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1. 发明申请

US20140151543A1 ANALYSIS DEVICE AND ANALYSIS METHOD 有权
标题翻译：分析装置和分析方法
公开(公告)号：US20140151543A1
公开(公告)日：2014-06-05
申请号：US13884755
申请日：2011-11-08
申请人： Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
发明人： Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
IPC分类号： H01J49/00 , H01J49/04
CPC分类号： H01J49/0422 , G01N1/2211 , G01N1/2214 , G01N33/0057 , G01N2001/028 , H01J49/00 , H01J49/0036 , H01J49/04 , H01J49/0459 , H01J49/0468 , Y02A50/25
摘要： Provided is a technique of analyzing particles in real time while collecting and condensing the particles continuously. Gas and/or particles as a detection target substance that are attached to an authentication target 2 are removed by air flow from a blowing region 5. The removed sample is sucked and is condensed and sampled at a sampling region 10, and ions of the sample are generated at an ion source 21 and are then subjected to mass analysis at a mass analysis region 23. Determination of the obtained mass spectrum is made as to the presence or not of a mass spectrum derived from the detection target substance, and a monitor 27 displays a result thereof. Thereby, the detection target substance attached to the authentication target 2 can be detected continuously in real time, promptly and with a less error rate.
摘要翻译：提供了一种在连续收集和冷凝颗粒时实时分析颗粒的技术。作为检测对象物质的作为检测对象物质的气体和/或颗粒被从吹扫区域5的空气流除去。将取出的样品抽吸并在采样区域10被冷凝并取样，并且样品的离子在离子源21处产生，然后在质量分析区域23进行质量分析。对获得的质谱进行测定，确定是否存在从检测目标物质得到的质谱，以及监测器27 显示其结果。因此，可以实时，及时且误码率较小的连续检测附着于认证对象2的检测对象物质。

2. 发明申请

US20130056633A1 MASS SPECTROMETER 审中-公开
标题翻译：质谱仪
公开(公告)号：US20130056633A1
公开(公告)日：2013-03-07
申请号：US13667386
申请日：2012-11-02
申请人： Yuichiro HASHIMOTO , Hideki HASEGAWA , Masuyuki SUGIYAMA , Hidetoshi MOROKUMA
发明人： Yuichiro HASHIMOTO , Hideki HASEGAWA , Masuyuki SUGIYAMA , Hidetoshi MOROKUMA
IPC分类号： H01J49/04 , H01J49/36
CPC分类号： H01J49/0422 , H01J49/0013 , H01J49/0495 , H01J49/24
摘要： A mass spectrometer having a resolution improved by introducing ions into a mass spectrometry part with a high efficiency is provided with a small-sized, simple configuration. The mass spectrometer includes an opening/closing mechanism provided between a sample introducing piping part for introducing a sample into the mass spectrometry part and the mass spectrometry part to conduct gas introduction intermittently and control sample passage. The mass spectrometer further includes a pump mechanism to evacuate a high pressure side of the sample introducing piping part, that is, an opposite side of the opening/closing mechanism to the mass spectrometry part to have a pressure in a range of 100 to 10,000 Pa.
摘要翻译：具有小型，简单的结构，提供通过以高效率将离子引入质谱部分而提高分辨率的质谱仪。该质谱仪包括设置在用于将样品引入质谱部分的样品导入管道部分和质谱部分间歇地导入气体引入并控制样品通道的开/关机构。质谱仪还包括泵机构，用于将样品导入管道部分的高压侧排出，即，将质量分析部件的开闭机构的相反侧压力为100〜10000Pa 。

3. 发明申请

US20120223223A1 MASS SPECTROMETER METHOD AND MASS SPECTROMETER 有权
标题翻译：质谱仪和质谱仪
公开(公告)号：US20120223223A1
公开(公告)日：2012-09-06
申请号：US13365355
申请日：2012-02-03
申请人： Masuyuki SUGIYAMA , Yuichiro HASHIMOTO , Hideki HASEGAWA , Shuhei HASHIBA , Shun KUMANO
发明人： Masuyuki SUGIYAMA , Yuichiro HASHIMOTO , Hideki HASEGAWA , Shuhei HASHIBA , Shun KUMANO
IPC分类号： H01J49/26 , H01J49/00
CPC分类号： H01J49/0031 , H01J49/0045
摘要： A variation in an ionization efficiency and the amount of sample which is introduced into an ion trap is corrected and quantified. Ions of an internal standard and ions of a sample are trapped in the ion trap at the same time, and a concentration of the sample is quantified according to an intensity of the ions of the internal standard which are mass-selectively ejected, and an intensity of fragment ions of the sample.
摘要翻译：电离效率的变化和引入离子阱的样品量被校正和量化。将内标的离子和样品的离子同时捕获在离子阱中，并且根据质量选择性地喷射的内标的离子的强度来量化样品的浓度，强度的样品的碎片离子。

4. 发明授权

US07800058B2 Mass spectrometer and mass spectrometry method 有权
标题翻译：质谱仪和质谱法
公开(公告)号：US07800058B2
公开(公告)日：2010-09-21
申请号：US11979811
申请日：2007-11-08
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
IPC分类号： H01J49/00
CPC分类号： H01J49/4225 , H01J49/4215
摘要： A mass spectrometer that is switchable to operate as a linear trap or as a mass filter, and attaining both high ejection efficiency when operated as a linear trap and high mass resolving power when operated as a mass filter. A mass spectrometer includes an ion source for ionizing a sample, a linear trap quadrupole rod lens supplied with ionized ions, a trap electrode for forming a potential to trap the supplied ions between one end of the quadrupole lens and the other end, a control unit to regulate the trap lens voltage, and a mass analyzer or detector to detect ions ejected from the linear trap, and characterized in switching between an operation where the supplied ions are trapped in a section quadrupole rod lens and ejected by the controller unit regulating the trap electrode voltage; and an operation where ions are selective passed through according to their mass. The ejection efficiency when operated as an ion trap, and the mass resolving power when operated as a quadrupole mass filter are vastly improved compared to conventional methods.
摘要翻译：可以切换为线性捕集器或质量过滤器的质谱仪，当作为质量过滤器操作时，作为线性捕集器操作时获得高喷射效率和高质量分辨能力的质谱仪。质谱仪包括用于电离样品的离子源，提供有离子化离子的线性捕获四极杆透镜，用于形成用于捕获四极透镜的一端与另一端之间的供应离子的电位的捕获电极，控制单元调节陷波透镜电压，以及质量分析器或检测器，用于检测从线性阱捕获的离子，并且其特征在于，在所提供的离子被捕获在四极杆棒状透镜中并由调节阱的控制器单元喷射的操作之间进行切换电极电压; 以及根据其质量选择性地通过离子的操作。当作为离子阱操作时的喷射效率以及当作为四极质量过滤器操作时的质量分辨能力与常规方法相比大大提高。

5. 发明申请

US20080121795A1 Mass spectrometer and mass spectrometry method 有权
标题翻译：质谱仪和质谱法
公开(公告)号：US20080121795A1
公开(公告)日：2008-05-29
申请号：US11979811
申请日：2007-11-08
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Hideki Hasegawa , Izumi Waki
IPC分类号： H01J49/42
CPC分类号： H01J49/4225 , H01J49/4215
摘要： A mass spectrometer that is switchable to operate as a linear trap or as a mass filter, and attaining both high ejection efficiency when operated as a linear trap and high mass resolving power when operated as a mass filter. A mass spectrometer includes an ion source for ionizing a sample, a linear trap quadrupole rod lens supplied with ionized ions, a trap electrode for forming a potential to trap the supplied ions between one end of the quadrupole lens and the other end, a control unit to regulate the trap lens voltage, and a mass analyzer or detector to detect ions ejected from the linear trap, and characterized in switching between an operation where the supplied ions are trapped in a section quadrupole rod lens and ejected by the controller unit regulating the trap electrode voltage; and an operation where ions are selective passed through according to their mass. The ejection efficiency when operated as an ion trap, and the mass resolving power when operated as a quadrupole mass filter are vastly improved compared to conventional methods.
摘要翻译：可以切换为线性捕集器或质量过滤器的质谱仪，当作为质量过滤器操作时，作为线性捕集器操作时获得高喷射效率和高质量分辨能力的质谱仪。质谱仪包括用于电离样品的离子源，提供有离子化离子的线性捕获四极杆透镜，用于形成用于捕获四极透镜的一端与另一端之间的供应离子的电位的捕获电极，控制单元调节陷波透镜电压，以及质量分析器或检测器，用于检测从线性阱捕获的离子，并且其特征在于，在所提供的离子被捕获在四极杆棒状透镜中并由调节阱的控制器单元喷射的操作之间进行切换电极电压; 以及根据其质量选择性地通过离子的操作。当作为离子阱操作时的喷射效率以及当作为四极质量过滤器操作时的质量分辨能力与常规方法相比大大提高。

6. 发明授权

US09040905B2 Analysis device and analysis method 有权
公开(公告)号：US09040905B2
公开(公告)日：2015-05-26
申请号：US13884755
申请日：2011-11-08
申请人： Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
发明人： Hisashi Nagano , Yasutaka Suzuki , Hideo Kashima , Yuichiro Hashimoto , Masuyuki Sugiyama , Masakazu Sugaya , Yasunori Doi , Koichi Terada
IPC分类号： H01J49/04 , G01N1/22 , G01N1/02 , H01J49/00 , G01N33/00
CPC分类号： H01J49/0422 , G01N1/2211 , G01N1/2214 , G01N33/0057 , G01N2001/028 , H01J49/00 , H01J49/0036 , H01J49/04 , H01J49/0459 , H01J49/0468 , Y02A50/25
摘要： Provided is a technique of analyzing particles in real time while collecting and condensing the particles continuously. Gas and/or particles as a detection target substance that are attached to an authentication target 2 are removed by air flow from a blowing region 5. The removed sample is sucked and is condensed and sampled at a sampling region 10, and ions of the sample are generated at an ion source 21 and are then subjected to mass analysis at a mass analysis region 23. Determination of the obtained mass spectrum is made as to the presence or not of a mass spectrum derived from the detection target substance, and a monitor 27 displays a result thereof. Thereby, the detection target substance attached to the authentication target 2 can be detected continuously in real time, promptly and with a less error rate.

7. 发明授权

US08710430B2 Mass spectrometry method 有权
标题翻译：质谱法
公开(公告)号：US08710430B2
公开(公告)日：2014-04-29
申请号：US13527619
申请日：2012-06-20
申请人： Masuyuki Sugiyama , Yuichiro Hashimoto , Shun Kumano , Yohei Kawaguchi , Hidetoshi Morokuma
发明人： Masuyuki Sugiyama , Yuichiro Hashimoto , Shun Kumano , Yohei Kawaguchi , Hidetoshi Morokuma
IPC分类号： H01J49/42 , H01J49/26 , H01J49/00
CPC分类号： H01J49/4265 , H01J49/0009 , H01J49/0036
摘要： A mass spectrometry method that corrects the effects from space charge and that achieves both sensitivity and a dynamic range. The mass axis of the mass spectrum is corrected based on the counts of ions accumulated within the ion trap at the point in time each ion was extracted.
摘要翻译：一种校正空间电荷效应并实现灵敏度和动态范围的质谱法。基于在每个离子被提取的时间点内积聚在离子阱内的离子的计数校正质谱的质量轴。

8. 发明申请

US20130334416A1 MASS SPECTROMETER AND ION SOURCE USED THEREFOR 有权
标题翻译：质谱仪及其使用的离子源
公开(公告)号：US20130334416A1
公开(公告)日：2013-12-19
申请号：US14001711
申请日：2012-01-27
申请人： Hiroyuki Satake , Hideki Hasegawa , Masuyuki Sugiyama , Yuichiro Hashimoto
发明人： Hiroyuki Satake , Hideki Hasegawa , Masuyuki Sugiyama , Yuichiro Hashimoto
IPC分类号： H01J49/10
CPC分类号： H01J49/10 , H01J49/0431 , H01J49/165
摘要： The quantitative accuracy of analysis is improved without reducing the dynamic range for measurement of concentrations by performing stable ionization through electrospray or the like which repeats sampling and ionization using a movable probe electrode.A voltage is applied from a high-voltage power source 4 to a sample transport electrode 7 having a plurality of probe electrodes 1 and a driving section 3 drives the sample transport electrode 7 to rotate. The plurality of probe electrodes 1, to which a sample solution 5 is adhered, are sequentially transported to an inlet 21 of a mass spectrometer 20, thus electrospray ionization is continuously performed.
摘要翻译：通过使用可移动探针电极重复取样和电离的电喷雾等进行稳定的电离，可以提高分析的定量精度，而不降低浓度测定的动态范围。从高电压电源4向具有多个探针电极1的检体输送电极7施加电压，驱动部3驱动检体输送电极7旋转。将附着有样品溶液5的多个探针电极1依次输送到质谱仪20的入口21，从而连续进行电喷雾离子化。

9. 发明申请

US20130240726A1 MASS SPECTROMETER 有权
标题翻译：质谱仪
公开(公告)号：US20130240726A1
公开(公告)日：2013-09-19
申请号：US13877717
申请日：2011-10-03
申请人： Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake , Yuichiro Hashimoto
发明人： Hideki Hasegawa , Masuyuki Sugiyama , Hiroyuki Satake , Yuichiro Hashimoto
IPC分类号： H01J49/06
CPC分类号： H01J49/063 , H01J49/005 , H01J49/068 , H01J49/4255
摘要： This mass spectrometer is provided with an ion guide (37) having a multipole rod electrode (1), a power source unit (5) for applying voltage to the multipole rod electrode, and a control unit for controlling the power source unit, said mass spectrometer being characterised by the multipole rod electrode having a rod electrode divided into a plurality of segmented rods (2A-1, 2A-2, 2B-1, 2B-2, 2C-1, 2C-2, 2D-1, 2D-2) at mutually different positions in the axial direction. Thus enabled is low-cost, high-throughput analysis.
摘要翻译：该质谱仪设置有具有多极杆电极（1）的离子引导件（37），用于向多极杆电极施加电压的电源单元（5），以及用于控制电源单元的控制单元，所述质量光谱仪的特征在于多极杆电极具有分为多个分段杆（2A-1,2A-2,2B-1,2B-2,2C-1,2C-2，2D-1，2D- 2）在轴向上相互不同的位置。因此启用了低成本，高通量分析。

10. 发明授权

US08368013B2 Analyzer, ionization apparatus and analyzing method 有权
标题翻译：分析仪，电离装置及分析方法
公开(公告)号：US08368013B2
公开(公告)日：2013-02-05
申请号：US13084930
申请日：2011-04-12
申请人： Masako Ishimaru , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Masuyuki Sugiyama , Hidetoshi Morokuma
发明人： Masako Ishimaru , Yuichiro Hashimoto , Hideki Hasegawa , Masuyoshi Yamada , Masuyuki Sugiyama , Hidetoshi Morokuma
IPC分类号： B01D59/44 , H01J49/00
CPC分类号： H01J49/145
摘要： An analyzer performs dielectric barrier discharge and ionization of a sample by a reaction between the sample and excited molecules or ions generated by the dielectric barrier discharge at a pressure lower than an atmospheric pressure.
摘要翻译：分析仪通过在低于大气压的压力下通过介电阻挡放电产生的样品和激发的分子或离子之间的反应来进行介电阻挡放电和样品的离子化。

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