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1. 发明申请

US20090020695A1 MASS SPECTROMETER 有权
标题翻译：质谱仪
公开(公告)号：US20090020695A1
公开(公告)日：2009-01-22
申请号：US12173328
申请日：2008-07-15
申请人： Hiroyuki Satake , Yuichiro Hashimoto , Yasuaki Takada
发明人： Hiroyuki Satake , Yuichiro Hashimoto , Yasuaki Takada
IPC分类号： B01D59/44
CPC分类号： H01J49/004 , H01J49/422 , H01J49/4255 , H01J49/427
摘要： A mass spectrometer includes a linear multipole electrode, an auxiliary electrode that applies a DC potential on the center axis of the linear multipole electrode, and a DC power supply that supplies a DC power to the auxiliary electrode. The DC potential slope formed on the center axis of the multipole electrode is changed according to the measuring condition. The ejection time of ions can be adjusted optimally by adjusting the potential slope so as to satisfy the measuring condition. If the ejection time of ions is shortened, confusion of different ion information items that might otherwise occur on a spectrum can be avoided. If the ejection time of ions is lengthened, detection limit exceeding can be avoided and ions can be measured efficiently, thereby highly efficient ion measurements are always assured.
摘要翻译：质谱仪包括线性多极电极，在线性多极电极的中心轴上施加直流电位的辅助电极和向辅助电极提供直流电力的直流电源。根据测量条件改变在多极电极的中心轴上形成的直流电位斜率。通过调整电位斜率以满足测量条件，可以最佳地调节离子的喷射时间。如果离子的喷射时间缩短，则可以避免在光谱上可能发生的不同离子信息项的混淆。如果离子的喷射时间延长，则可以避免超过检测极限，有效测量离子，从而确保高效的离子测量。

2. 发明授权

US08044349B2 Mass spectrometer 有权
标题翻译：质谱仪
公开(公告)号：US08044349B2
公开(公告)日：2011-10-25
申请号：US12173328
申请日：2008-07-15
申请人： Hiroyuki Satake , Yuichiro Hashimoto , Yasuaki Takada
发明人： Hiroyuki Satake , Yuichiro Hashimoto , Yasuaki Takada
IPC分类号： H01J49/00
CPC分类号： H01J49/004 , H01J49/422 , H01J49/4255 , H01J49/427
摘要： A mass spectrometer includes a linear multipole electrode, an auxiliary electrode that applies a DC potential on the center axis of the linear multipole electrode, and a DC power supply that supplies a DC power to the auxiliary electrode. The DC potential slope formed on the center axis of the multipole electrode is changed according to the measuring condition. The ejection time of ions can be adjusted optimally by adjusting the potential slope so as to satisfy the measuring condition. If the ejection time of ions is shortened, confusion of different ion information items that might otherwise occur on a spectrum can be avoided. If the ejection time of ions is lengthened, detection limit exceeding can be avoided and ions can be measured efficiently, thereby highly efficient ion measurements are always assured.
摘要翻译：质谱仪包括线性多极电极，在线性多极电极的中心轴上施加直流电位的辅助电极和向辅助电极提供直流电力的直流电源。根据测量条件改变在多极电极的中心轴上形成的直流电位斜率。通过调整电位斜率以满足测量条件，可以最佳地调节离子的喷射时间。如果离子的喷射时间缩短，则可以避免在光谱上可能发生的不同离子信息项的混淆。如果离子的喷射时间延长，则可以避免超过检测极限，有效测量离子，从而确保高效的离子测量。

3. 发明授权

US06580067B1 Sample analyzing monitor and combustion control system using the same 有权
标题翻译：采用分析监测和燃烧控制系统的样品分析
公开(公告)号：US06580067B1
公开(公告)日：2003-06-17
申请号：US09712132
申请日：2000-11-15
申请人： Masuyoshi Yamada , Yuichiro Hashimoto , Minoru Sakairi , Yasuaki Takada , Masami Sakamoto , Tomoyuki Tobita
发明人： Masuyoshi Yamada , Yuichiro Hashimoto , Minoru Sakairi , Yasuaki Takada , Masami Sakamoto , Tomoyuki Tobita
IPC分类号： H01J4900
CPC分类号： H01J49/0009 , F23G5/50 , G01N33/0049 , H01J49/0422
摘要： The present invention is to provide a monitoring device making it possible to measure the concentration of a target trace gas which has an ionization efficiency changed by the affect of impurities and which is absorbed on a pretreatment portion or piping, at a high accuracy and at real time, by adding an internal standard having a known concentration to the target trace gas. The concentration of the target trace gas is measured while an internal standard having substantially the same properties (such as ionization efficiency change and vapor pressure) as the target trace gas is added. The ion strengths of the target trace gas and the internal standard are compared to calibrate the concentration of the target trace gas. According to the present invention, the concentration of the target trace gas in gas containing impurities can be online measured at a real time and at high accuracy while being continuously calibrated.
摘要翻译：本发明提供一种监测装置，使得可以以高精度和实际地测量具有由杂质影响而改变并且被吸收在预处理部分或管道上的电离效率的目标痕量气体的浓度通过向目标痕量气体添加具有已知浓度的内标，测定目标痕量气体的浓度，同时测定作为目标痕量气体具有基本相同性质（如电离效率变化和蒸气压）的内标被添加。将目标痕量气体和内标的离子强度进行比较，校正目标痕量气体的浓度。根据本发明，可以在线测量含有杂质的气体中的痕量气体的浓度，在高精度的同时连续校准。

4. 发明授权

US06194716B1 Method for mass calibration 有权
标题翻译：质量校准方法
公开(公告)号：US06194716B1
公开(公告)日：2001-02-27
申请号：US09143399
申请日：1998-08-28
申请人： Yasuaki Takada , Takayuki Nabeshima , Minoru Sakairi , Yuichiro Hashimoto
发明人： Yasuaki Takada , Takayuki Nabeshima , Minoru Sakairi , Yuichiro Hashimoto
IPC分类号： B01D5944
CPC分类号： H01J49/424 , H01J49/0009 , H01J49/428
摘要： A method for performing a mass calibration under an application of a desired ion peak position of mass spectrum attained by a mass scanning of ions of substance having a known value of m/z and the known value of m/z is added with a step for ejecting an amount of unnecessary ions not contributing to the aforesaid mass calibration accumulated in the aforesaid ion trap type mass analysis region prior to the aforesaid mass scanning operation. An accumulation of a large amount of unnecessary ions in the ion trap type mass analysis region is restricted, a disturbance of electric field in the ion trap mass analysis region generated under an influence of a spatial charge caused by accumulation of the unnecessary ions can be prevented and the aforesaid mass calibration can be performed in an easy and accurate manner.
摘要翻译：在通过具有已知m / z值的物质的离子的质量扫描和已知的m / z值获得的质谱所需离子峰位置的施加下进行质量校准的方法添加了用于在上述质量扫描操作之前，排出在上述离子阱型质量分析区域中累积的对上述质量校准无贡献的不需要的离子的量。离子阱型质量分析区域中的大量不需要的离子的积聚受到限制，可以防止在由不需要的离子的积聚引起的空间电荷的影响下产生的离子阱质量分析区域中的电场的扰动并且可以容易且准确地进行上述质量校准。

5. 发明申请

US20120112059A1 MASS SPECTROMETER AND MASS SPECTROMETRY METHOD 有权
标题翻译：质谱仪和质谱方法
公开(公告)号：US20120112059A1
公开(公告)日：2012-05-10
申请号：US13383371
申请日：2010-07-09
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hisashi Nagano , Hideki Hasegawa , Yasuaki Takada , Masuyoshi Yamada
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hisashi Nagano , Hideki Hasegawa , Yasuaki Takada , Masuyoshi Yamada
IPC分类号： H01J49/26
CPC分类号： H01J49/004
摘要： An object is to measure both cations and anions with high duty cycle. In a mass spectrometer comprising an ion source (1), an ion guide part (31), and an ion trap (32), while ions are being mass-selectively ejected from the ion trap, ions having a polarity reverse to that of the ions trapped in the ion trap are introduced into the ion guide part.
摘要翻译：一个目标是测量阳离子和阴离子高占空比。在离子源（1），离子引导部（31）和离子阱（32）的质谱仪中，离子从离子阱中质量选择性地喷出时，具有与捕获在离子阱中的离子被引入离子引导部。

6. 发明申请

US20090179149A1 MASS SPECTROMETER AND MASS SPECTROMETRIC ANALYSIS METHOD 有权
标题翻译：质谱仪和质谱分析方法
公开(公告)号：US20090179149A1
公开(公告)日：2009-07-16
申请号：US12354245
申请日：2009-01-15
申请人： Masuyuki SUGIYAMA , Yuichiro Hashimoto , Hideki Hasegawa , Yasuaki Takada
发明人： Masuyuki SUGIYAMA , Yuichiro Hashimoto , Hideki Hasegawa , Yasuaki Takada
IPC分类号： B01D59/44 , H01J49/26
CPC分类号： H01J49/0045
摘要： An MS/MS spectrometric analysis method obtains throughput and mass resolving power of precursor ions. In a mass spectrometer, ions, which are introduced and accumulated in an ion trap unit, are resonance-extracted mass-selectively. A profile of precursor ions at the m/z axis of the ion trap and a profile at the mass analyzer portion, which performs mass analysis of the ions extracted from a collision induced dissociation portion, is obtained by performing a measurement when the injection energy to the collision induced dissociation portion is low, and when the injection energy to the collision induced dissociation portion is high. The profile at the m/z axis of the ion trap of the obtained two-dimensional spectrum is substituted with the profile at the m/z axis of the mass analyzer portion. In this way, the m/z of both the precursor ions and the fragment ions can be determined with high mass resolving power.
摘要翻译： MS / MS光谱分析方法获得前体离子的通量和质量分辨能力。在质谱仪中，离子阱单元中引入和积聚的离子是质量选择性共振提取的。在离子阱的m / z轴处的前体离子的轮廓和质量分析器部分的轮廓，其进行从碰撞诱导的解离部分提取的离子的质量分析，通过在将注入能量碰撞诱导的解离部分低，并且当碰撞诱导解离部分的注入能量高时。所获得的二维光谱的离子阱的m / z轴的轮廓被质量分析器部的m / z轴的轮廓所取代。以这种方式，可以以高质量分辨能力确定前体离子和碎片离子两者的m / z。

7. 发明申请

US20080277575A1 Ion mobility spectrometer and ion-mobility-spectrometry/mass-spectrometry hybrid spectrometer 有权
标题翻译：离子迁移光谱仪和离子迁移光谱/质谱混合光谱仪
公开(公告)号：US20080277575A1
公开(公告)日：2008-11-13
申请号：US12149737
申请日：2008-05-07
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Yasuaki Takada
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Yasuaki Takada
IPC分类号： H01J49/10
CPC分类号： G01N27/622
摘要： A low-cost and high-ion-transmission-ratio ion-mobility spectrometry filter, including an ion source, a first drift region in which a gas flow direction and a DC electric-field direction are opposite to each other, a second drift region in which a gas flow direction is provided, the gas flow direction being different from the gas flow direction in the first drift region, and being opposite to a DC electric-field application direction in the second drift region, an intermediate region having an electric field for causing ions to travel between the first drift region and the second drift region, and a detector for detecting ions which have passed through the first drift region and the second drift region.
摘要翻译：一种低成本和高离子透射比的离子迁移谱分析滤光器，包括离子源，气流方向和DC电场方向彼此相反的第一漂移区，第二漂移区其中设置有气体流动方向，气体流动方向与第一漂移区域中的气体流动方向不同，并且与第二漂移区域中的DC电场施加方向相反，具有电场的中间区域用于使离子在第一漂移区域和第二漂移区域之间行进;以及检测器，用于检测已经通过第一漂移区域和第二漂移区域的离子。

8. 发明授权

US06639215B2 Ion source and mass spectrometer 有权
标题翻译：离子源和质谱仪
公开(公告)号：US06639215B2
公开(公告)日：2003-10-28
申请号：US10053567
申请日：2002-01-24
申请人： Yasuaki Takada , Masuyoshi Yamada , Masao Suga , Yuichiro Hashimoto
发明人： Yasuaki Takada , Masuyoshi Yamada , Masao Suga , Yuichiro Hashimoto
IPC分类号： B01D5944
CPC分类号： H01J49/168 , H01J49/0445
摘要： To provide a mass spectrometer having a high sensitivity to dioxins. In the mass spectrometer including: a sample supply tube for supplying a sample solution containing a sample to be measured; a nebulizer for nebulizing the sample solution supplied from the sample supply tube; an ion source having a needle electrode for ionizing the sample nebulized and vaporized in the nebulizer; and a mass analyzer for analyzing ions formed in the ion source, and a gas of a flow rate corresponding to the flow rate of the sample solution is mixed to the vaporized sample, and a moving direction of the sample is made opposite to a moving direction of ions at a tip of the needle electrode.
摘要翻译：提供对二恶英具有高度敏感性的质谱仪。在质谱仪中，包括：供给含有待测样品的样品溶液的样品供给管; 用于将从样品供应管提供的样品溶液雾化的雾化器; 离子源，其具有针状电极，用于将在雾化器中雾化和蒸发的样品电离; 以及用于分析在离子源中形成的离子的质量分析器，将与样品溶液的流量对应的流量的气体混合到蒸发的样品中，使样品的移动方向与移动方向相反的针电极尖端的离子。

9. 发明授权

US08164053B2 Mass analyzer and mass analyzing method 有权
标题翻译：质量分析仪和质量分析方法
公开(公告)号：US08164053B2
公开(公告)日：2012-04-24
申请号：US12039306
申请日：2008-02-28
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Yasuaki Takada
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Yasuaki Takada
IPC分类号： B01D59/44
CPC分类号： H01J49/0045
摘要： There has been a problem that both detection sensitivity and throughput cannot be improved simultaneously by a conventional MS/MS analysis method.A mass analyzer having an ion trap for ejecting ions in a specific mass range, a collisional dissociation part for causing ions ejected from the ion trap to be dissociated, a mass analyzing part for performing a mass analysis of ions ejected from the collisional dissociation part, and a control part including a list in which measurement conditions for each ion are stored selectively resonance-ejects ions introduced into and accumulated in the ion trap based on masses. A scanning operation is a repetition of an operation of ejecting specific precursor ions in a direction of the collisional dissociation part and an operation of ejecting nothing, and each ion can be measured under optimal measurement conditions by controlling an output voltage of each part with reference to list information, realizing a mass analyzer that can perform an MS/MS measurement with high throughput and high sensitivity.
摘要翻译：存在通过常规MS / MS分析方法不能同时改善检测灵敏度和通过量的问题。 1.一种质量分析装置，具有用于将特定质量范围的离子排出的离子阱，用于使从离子阱排出的离子离解的碰撞解离部，用于进行从碰撞解离部喷出的离子的质量分析的质量分析部，以及包括其中存储每个离子的测量条件的列表的控制部分选择性地基于质量共振 - 喷射引入和积聚在离子阱中的离子。扫描操作是重复在碰撞解离部分的方向上排出特定的前体离子的操作和不喷射的操作，并且可以在最佳测量条件下测量每个离子，通过参考每个部分的输出电压列表信息，实现能够以高吞吐量和高灵敏度执行MS / MS测量的质量分析器。

10. 发明授权

US07718960B2 Ion mobility spectrometer and ion-mobility-spectrometry/mass-spectrometry hybrid spectrometer 有权
标题翻译：离子迁移光谱仪和离子迁移光谱/质谱混合光谱仪
公开(公告)号：US07718960B2
公开(公告)日：2010-05-18
申请号：US12149737
申请日：2008-05-07
申请人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Yasuaki Takada
发明人： Yuichiro Hashimoto , Hideki Hasegawa , Masuyuki Sugiyama , Yasuaki Takada
IPC分类号： H01J49/10 , H01J49/40
CPC分类号： G01N27/622
摘要： A low-cost and high-ion-transmission-ratio ion-mobility spectrometry filter, including an ion source, a first drift region in which a gas flow direction and a DC electric-field direction are opposite to each other, a second drift region in which a gas flow direction is provided, the gas flow direction being different from the gas flow direction in the first drift region, and being opposite to a DC electric-field application direction in the second drift region, an intermediate region having an electric field for causing ions to travel between the first drift region and the second drift region, and a detector for detecting ions which have passed through the first drift region and the second drift region.
摘要翻译：一种低成本和高离子透射率的离子迁移谱分析滤光器，包括离子源，气流方向和DC电场方向彼此相反的第一漂移区，第二漂移区其中设置有气体流动方向，气体流动方向与第一漂移区域中的气体流动方向不同，并且与第二漂移区域中的直流电场施加方向相反，具有电场的中间区域用于使离子在第一漂移区域和第二漂移区域之间行进;以及检测器，用于检测已经通过第一漂移区域和第二漂移区域的离子。

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