M, wherein said arenyl ligand includes at least one halogen substituent directly bonded to any sp2 carbon atom at a bondable ring position of the ligand; and the or each X is a univalent anionic ligand, or two X are joined and bound to the metal atom to form a metallocycle ring, or two X are joined to form a chelating ligand, a diene ligand, or an alkylidene ligand.
摘要翻译：金属茂化合物由式（1）表示：AMXn-1其中M是具有选自元素周期表第3,4,5或6族的配位数n的过渡金属原子，或镧系元素金属原子，或锕系金属原子; A是与M结合的取代的单环或多环的烷基配体，其中所述的异戊基配位体包括至少一个与配体的可键合环位置上的任何sp 2碳原子键合的卤素取代基; 并且该X或每个X是一价阴离子配体，或两个X连接并结合到金属原子上以形成金属环，或者两个X连接形成螯合配体，二烯配体或亚烷基配体。

5. 发明授权

US07868197B2 Halogen substituted heteroatom-containing metallocene compounds for olefin polymerization 有权
标题翻译：用于烯烃聚合的卤素取代的含杂原子的茂金属化合物
公开(公告)号：US07868197B2
公开(公告)日：2011-01-11
申请号：US11300240
申请日：2005-12-14
申请人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
发明人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
IPC分类号： C07F17/00 , C08F4/6192 , C08F4/6592 , B01J31/22
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65925 , C08F2420/02 , C08F2420/06 , Y10S526/943 , C08F4/65927 , C08F4/6592 , C08F110/06 , C08F2500/02 , C08F2500/03 , C08F210/16 , C08F210/14 , C08F110/02
摘要： Halogen substituted metallocene compounds are described and comprise one or more monocyclic or polycyclic ligands that are pi-bonded to the metal atom and include at least one halogen substituent directly bonded to an sp2 carbon atom at a bondable ring position of the ligand, wherein the or at least one ligand has one or more ring heteroatoms in its cyclic structure. When combined with a suitable activator, these compounds show activity in the polymerization of olefins, such as ethylene and propylene.
摘要翻译：描述了卤素取代的茂金属化合物，并且包含一个或多个单键或多环配体，其与金属原子π键合，并且包括至少一个与配体的可键合环位置上的sp2碳原子键合的卤素取代基，其中或至少一个配体在其环状结构中具有一个或多个环杂原子。当与合适的活化剂组合时，这些化合物在烯烃如乙烯和丙烯的聚合中显示出活性。

6. 发明授权

US08173828B2 Halogen substituted heteroatom-containing metallocene compounds for olefin polymerization 有权
标题翻译：用于烯烃聚合的卤素取代的含杂原子的茂金属化合物
公开(公告)号：US08173828B2
公开(公告)日：2012-05-08
申请号：US12951814
申请日：2010-11-22
申请人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
发明人： Alexander Z. Voskoboynikov , Alexey N. Ryabov , Mikhail V. Nikulin , Alexander V. Lygin , Dmitry V. Uborsky , Catalina L. Coker , Jo Ann M. Canich
IPC分类号： C07F17/00 , C08F4/6192 , C08F4/6592 , B01J31/22
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65925 , C08F2420/02 , C08F2420/06 , Y10S526/943 , C08F4/65927 , C08F4/6592 , C08F110/06 , C08F2500/02 , C08F2500/03 , C08F210/16 , C08F210/14 , C08F110/02
摘要： Halogen substituted metallocene compounds are described and comprise one or more monocyclic or polycyclic ligands that are pi-bonded to the metal atom and include at least one halogen substituent directly bonded to an sp2 carbon atom at a bondable ring position of the ligand, wherein the or at least one ligand has one or more ring heteroatoms in its cyclic structure. When combined with a suitable activator, these compounds show activity in the polymerization of olefins, such as ethylene and propylene.
摘要翻译：描述了卤素取代的茂金属化合物，并且包含一个或多个单键或多环配体，其与金属原子π键合，并且包括至少一个与配体的可键合环位置上的sp2碳原子键合的卤素取代基，其中或至少一个配体在其环状结构中具有一个或多个环杂原子。当与合适的活化剂组合时，这些化合物在烯烃如乙烯和丙烯的聚合中显示出活性。

7. 发明申请

US20130276519A1 Methods of Separating Compounds 审中-公开
标题翻译：分离化合物的方法
公开(公告)号：US20130276519A1
公开(公告)日：2013-10-24
申请号：US13452429
申请日：2012-04-20
申请人： Dmitry V. Uborsky , Alexander Z. Voskoboynikov , Hasnain Rangwalla , Jo Ann M. Canich
发明人： Dmitry V. Uborsky , Alexander Z. Voskoboynikov , Hasnain Rangwalla , Jo Ann M. Canich
IPC分类号： G01N1/34
CPC分类号： G01N1/34 , B01D15/08
摘要： Methods for chromatography for metal compounds are disclosed herein. These methods relate to introducing an analyte solution into a chromatographic system comprising a liquid phase flowing through a solid stationary phase, wherein the solid stationary phase comprises graphitic carbon; and eluting compounds from the stationary phase with a retention factor greater than zero, wherein a chromatogram of the eluted compounds shows that the compounds are substantially resolved. Methods for determining the purity of mixtures of metal compounds are also disclosed.
摘要翻译：金属化合物的层析方法在本文中公开。这些方法涉及将分析物溶液引入包含流过固体固定相的液相的色谱系统，其中固体固定相包括石墨碳; 并从保留因子大于零的固定相洗脱化合物，其中洗脱的化合物的色谱图显示化合物基本上分解。还公开了确定金属化合物混合物的纯度的方法。

8. 发明授权

US08541522B2 Catalyst compounds and use thereof 失效
标题翻译：催化剂化合物及其用途
公开(公告)号：US08541522B2
公开(公告)日：2013-09-24
申请号：US12908268
申请日：2010-10-20
申请人： Garth R. Giesbrecht , Timothy M. Boller , Alexander Z. Voskoboynikov , Andrey F. Asachenko , Mikhail V. Nikulin , Alexey A. Tsarev
发明人： Garth R. Giesbrecht , Timothy M. Boller , Alexander Z. Voskoboynikov , Andrey F. Asachenko , Mikhail V. Nikulin , Alexey A. Tsarev
IPC分类号： C08F4/76 , C08F4/64 , C07F7/00
CPC分类号： C07F7/00
摘要： This invention relates to Group 4 catalyst compounds containing di-anionic tridentate nitrogen/oxygen based ligands. The catalyst compounds are useful, with or without activators, to polymerize olefins, particularly α-olefins, or other unsaturated monomers. Systems and processes to oligomerize and/or polymerize one or more unsaturated monomers using the catalyst compound, as well as the oligomers and/or polymers produced therefrom are also provided.
摘要翻译：本发明涉及含有二阴离子三齿氮/氧基配体的第4族催化剂化合物。催化剂化合物可用于或不使用活化剂聚合烯烃，特别是α-烯烃或其它不饱和单体。还提供了使用催化剂化合物低聚和/或聚合一种或多种不饱和单体的系统和方法，以及由其制备的低聚物和/或聚合物。

9. 发明申请

US20110098430A1 Catalyst Compounds and Use Thereof 失效
标题翻译：催化剂化合物及其用途
公开(公告)号：US20110098430A1
公开(公告)日：2011-04-28
申请号：US12908550
申请日：2010-10-20
申请人： Garth R. GIESBRECHT , Timothy M. Boller , Alexander Z. Voskoboynikov , Andrey F. Asachenko , Mikhail V. Nikulin , Alexey A. Tsarev
发明人： Garth R. GIESBRECHT , Timothy M. Boller , Alexander Z. Voskoboynikov , Andrey F. Asachenko , Mikhail V. Nikulin , Alexey A. Tsarev
IPC分类号： C08F4/76 , C07F7/00 , C07D213/30 , B01J31/12
CPC分类号： C07F7/00
摘要： This invention relates to Group 4 catalyst compounds containing di-anionic tridentate nitrogen/oxygen based ligands. The catalyst compounds are useful, with or without activators, to polymerize olefins, particularly α-olefins, or other unsaturated monomers. Systems and processes to oligomerize and/or polymerize one or more unsaturated monomers using the catalyst compound, as well as the oligomers and/or polymers produced therefrom are also provided.
摘要翻译：本发明涉及含有二阴离子三齿氮/氧基配体的第4族催化剂化合物。催化剂化合物在有或没有活化剂的情况下可用于聚合烯烃，特别是α-烯烃或其它不饱和单体。还提供了使用催化剂化合物低聚和/或聚合一种或多种不饱和单体的系统和方法，以及由其制备的低聚物和/或聚合物。

10. 发明授权

US07910783B2 Preparation of substituted bridged indenyl and related ligands 失效
标题翻译：取代的桥连茚基和相关配体的制备
公开(公告)号：US07910783B2
公开(公告)日：2011-03-22
申请号：US11302846
申请日：2005-12-14
申请人： Alexander Z. Voskoboynikov , Mikhail V. Nikulin , Alexey N. Ryabov , Alexander V. Lygin , Catalina L. Coker , Jo Ann M. Canich
发明人： Alexander Z. Voskoboynikov , Mikhail V. Nikulin , Alexey N. Ryabov , Alexander V. Lygin , Catalina L. Coker , Jo Ann M. Canich
IPC分类号： C07C13/28 , C07C13/32 , C07C13/465 , C07C13/567
CPC分类号： C07F17/00
摘要： A process for preparing a chelating ligand of the formula (II) from a chelating ligand of the formula (I) via an sp2-sp2 or sp2-sp3 coupling reaction with an organometallic compound of the formula (III). wherein B is a bridging group that is bonded to L1 and L2 in formula (I) and to L3 and L4 in formula (II); L1 is a substituted monocyclic or polycyclic ligand that comprises at least one chlorine, bromine, iodine, or sulfonate substituent, directly bonded to an sp2 carbon atom of the ring structure of the ligand; L2 is a monoanionic ligand; or L2 may, independently, be defined as L1; L3 is the same group as L1, but said at least one chlorine, bromine, iodine, or sulfonate substituent is replaced with a hydrocarbyl, substituted hydrocarbyl, halocarbyl, or substituted halocarbyl fragment; L4 is the same group as L2, though, when L2 is defined as L1, L4 may be the same as L3 or L1; R1 is a hydrocarbyl, substituted hydrocarbyl, halocarbyl, or substituted halocarbyl; M1 is an element of group 1, 2, 12, 13 or 14 of the Periodic Table of the Elements; each X2, if present, is selected independently from the group consisting of halogen atoms, the hydroxyl group, alkoxy groups, aryloxy groups, mesylate, tosylate and triflate; r is 1, 2 or 3, and t is 0, 1 or 2, where r+t corresponds to the oxidation number of M1.
摘要翻译：通过与式（III）的有机金属化合物的sp2-sp2或sp2-sp3偶联反应从式（I）的螯合配体制备式（II）的螯合配体的方法。其中B是与式（I）中的L1和L2键合并且在式（II）中与L3和L4键合的桥连基团; L1是取代的单环或多环配体，其包含直接键合到配体的环结构的sp2碳原子上的至少一个氯，溴，碘或磺酸盐取代基; L2是单阴离子配体; 或L2可以独立地定义为L1; L3是与L1相同的基团，但是所述至少一个氯，溴，碘或磺酸酯取代基被烃基取代的烃基，卤代烃基或取代的卤代烃基片段代替; L4与L2相同，但当L2定义为L1时，L4可以与L3或L1相同; R 1是烃基，取代的烃基，卤代烃基或取代的卤代烃基; M1是元素周期表第1,2,12,13或14族的元素; 每个X 2如果存在，独立地选自卤素原子，羟基，烷氧基，芳氧基，甲磺酸酯，甲苯磺酸酯和三氟甲磺酸酯; r为1,2或3，t为0,1或2，其中r + t对应于M1的氧化数。

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