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    • 1. 发明授权
    • Method for producing optical glass
    • 光学玻璃的制造方法
    • US4324576A
    • 1982-04-13
    • US209711
    • 1980-11-21
    • Iwao MatsuyamaKenzo SusaShin SatohTsuneo Suganuma
    • Iwao MatsuyamaKenzo SusaShin SatohTsuneo Suganuma
    • C01B33/16C03B8/02C03B19/12C03B37/016C03C3/04C03C13/04C03C3/06
    • C01B33/163C03B19/12C03B37/016C03C13/045C03C3/04Y02P40/57Y10S65/901
    • A method for producing optical glass, which comprises charging a mixed solution capable of forming a high-silica-content gel by hydrolysis reaction into a vessel, the inner wall face of which is composed of a material unwettable to the mixed solution, such as a fluorocarbon resin or silicone resin, causing gelation of the mixed solution in the vessel, drying the obtained gel, and heating and sintering the obtained dry gel. When electrodes are placed in the mixed solution at the gelation step and an electric voltage is applied, the time required for formation of the gel is shortened. Furthermore, at the gel-drying step, if the amount of materials evaporated from the gel is detected or the weight of the gel is measured, the detected amount of the evaporated materials or the change of the weight of the gel is fed back to a factor regulating the drying speed, such as the drying temperature to control the drying speed to an appropriate level.
    • 一种光学玻璃的制造方法,其特征在于,将能够通过水解反应形成高二氧化硅含量凝胶的混合溶液装入容器内,该容器的内壁面由不能混合的溶液的材料构成, 氟树脂或有机硅树脂,使混合溶液凝胶化,容器干燥,加热烧结得到的干凝胶。 当在凝胶化步骤中将电极置于混合溶液中并施加电压时,形成凝胶所需的时间缩短。 此外,在凝胶干燥步骤中,如果检测到从凝胶蒸发的材料的量或测量凝胶的重量,则将检测到的蒸发材料量或凝胶重量的改变反馈至 调节干燥速度的因素,如干燥温度,将干燥速度控制在适当的水平。
    • 6. 发明授权
    • Method of producing optical fiber
    • 生产光纤的方法
    • US4203743A
    • 1980-05-20
    • US933672
    • 1978-08-14
    • Tsuneo SuganumaKoji IshidaShin SatohMamoru SugieToshio KatsuyamaGyozo Toda
    • Tsuneo SuganumaKoji IshidaShin SatohMamoru SugieToshio KatsuyamaGyozo Toda
    • C03B37/018G02B6/02G02B6/028C03B37/02
    • G02B6/03627C03B37/018C03B37/01861G02B6/02C03B2203/26G02B6/0281G02B6/03611Y10S65/16
    • A method of producing an optical fiber comprising (i) the step of depositing a glass film of desired refractive index onto the inner wall surface of a quartz tube by the CVD (chemical vapor deposition) process, (ii) the step of heating the quartz tube to a high temperature while the gas of a compound which forms an oxide, enhancing the refractive index of the glass film, in an oxidizing atmosphere at the high temperature is kept flowing into the quartz tube along with an oxidizing gas, (iii) the step of heating and collapsing the quartz tube into a solid rod or the so-called preform, and (iv) the step of heating and drawing the optical fiber preform into the optical fiber.In the optical fiber produced by this method of manufacture, the lowering of the refractive index of the central part of the optical fiber is sharply reduced.At the step (iii), one end of the quartz tube is sealed and a gas is introduced into the tube from the other end so as to slightly raise the internal pressure of the tube, whereby a more favorable result is obtained.
    • 一种制造光纤的方法,包括(i)通过CVD(化学气相沉积)工艺在石英管的内壁表面上沉积所需折射率的玻璃膜的步骤,(ii)加热石英的步骤 在高温下在氧化气氛中形成氧化物的化合物的气体(在玻璃膜的氧化气氛中)的气体与氧化气体一起流入石英管中,(iii) 将石英管加热和塌缩成实心棒或所谓的预制件的步骤,以及(iv)将光纤预制件加热和拉制成光纤的步骤。 在通过该制造方法制造的光纤中,光纤的中心部分的折射率的降低急剧降低。 在步骤(iii)中,密封石英管的一端,从另一端引入气体,从而稍微升高管的内压,得到更好的结果。