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    • 1. 发明专利
    • Method for continuously producing organic titanium peroxo compound and device therefor
    • 连续生产有机钛白粉化合物的方法及其装置
    • JP2004043353A
    • 2004-02-12
    • JP2002202342
    • 2002-07-11
    • Japan Science & Technology CorpJfe Soldec CorpJfeソルデック株式会社Masato Kakihana垣花 眞人科学技術振興事業団
    • KAKIHANA MASATOMOCHIDA NORIAKISHINYA KIYOSHI
    • C07F7/28
    • PROBLEM TO BE SOLVED: To provide a method for continuously producing an organic titanium peroxo compound, by which the organic titanium peroxo compound having a high quality can stably be produced, and to provide a device for producing the same.
      SOLUTION: This method for continuously producing the organic titanium peroxo compound is characterized by comprising the first reaction process for continuously feeding metal titanium powder, hydrogen peroxide and ammonia water into a dissolution reaction tank maintained at a prescribed temperature to dissolve the metal titanium, thus producing the solution of the peroxotitanic acid, and the second reaction process for continuously feeding one or more organic complexing agents selected from the group consisting of carboxylic acids, acetylacetone and amines to the peroxotitanic acid solution discharged from the first reaction process, thus reacting with the peroxotatanic acid to produce the organic peroxo compound solution.
      COPYRIGHT: (C)2004,JPO
    • 待解决的问题:提供一种连续生产有机钛过氧化合物的方法,通过该方法可以稳定地制备高质量的有机钛过氧化合物,并提供其制造方法。 解决方案:用于连续生产有机钛过氧化合物的方法的特征在于包括将金属钛粉末,过氧化氢和氨水连续地供入到保持在规定温度下的溶解反应槽中以溶解金属钛的第一反应方法 ,从而产生过氧钛酸的溶液,以及将从羧酸,乙酰丙酮和胺中选择的一种以上有机络合剂连续供给到从第一反应工序排出的过氧钛酸溶液的第二反应方法, 用过氧自由酸生成有机过氧化合物溶液。 版权所有(C)2004,JPO