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1. 发明授权

US5306681A Method for recovery or maintaining the activity of hydroisomerization catalysts 失效
标题翻译：回收或维持加氢异构化催化剂活性的方法
公开(公告)号：US5306681A
公开(公告)日：1994-04-26
申请号：US37218
申请日：1993-03-26
申请人： James J. Schorfheide , Biddanda U. Achia
发明人： James J. Schorfheide , Biddanda U. Achia
IPC分类号： B01J27/13 , B01J23/96 , B01J27/28 , B01J38/50 , B01J38/56 , C10C3/04 , B01J20/34 , C10G73/00
CPC分类号： B01J23/96 , B01J38/56
摘要： The isomerization activity of hydroisomerization catalyst is recovered by subjecting the catalyst to a wash using light aromatic solvents at elevated temperature, e.g. toluene at 300.degree. C. This hot aromatic solvent wash may be preceded by a hot hydrogen containing gas strip. Catalyst activity can be maintained by the continuous or periodic addition of light aromatic solvent or light aromatic containing materials to the feeds sent to the isomerization catalyst.
摘要翻译：加氢异构化催化剂的异构化活性通过使用轻质芳族溶剂在高温下进行洗涤来回收。甲苯在300摄氏度。这种热的芳族溶剂洗涤之前可以是含氢气的氢气条。催化剂活性可以通过将轻芳族芳族溶剂或轻质芳族化合物材料连续或周期性地加入到送入异构化催化剂的进料中来维持。

2. 发明授权

US5212128A Method for recovering or maintaining the activity of hydroisomerization catalysts 失效
标题翻译：回收或维持加氢异构化催化剂活性的方法
公开(公告)号：US5212128A
公开(公告)日：1993-05-18
申请号：US799810
申请日：1991-11-29
申请人： James J. Schorfheide , Biddanda U. Achia
发明人： James J. Schorfheide , Biddanda U. Achia
IPC分类号： B01J27/13 , B01J23/96 , B01J27/28 , B01J38/50 , B01J38/56 , C10C3/04
CPC分类号： B01J23/96 , B01J38/56
摘要： The isomerization activity of hydroisomerization catalyst is recovered by subjecting the catalyst to a wash using light aromatic solvents at elevated temperature, e.g. toluene at 300.degree. C. This hot aromatic solvent wash may be preceded by a hot hydrogen containing gas strip. Catalyst activity can be maintained by the continuous or periodic addition of light aromatic solvent or light aromatic containing materials to the feeds sent to the isomerization catalyst.

3. 发明授权

US4592832A Process for increasing Bright Stock raffinate oil production 失效
标题翻译：增加明亮库存残油生产的过程
公开(公告)号：US4592832A
公开(公告)日：1986-06-03
申请号：US648013
申请日：1984-09-06
申请人： Duncan J. Bristow , Biddanda U. Achia , Lawrence J. Evers
发明人： Duncan J. Bristow , Biddanda U. Achia , Lawrence J. Evers
IPC分类号： C10G53/06 , C10G21/00
CPC分类号： C10G53/06
摘要： A process for increasing the production of Bright Stock oil in a lube oil process scheme. Aromatic extract oil, after being separated from the extraction solvent, is recycled back to the deasphalter unit and combined with a vacuum residuum in 10-20 LV %, based on the total deasphalter feed, prior to deasphalting. After deasphalting and aromatics extraction the absolute yield of raffinate is increased.
摘要翻译：一种在润滑油加工方案中增加Bright Stock油的生产的过程。芳烃提取油在与萃取溶剂分离后，再循环回脱沥青装置，并在脱沥青前基于脱沥青进料，与10-20％左右的真空残渣混合。脱沥青和芳烃萃取后，萃余液的绝对收率提高。

4. 发明授权

US5059299A Method for isomerizing wax to lube base oils 失效
标题翻译：将蜡异构化成润滑油基础油的方法
公开(公告)号：US5059299A
公开(公告)日：1991-10-22
申请号：US522275
申请日：1990-05-11
申请人： Ian A. Cody , James D. Bell , Theodore H. West , William A. Wachter , Biddanda U. Achia
发明人： Ian A. Cody , James D. Bell , Theodore H. West , William A. Wachter , Biddanda U. Achia
IPC分类号： C10G67/04
CPC分类号： C10G67/04
摘要： Slack waxes and synthetic wax are isomerized and processed into high viscosity index and very low pour point lube base stock oils and blending stocks by the process comprising the steps of hydrotreating the wax, if necessary, to remove heteroatom and polynuclear aromatic compounds and/or deoiling the wax, if necessary, to an oil content between about 5-20% oil, isomerizing the wax over a Group VI-Group VIII on halogenated refractory metal oxide support catalyst, said isomerization being conducted to a level of conversion such that .about.40% and less unconverted wax remains in the 330.degree. C..sup.+, preferably the 370.degree. C..sup.+ fraction sent to the dewaxer. The total isomerate from the isomerization unit is fractionated into a lube oil fraction boiling at 330.degree. C..sup.+, preferably 370.degree.p9 C..sup.+. This oil fraction is solvent dewaxed preferably using MEK/MIBK at 20/80 ratio and unconverted wax is recycled to the isomerization unit. Operating in this manner permits one to obtain isomerate oil of very high VI (in excess of 130) possessing low pours (-21.degree. C., preferably -24.degree. C., most preferably -27.degree. C.).
摘要翻译：松散蜡和合成蜡被异构化并加工成高粘度指数和极低倾点润滑油基础油和通过包括以下步骤的混合原料的方法：如果需要，加氢处理蜡以除去杂原子和多核芳族化合物和/或脱油如果需要，蜡可以含有约5-20％的油，在卤代难熔金属氧化物载体催化剂上使VI族VIII族上的蜡异构化，所述异构化进行到转化水平，使得DIFFERENCE 40％并且较少未转化的蜡保留在330℃+，优选370℃+馏分送至脱蜡机。来自异构化单元的总异构体被分馏成沸点在330℃+，优选370°p9℃+的润滑油馏分。该油馏分优选使用20/80比例的MEK / MIBK进行溶剂脱蜡，未转化的蜡再循环至异构化单元。以这种方式操作，可以获得具有低倾点（-21℃，优选-24℃，最优选-27℃）的非常高VI（超过130）的异构油。

5. 发明授权

US4937399A Method for isomerizing wax to lube base oils using a sized isomerization catalyst 失效
标题翻译：使用大小异构化催化剂将蜡异构化成润滑油基础油的方法
公开(公告)号：US4937399A
公开(公告)日：1990-06-26
申请号：US283680
申请日：1988-12-13
申请人： William A. Wachter , Ian A. Cody , Glen P. Hamner, deceased , Biddanda U. Achia
发明人： William A. Wachter , Ian A. Cody , Glen P. Hamner, deceased , Biddanda U. Achia
IPC分类号： B01J23/40 , B01J37/18 , B01J37/26 , C10G45/62
CPC分类号： B01J37/26 , B01J23/40 , B01J37/18 , C10G2400/10
摘要： The present invention is directed to a process for the catalytic isomerization of waxes to liquid products, particularly to the production of high yields of liquid products boiling in the 370.degree. C..sup.+ range suitable for use as lube oil base stocks or blending stocks, said process employing as the catalyst a material made by depositing a hydrogenation metal component on a refractory metal oxide base, preferably alumina, fluoriding said metal loaded base using aqueous HF and subsequently crushing the fluorided metal loaded base to produce a sized material of 1/32 inch and less its largest cross-sectional dimension. Alternately the catalyst can be made by depositing a hydrogenation metal component on a refractory metal oxide base of 1/32 inch and less across its largest cross-sectional dimension and subsequently fluoriding said sized material using aqueous HF. In either case the catalyst is activated before being used by heating in a hydrogen atmosphere to from 350.degree. C. to 500.degree. C. for from 1 to 48 hours or more.
摘要翻译：本发明涉及一种将蜡催化异构化成液体产品的方法，特别是在适用于润滑油基础油或混合原料的370℃+范围内沸腾的高产量液体产物的生产，所述方法该方法使用通过在难熔金属氧化物基底（优选氧化铝）上沉积氢化金属组分制备的材料，使用HF水溶液氟化所述金属负载的基底，随后粉碎载有氟化金属的基底以产生1/32英寸的尺寸的材料并且减小其最大横截面尺寸。或者，催化剂可以通过在其最大横截面尺寸上在1/32英寸以下的难熔金属氧化物基底上沉积加氢金属组分并随后使用HF水溶液氟化所述尺寸的材料来制备。在任一情况下，催化剂在通过在氢气气氛中加热至350℃至500℃使用1至48小时或更长时间之前被活化。

6. 发明授权

US4673485A Process for increasing deasphalted oil production from upgraded residua 失效
标题翻译：从升级后的残渣中提高脱沥青油产量的过程
公开(公告)号：US4673485A
公开(公告)日：1987-06-16
申请号：US597437
申请日：1984-04-06
申请人： Duncan J. Bristow , Biddanda U. Achia , Lawrence J. Evers
发明人： Duncan J. Bristow , Biddanda U. Achia , Lawrence J. Evers
IPC分类号： C10G21/00 , C10G55/04 , C10G67/04 , C10C3/00 , C10G1/00 , C10G1/04
CPC分类号： C10G67/0454 , C10G21/003 , C10G55/04
摘要： A process in fuels production for increasing the yield of deasphalted oil production from upgraded residua and improving deasphalter operability involving mixing the upgraded residua with an aromatics solubilizing aid to prevent the formation of an immiscible third phase during deasphalting.
摘要翻译：一种燃料生产过程，用于提高脱沥青油产量从升级残渣中获得的产量，并改善脱沥青的可操作性，包括将升华后的残渣与芳烃增溶助剂混合，以防止在脱沥青期间形成不混溶的第三相。

7. 发明授权

US4203824A Polyvinylpyrrolidone dewaxing aid for bright stocks 失效
标题翻译：聚乙烯吡咯烷酮脱蜡助剂
公开(公告)号：US4203824A
公开(公告)日：1980-05-20
申请号：US972230
申请日：1978-12-22
申请人： Biddanda U. Achia , David H. Shaw
发明人： Biddanda U. Achia , David H. Shaw
IPC分类号： C10G73/16 , C10G73/04 , C10G43/06 , C10G43/08
CPC分类号： C10G73/04
摘要： Polyvinylpyrrolidone having a number average molecular weight ranging from about 150,000 to 400,000 has been found to be an effective dewaxing aid for bright stock in ketone dewaxing processes. Using as little as 100 ppm based on the waxy oil can result in almost a 50% increase in the filter rate of the dewaxed oils from the wax.
摘要翻译：已经发现数均分子量为约150,000至400,000的聚乙烯吡咯烷酮是用于酮脱蜡方法中光亮原料的有效脱蜡助剂。基于蜡油使用少至100ppm可以使来自蜡的脱蜡油的过滤速率几乎增加50％。

8. 发明授权

US4594142A Dewaxing waxy hydrocarbon oils using di-alkyl fumarate-vinyl laurate copolymer dewaxing aids 失效
标题翻译：使用富马酸二烷基酯 - 月桂酸乙烯酯共聚物脱蜡助剂来脱蜡蜡质油
公开(公告)号：US4594142A
公开(公告)日：1986-06-10
申请号：US727021
申请日：1985-04-25
申请人： Biddanda U. Achia , Abraham R. DeKraker , Albert Rossi
发明人： Biddanda U. Achia , Abraham R. DeKraker , Albert Rossi
IPC分类号： C10G73/02 , C10G73/04 , C10G73/12
CPC分类号： C10G73/04
摘要： A solvent dewaxing process is described comprising mixing a waxy hydrocarbon oil, preferably a waxy petroleum oil, most preferably a waxy lube or specialties oil, with dewaxing solvent and a dewaxing aid comprising (A) a dialkylfumarate-vinyl laurate copolymer and (B) a wax-naphthalene condensation copolymer, a dialkyl fumarate-vinyl acetate copolymer or an ethylene vinyl acetate copolymer and chilling the mixture to yield a slurry comprising solid particles of precipitated wax and a solution of dewaxed oil and solvent and separating said solid wax from dewaxed oil solution.
摘要翻译：描述了溶剂脱蜡方法，其包括将蜡质烃油，优选石蜡油，最优选蜡状润滑剂或特种油与脱蜡溶剂和脱蜡助剂混合，所述脱蜡助剂包含（A）富马酸二乙酯 - 月桂酸乙烯酯共聚物和（B）蜡 - 萘缩合共聚物，富马酸二乙酯 - 乙酸乙烯酯共聚物或乙烯 - 乙酸乙烯酯共聚物，并冷却该混合物以产生包含沉淀蜡的固体颗粒和脱蜡油和溶剂的溶液的浆料，并将所述固体蜡与脱蜡油溶液。

9. 发明授权

US4522710A Method for increasing deasphalted oil production 失效
标题翻译：增加脱沥青油生产的方法
公开(公告)号：US4522710A
公开(公告)日：1985-06-11
申请号：US559736
申请日：1983-12-09
申请人： Biddanda U. Achia , David H. Shaw , James D. Bushnell
发明人： Biddanda U. Achia , David H. Shaw , James D. Bushnell
IPC分类号： C10G21/00 , C10C3/06 , C10C3/08
CPC分类号： C10G21/003
摘要： A method for increasing the production of deasphalted oil is described. The method comprises passing a hydrocarbon feedstock into a first distillation zone wherein the feedstock is separated into a first distillate and a first residuum. First residuum is passed to a second distillation zone wherein the fraction is separated into a second distillate and a second residuum. Second distillate and residuum are passed to a deasphalting zone and contacted with a solvent to produce a deasphalted oil. This method may produce increased quantities of acceptable quality deasphalted oil where the deasphalting zone is rate-limiting.
摘要翻译：描述了用于增加脱沥青油的生产的方法。该方法包括使烃原料进入第一蒸馏区，其中原料被分离成第一馏出物和第一残渣。将第一残渣送入第二蒸馏区，其中将馏分分离成第二馏出物和第二残渣。第二馏出物和残渣通入脱沥青区并与溶剂接触以产生脱沥青油。该方法可以产生更多量的可接受质量的脱沥青油，其中脱沥青区是速率限制的。

10. 发明授权

US4377467A Solvent dewaxing waxy hydrocarbon oils using dewaxing aid 失效
标题翻译：使用脱蜡助剂的溶剂脱蜡蜡质烃油
公开(公告)号：US4377467A
公开(公告)日：1983-03-22
申请号：US229664
申请日：1981-01-30
申请人： Biddanda U. Achia
发明人： Biddanda U. Achia
IPC分类号： C10G73/04 , C10G73/06 , C10G73/08
CPC分类号： C10G73/04
摘要： An improved dewaxing aid for solvent dewaxing processes comprising a mixture of (a) lithium isostearate and (b) a polymer of an ester of at least one aliphatic alcohol with methacrylic acid or acrylic acid having an average molecular weight ranging from between about 300,000 to 2,000,000. The lithium isostearate, when combined with the acrylic polymer, synergistically improves the efficiency of wax separation. This has been found to be especially useful for dewaxing heavy petroleum oil fractions, such as bright stocks.
摘要翻译：一种用于溶剂脱蜡方法的改进的脱蜡助剂，其包含（a）异硬脂酸锂和（b）至少一种脂族醇与甲基丙烯酸或丙烯酸的酯的平均分子量在约30万至200万。异硬脂酸锂与丙烯酸聚合物组合时，协同地提高了蜡分离的效率。已经发现这对于脱蜡重质石油馏分如亮油是特别有用的。

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