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1. 发明授权

US06797828B1 Processes for the preparation of 4(5)-amino-5(4)-carboxamidoimidazoles and intermediates thereof 有权
标题翻译：制备4（5） - 氨基-5（4） - 羧酰氨基咪唑的方法及其中间体
公开(公告)号：US06797828B1
公开(公告)日：2004-09-28
申请号：US10088425
申请日：2002-03-15
申请人： Hiroaki Shibasaki , Fumihiko Nagasaki , Mitsuru Takase , Satoru Yamazaki , Yutaka Ishii , Kimihiko Oohata
发明人： Hiroaki Shibasaki , Fumihiko Nagasaki , Mitsuru Takase , Satoru Yamazaki , Yutaka Ishii , Kimihiko Oohata
IPC分类号： C07D23370
CPC分类号： C07C257/14 , C07D233/90
摘要： The invention provides novel processes for preparing efficiently compounds of general formula (1) (wherein R1 and R2 are each independently hydrogen, optionally substituted C1-C10 alkyl, C3-C14 hydrocarbyl bearing alicyclic skeleton, or the like) and initermediates thereof. Compounds of general formula (I) can be prepared by subjecting compounds of general formula (II) and/or salts thereof to cyclization hydrolysis in an aqueous basic solution. Further, compounds of general formula (II) can be prepared from industrially easily available diaminomaleonitrile in a high yield.
摘要翻译：本发明提供有效制备通式（1）化合物（其中R 1和R 2各自独立地为氢，任选取代的C 1 -C 10烷基，C 3 -C 14烃基带有脂环骨架等）的化合物及其初始化物的新方法。通式（I）的化合物可以通过使通式（II）的化合物和/或其盐在碱性水溶液中进行环化水解来制备。此外，通式（II）的化合物可以从工业上容易获得的二氨基马来腈以高产率制备。

2. 发明授权

US08829139B2 Process for production of polysilane compound 有权
标题翻译：生产聚硅烷化合物的方法
公开(公告)号：US08829139B2
公开(公告)日：2014-09-09
申请号：US12992775
申请日：2009-05-15
申请人： Kimihiko Oohata , Satoru Yamazaki , Masamichi Yasuhara , Jyunichi Kawachi
发明人： Kimihiko Oohata , Satoru Yamazaki , Masamichi Yasuhara , Jyunichi Kawachi
IPC分类号： C08G77/08 , C08G77/60 , C08G77/34
CPC分类号： C08G77/60 , C08G77/08 , C08G77/34
摘要： A method for easily producing high-purity polydimethylsilane or polydiphenylsilane, where by-products such as alkali metal salt and alkaline earth metal salt can be efficiently removed, is provided. Dimethyldichlorosilane or diphenyldichlorosilane is reacted with an alkali metal such as metal sodium and metal magnesium and/or an alkaline earth metal in an organic solvent such as toluene to obtain crude polydimethylsilane or crude polydiphenylsilane, methanol having dissolved therein an ether ester-type nonionic surfactant or a surfactant such as alkylbenzenesulfonate is added to the crude polydimethylsilane or the crude polydiphenylsilane to deactivate the remaining alkali metal and alkaline earth metal, and the crude polydimethylsilane or the crude polydiphenylsilane is washed with water in the presence of a surfactant to efficiently remove an alkali metal salt, an alkaline earth metal salt and the like, whereby high-purity polydimethylsilane or polydiphenylsilane is obtained.
摘要翻译：提供容易生产高纯度聚二甲基硅烷或聚二苯基硅烷的方法，其中可以有效地除去碱金属盐和碱土金属盐等副产物。二甲基二氯硅烷或二苯基二氯硅烷与有机溶剂如甲苯中的金属钠和金属镁和/或碱土金属的碱金属反应，得到粗的聚二甲基硅烷或粗的聚二苯基硅烷，其中溶解有醚酯型非离子表面活性剂的甲醇或将烷基苯磺酸盐等表面活性剂加入到粗聚二甲基硅烷或粗聚二苯基硅烷中，使剩余的碱金属和碱土金属失活，粗面聚二甲基硅烷或粗聚二苯基硅烷在表面活性剂存在下用水洗涤，有效地除去碱金属盐，碱土金属盐等，得到高纯度聚二甲基硅烷或聚二苯基硅烷。

3. 发明申请

US20110071269A1 PROCESS FOR PRODUCTION OF POLYSILANE COMPOUND 有权
标题翻译：制备多晶体化合物的方法
公开(公告)号：US20110071269A1
公开(公告)日：2011-03-24
申请号：US12992775
申请日：2009-05-15
申请人： Kimihiko Oohata , Satoru Yamazaki , Masamichi Yasuhara , Jyunichi Kawachi
发明人： Kimihiko Oohata , Satoru Yamazaki , Masamichi Yasuhara , Jyunichi Kawachi
IPC分类号： C08G77/12
CPC分类号： C08G77/60 , C08G77/08 , C08G77/34
摘要： A method for easily producing high-purity polydimethylsilane or polydiphenylsilane, where by-products such as alkali metal salt and alkaline earth metal salt can be efficiently removed, is provided. Dimethyldichlorosilane or diphenyldichlorosilane is reacted with an alkali metal such as metal sodium and metal magnesium and/or an alkaline earth metal in an organic solvent such as toluene to obtain crude polydimethylsilane or crude polydiphenylsilane, methanol having dissolved therein an ether ester-type nonionic surfactant or a surfactant such as alkylbenzenesulfonate is added to the crude polydimethylsilane or the crude polydiphenylsilane to deactivate the remaining alkali metal and alkaline earth metal, and the crude polydimethylsilane or the crude polydiphenylsilane is washed with water in the presence of a surfactant to efficiently remove an alkali metal salt, an alkaline earth metal salt and the like, whereby high-purity polydimethylsilane or polydiphenylsilane is obtained.
摘要翻译：提供容易生产高纯度聚二甲基硅烷或聚二苯基硅烷的方法，其中可以有效地除去碱金属盐和碱土金属盐等副产物。二甲基二氯硅烷或二苯基二氯硅烷与有机溶剂如甲苯中的金属钠和金属镁和/或碱土金属的碱金属反应，得到粗的聚二甲基硅烷或粗的聚二苯基硅烷，其中溶解有醚酯型非离子表面活性剂的甲醇或将烷基苯磺酸盐等表面活性剂加入到粗聚二甲基硅烷或粗聚二苯基硅烷中，使剩余的碱金属和碱土金属失活，粗面聚二甲基硅烷或粗聚二苯基硅烷在表面活性剂存在下用水洗涤，有效地除去碱金属盐，碱土金属盐等，得到高纯度聚二甲基硅烷或聚二苯基硅烷。

4. 发明申请

US20120016149A1 PROCESS FOR PRODUCTION OF CYCLIC SILANE COMPOUND AND/OR CYCLIC CARBOSILANE COMPOUND 有权
标题翻译：生产环状硅烷化合物和/或环状碳酸酯化合物的方法
公开(公告)号：US20120016149A1
公开(公告)日：2012-01-19
申请号：US13259554
申请日：2010-04-09
申请人： Satoru Yamazaki , Kimihiko Oohata , Minoru Okada , Masamichi Yasuhara , Hideki Maekawa , Hiroyuki Yamanaka
发明人： Satoru Yamazaki , Kimihiko Oohata , Minoru Okada , Masamichi Yasuhara , Hideki Maekawa , Hiroyuki Yamanaka
IPC分类号： C07F7/08 , C07F7/02
CPC分类号： C07F7/0896 , C07F7/0803 , C07F7/0807 , C07F7/21
摘要： The present invention relates to: a process for producing a cyclic silane compound, which comprises subjecting a chained polysilane to pyrolysis in the presence of an oxide of a transition metal belonging to Group 8 or Group 11 of the periodic table; and a process for producing a cyclic carbosilane compound, which comprises subjecting a chained polysilane to pyrolysis in the presence of a simple substance of a metal selected from the group consisting of transition metal elements and elements belonging to Groups 12 to 15 of the periodic table or a compound thereof.
摘要翻译：本发明涉及一种环状硅烷化合物的制备方法，其包括使链状聚硅烷在属于周期表第8族或第11族的过渡金属的氧化物存在下进行热解; 以及环状碳硅烷化合物的制造方法，其特征在于，在选自过渡金属元素和元素周期表第12〜15族的元素的金属的单质的存在下，使链状聚硅烷进行热解，或其化合物。

5. 发明授权

US08669390B2 Process for production of cyclic silane compound and/or cyclic carbosilane compound 有权
标题翻译：环状硅烷化合物和/或环状碳硅烷化合物的制造方法
公开(公告)号：US08669390B2
公开(公告)日：2014-03-11
申请号：US13259554
申请日：2010-04-09
申请人： Satoru Yamazaki , Kimihiko Oohata , Minoru Okada , Masamichi Yasuhara
发明人： Satoru Yamazaki , Kimihiko Oohata , Minoru Okada , Masamichi Yasuhara
IPC分类号： C07F7/21
CPC分类号： C07F7/0896 , C07F7/0803 , C07F7/0807 , C07F7/21
摘要： The present invention relates to: a process for producing a cyclic silane compound, which comprises subjecting a chained polysilane to pyrolysis in the presence of an oxide of a transition metal belonging to Group 8 or Group 11 of the periodic table; and a process for producing a cyclic carbosilane compound, which comprises subjecting a chained polysilane to pyrolysis in the presence of a simple substance of a metal selected from the group consisting of transition metal elements and elements belonging to Groups 12 to 15 of the periodic table or a compound thereof.
摘要翻译：本发明涉及一种环状硅烷化合物的制备方法，其包括使链状聚硅烷在属于周期表第8族或第11族的过渡金属的氧化物存在下进行热解; 以及环状碳硅烷化合物的制造方法，其特征在于，在选自过渡金属元素和元素周期表第12〜15族的元素的金属的单质的存在下，使链状聚硅烷进行热解，或其化合物。

6. 发明申请

US20060287527A1 Process for producing acrylic acid derivative 审中-公开
标题翻译：制备丙烯酸衍生物的方法
公开(公告)号：US20060287527A1
公开(公告)日：2006-12-21
申请号：US11446448
申请日：2006-06-01
申请人： Yasuyuki Miyazawa , Takahiro Sagae , Yutaka Ishii , Hiroyuki Yazaki , Makoto Funabora , Satoru Yamazaki
发明人： Yasuyuki Miyazawa , Takahiro Sagae , Yutaka Ishii , Hiroyuki Yazaki , Makoto Funabora , Satoru Yamazaki
IPC分类号： C07D239/34
CPC分类号： C07D239/56 , C07C67/31 , C07C67/343 , C07D239/34 , C07D239/52 , C07C69/734 , C07C69/732
摘要： Processes for producing a compound represented by the formula (1), which includes an acrylic acid derivative and is useful as an agricultural chemical or medicine. One of the processes comprises the step of formulating a compound (3) and converting the OH of the resultant compound (2) into OR″. The first step comprises reacting a formic or orthoformic ester in the presence of a Lewis acid and a base. The second step comprises reacting the compound with R″OH or with R″OH and CH(OR″)3 under acidic conditions or using a phase-transfer catalyst in a two-phase system and regulating the base and the concentration thereof to stereoselectively synthesize the target compound. In another, process, the compound is efficiently produced without isolating the compound. The compound can also be produced without the compound (2).
摘要翻译：制备由式（1）表示的化合物的方法，其包括丙烯酸衍生物并且可用作农业化学品或药物。其中一个方法包括配制化合物（3）并将所得化合物（2）的OH转化为OR“的步骤。第一步包括在路易斯酸和碱的存在下使甲酸或正癸酸酯反应。第二步包括在酸性条件下或在两相体系中使用相转移催化剂使化合物与R''OH或与R''OH和CH（OR“）3'反应，调节碱和其浓度以立体选择性合成目标化合物。在另一个方法中，化合物在不分离化合物的情况下有效生产。化合物也可以不用化合物（2）制备。

7. 外观设计

USD627983S1 Chair 有权
公开(公告)号：USD627983S1
公开(公告)日：2010-11-30
申请号：US29347239
申请日：2009-11-09
申请人： Kouichi Wakasugi , Satoru Yamazaki , Yasuaki Chiba , Motomi Kawakami
设计人： Kouichi Wakasugi , Satoru Yamazaki , Yasuaki Chiba , Motomi Kawakami

8. 发明授权

US6137111A Charged particle-beam exposure device and charged-particle-beam exposure method 失效
标题翻译：带电粒子束曝光装置和带电粒子束曝光方法
公开(公告)号：US6137111A
公开(公告)日：2000-10-24
申请号：US84952
申请日：1998-05-28
申请人： Akio Yamada , Satoru Sagou , Hitoshi Watanabe , Satoru Yamazaki , Kiichi Sakamoto , Manabu Ohno , Kenichi Kawakami , Katsuhiko Kobayashi
发明人： Akio Yamada , Satoru Sagou , Hitoshi Watanabe , Satoru Yamazaki , Kiichi Sakamoto , Manabu Ohno , Kenichi Kawakami , Katsuhiko Kobayashi
IPC分类号： G03F1/00 , G03F1/20 , H01J37/304 , H01J37/317 , G03F9/00 , H01J37/00
CPC分类号： B82Y10/00 , B82Y40/00 , G03F1/86 , H01J37/3045 , H01J37/3174 , G03F1/20 , H01J2237/2817 , H01J2237/31794
摘要： A method of detecting deficiency of an aperture used in a charged-particle-beam exposure process employing at least two exposure columns is disclosed, where each of the two exposure columns passes a charged-particle beam through the aperture formed through a mask to shape a cross section of the charged-particle beam before exposing the charged-particle beam onto an object. The method includes the steps of mounting masks having the same aperture to the at least two exposure columns; scanning, in each of the at least two exposure columns, the charged-particle beam over an area containing a mark on a surface substantially at the same height as the object after passing the charged-particle beam through the same aperture; obtaining, in each of the at least two exposure columns, a signal waveform corresponding to the scan by detecting charged particles scattered by the mark; and comparing the signal waveform between the at least two exposure columns.
摘要翻译：公开了一种检测在使用至少两个曝光柱的带电粒子束曝光工艺中使用的孔的缺陷的方法，其中两个曝光柱中的每一个通过带电粒子束穿过通过掩模形成的孔以形成在将带电粒子束暴露在物体上之前的带电粒子束的横截面。该方法包括以下步骤：将具有相同孔径的掩模安装到至少两个曝光柱; 在所述至少两个曝光柱中的每一个中，在将带电粒子束通过相同的孔之后，将包含在与物体基本上处于相同高度的表面上的标记的区域上的带电粒子束扫描; 在所述至少两个曝光列中的每一个中，通过检测由所述标记散射的带电粒子来获得对应于所述扫描的信号波形; 以及比较所述至少两个曝光列之间的信号波形。

9. 发明授权

US5248748A Diacetylene compound having double bond and shaped article thereof 失效
标题翻译：具有双键的乙炔化合物及其成型制品
公开(公告)号：US5248748A
公开(公告)日：1993-09-28
申请号：US630225
申请日：1990-12-19
申请人： Katsuyuki Nakamura , Satoru Yamazaki , Jinichiro Kato , Kensaku Tokushige
发明人： Katsuyuki Nakamura , Satoru Yamazaki , Jinichiro Kato , Kensaku Tokushige
IPC分类号： A61K8/43 , A61K8/73 , A61Q11/00 , C07C69/007 , C07C69/017 , C07C211/23 , C07C211/28 , C07C211/50 , C07C233/09 , C07C233/11 , C07C233/38 , C07C233/39 , C07C233/40 , C07C233/58 , C07C233/62 , C07C271/28 , C07C271/58 , C07D209/76 , C08F38/00
CPC分类号： C08F38/00 , A61K8/43 , A61K8/731 , A61Q11/00 , C07C211/23 , C07C211/28 , C07C211/50 , C07C233/09 , C07C233/11 , C07C233/38 , C07C233/39 , C07C233/40 , C07C233/58 , C07C233/62 , C07C271/28 , C07C271/58 , C07C69/007 , C07C69/017 , C07D209/76
摘要： Disclosed is a diacetylene compound comprising, as structural units, (a) at least one member selected from diacetylene group-containing organic groups of the formulae (I) and (II):R.sup.I --C.tbd.C--C.tbd.C--R.sup.II -- (I)and--R.sup.III --C.tbd.C--C.tbd.C--R.sup.IV -- (II)wherein R.sup.I is hydrogen or a (C1-16) monovalent organic group, and R.sup.II, R.sup.III and R.sup.IV are a (C1-13) divalent organic group,(b) at least one organic group having at least one carbon-to-carbon double bond, and (c) at least one connecting group connecting the units (a) and (b) , which connecting group is selected from amide, imide, ester, ether, amino, imino, urethane, sulfonyl and carbonyl bonds. A cured shaped article made of this compound exhibits isotropically a high elastic modulus and has excellent mechanical properties.
摘要翻译：公开了包含作为结构单元的（a）至少一种选自式（I）和（II）的含二炔基的有机基团的组分的联乙炔化合物：RI-C 3BOND CC 3BOND C-RII-（I）和RIII-C 3BOND CC 3BOND C-RIV-（II）其中RI是氢或（C1-16）一价有机基团，RII，RIII和RIV是（C1-13）二价有机基团，（b）至少一个具有至少一个碳 - 碳双键的有机基团，和（c）连接单元（a）和（b）的至少一个连接基团，该连接基团选自酰胺，酰亚胺，酯，醚，氨基，亚氨基，氨基甲酸酯，磺酰基和羰基键。由该化合物制成的固化成型制品各向同性地表现出高的弹性模量并且具有优异的机械性能。

10. 发明授权

US5175307A Diacetylene compound having double bond and shaped article thereof 失效
标题翻译：具有双键的乙炔化合物及其成型制品
公开(公告)号：US5175307A
公开(公告)日：1992-12-29
申请号：US618997
申请日：1990-11-28
申请人： Katsuyuki Nakamura , Satoru Yamazaki , Jinichiro Kato , Kensaku Tokushige
发明人： Katsuyuki Nakamura , Satoru Yamazaki , Jinichiro Kato , Kensaku Tokushige
IPC分类号： A61K8/43 , A61K8/73 , A61Q11/00 , C07C69/007 , C07C69/017 , C07C211/23 , C07C211/28 , C07C211/50 , C07C233/09 , C07C233/11 , C07C233/38 , C07C233/39 , C07C233/40 , C07C233/58 , C07C233/62 , C07C271/28 , C07C271/58 , C07D209/76 , C08F38/00
CPC分类号： C08F38/00 , A61K8/43 , A61K8/731 , A61Q11/00 , C07C211/23 , C07C211/28 , C07C211/50 , C07C233/09 , C07C233/11 , C07C233/38 , C07C233/39 , C07C233/40 , C07C233/58 , C07C233/62 , C07C271/28 , C07C271/58 , C07C69/007 , C07C69/017 , C07D209/76
摘要： Disclosed is a diacetylene compound comprising, as structural units,(a) at least one member selected from diacetylene group-containing organic groups of the formulae (I) and (II):R.sup.I --C.tbd.C--C.tbd.C--R.sup.II -- (I)and--R.sup.III --C.tbd.C--C.tbd.C--R.sup.IV -- (II) wherein R.sup.I is hydrogen or a (Cl-16) monovalent organic group, and R.sup.II, R.sup.III and R.sup.IV are a (C1-13) divalent organic group,(b) at least one organic group having at least one carbon-to-carbon double bond, and (c) at least one connecting group connecting the units (a) and (b), which connecting group is selected from amide, imide, ester, ether, amino, imino, urethane, sulfonyl and carbonyl bonds. A cured shaped article made of this compound exhibits isotropically a high elastic modulus and has excellent mechanical properties.
摘要翻译：公开了包含作为结构单元的（a）至少一种选自式（I）和（II）的含二炔基的有机基团的组分的联乙炔化合物：RI-C 3BOND CC 3BOND C-RII-（I）（II）其中RI是氢或（C1-16）一价有机基团，RII，RIII和RIV是（C1-13）二价有机基团，（b）至少一个具有至少一个碳 - 碳双键的有机基团，和（c）连接单元（a）和（b）的至少一个连接基团，该连接基团选自酰胺，酰亚胺，酯，醚，氨基，亚氨基，氨基甲酸酯，磺酰基和羰基键。由该化合物制成的固化成型制品各向同性地表现出高的弹性模量并且具有优异的机械性能。

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