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1. 发明申请

US20090171107A1 PROCESS FOR PREPARING POROUS METAL ORGANIC FRAMEWORKS 有权
标题翻译：制备多孔金属有机框架的方法
公开(公告)号：US20090171107A1
公开(公告)日：2009-07-02
申请号：US12300902
申请日：2007-05-11
申请人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
发明人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
IPC分类号： C07F1/08
CPC分类号： C25B3/12
摘要： The present invention relates to a process for preparing a porous metal organic framework comprising at least two organic compounds coordinated to at least one metal ion, which comprises the steps (a) oxidation of at least one anode comprising the metal corresponding to at least one metal ion in a reaction medium in the presence of at least one first organic compound which is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbons have been replaced by heteroatoms selected from the group consisting of N, O and S to form a reaction intermediate comprising the at least one metal ion and the first organic compound; and (b) reaction of the reaction intermediate at a prescribed temperature with at least one second organic compound which coordinates to the at least one metal ion, with the second organic compound being derived from a dicarboxylic, tricarboxylic or tetracarboxylic acid.
摘要翻译：本发明涉及一种制备多孔金属有机骨架的方法，所述多孔金属有机骨架包括与至少一种金属离子配位的至少两种有机化合物，其包括以下步骤：（a）至少一个阳极的氧化，所述至少一个阳极包含对应于至少一种金属在至少一种第一有机化合物存在下的反应介质中，所述第一有机化合物是任选取代的单环，双环或多环饱和或不饱和烃，其中至少两个环碳已经被选自N，O 和S形成包含所述至少一种金属离子和所述第一有机化合物的反应中间体; 和（b）将反应中间体在规定温度下与至少一种与至少一种金属离子配位的第二有机化合物反应，第二有机化合物衍生自二羧酸，三羧酸或四羧酸。

2. 发明授权

US07879221B2 Process for preparing porous metal organic frameworks 有权
标题翻译：制备多孔金属有机骨架的方法
公开(公告)号：US07879221B2
公开(公告)日：2011-02-01
申请号：US12300902
申请日：2007-05-11
申请人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
发明人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
IPC分类号： C25B3/12 , C07F15/00 , C07F3/00
CPC分类号： C25B3/12
摘要： The present invention relates to a process for preparing a porous metal organic framework comprising at least two organic compounds coordinated to at least one metal ion, which comprises the steps (a) oxidation of at least one anode comprising the metal corresponding to at least one metal ion in a reaction medium in the presence of at least one first organic compound which is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbons have been replaced by heteroatoms selected from the group consisting of N, O and S to form a reaction intermediate comprising the at least one metal ion and the first organic compound; and (b) reaction of the reaction intermediate at a prescribed temperature with at least one second organic compound which coordinates to the at least one metal ion, with the second organic compound being derived from a dicarboxylic, tricarboxylic or tetracarboxylic acid.
摘要翻译：本发明涉及一种制备多孔金属有机骨架的方法，所述多孔金属有机骨架包括与至少一种金属离子配位的至少两种有机化合物，其包括以下步骤：（a）至少一个阳极的氧化，所述至少一个阳极包含对应于至少一种金属在至少一种第一有机化合物存在下的反应介质中，所述第一有机化合物是任选取代的单环，双环或多环饱和或不饱和烃，其中至少两个环碳已经被选自N，O 和S形成包含所述至少一种金属离子和所述第一有机化合物的反应中间体; 和（b）将反应中间体在规定温度下与至少一种与至少一种金属离子配位的第二有机化合物反应，第二有机化合物衍生自二羧酸，三羧酸或四羧酸。

3. 发明申请

US20110110847A1 MAGNESIUM BUTYLISOPHTHALATE AS POROUS METAL ORGANIC FRAMEWORK 审中-公开
标题翻译：作为多孔金属有机骨架的镁合金
公开(公告)号：US20110110847A1
公开(公告)日：2011-05-12
申请号：US13006581
申请日：2011-01-14
申请人： Natalia TRUKHAN , Ulrich Müller , Markus Schubert
发明人： Natalia TRUKHAN , Ulrich Müller , Markus Schubert
IPC分类号： B01D53/02 , C01B5/00
CPC分类号： B01J31/1691 , B01D53/02 , B01D2253/204 , B01J20/226 , B01J2531/22 , C01B3/0015 , C01B6/003 , C01B7/00 , C01B13/0281 , C01B21/0455 , C01B23/0057 , C07C63/24 , C07F3/003 , F17C11/005 , Y02C10/08 , Y02E60/328
摘要： A method for storing, separating or controlled releasing of at least one substance, by up taking the at least one substance by a porous metal organic framework material formed by Mg2+ ions to which 5-tert-buthylisophthalate ions are coordinated to form a framework structure.
摘要翻译：一种用于储存，分离或控制释放至少一种物质的方法，通过将由Mg2 +离子形成的多孔金属有机骨架材料取代至少一种物质，其中5-叔丁基间苯二甲酸酯离子被配位以形成骨架结构。

4. 发明申请

US20090305040A1 METAL OXIDES FROM METAL-ORGANIC FRAMEWORK MATERIALS 失效
标题翻译：金属有机骨架材料的金属氧化物
公开(公告)号：US20090305040A1
公开(公告)日：2009-12-10
申请号：US12297298
申请日：2007-04-12
申请人： Markus Schubert , Ulrich Müller , Natalia Trukhan
发明人： Markus Schubert , Ulrich Müller , Natalia Trukhan
IPC分类号： C01F7/30 , C01F5/06 , C01G25/02
CPC分类号： B01J20/0211 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/28042 , B01J20/28057 , C01F5/02 , C01F7/30 , C01G1/02 , C01G9/02 , C01G23/047 , C01G25/00 , C01G25/02 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C01P2006/13 , C07C51/418 , Y10T428/2982 , C07C63/38 , C07C63/26 , C07C57/15
摘要： The present invention relates to a method for producing a metal oxide by heating a porous metal-organic framework material, the framework material comprising at least one at least bidentate organic compound bound to at least one metal ion by coordination, and the metal ion being selected from the metals comprising groups to 4 and 13 of the Periodic Table of the Elements, above the complete decomposition temperature of the framework material, and also to metal oxides obtainable by this method, and to the use thereof.
摘要翻译：本发明涉及通过加热多孔金属 - 有机骨架材料来生产金属氧化物的方法，所述骨架材料包含至少一种至少二齿有机化合物，其通过配位与至少一种金属离子结合，并且选择金属离子从元素周期表中的4至13的金属组成，高于骨架材料的完全分解温度，以及可通过该方法获得的金属氧化物及其用途。

5. 发明授权

US08501150B2 Metal oxides from metal-organic framework materials 失效
标题翻译：金属 - 有机骨架材料的金属氧化物
公开(公告)号：US08501150B2
公开(公告)日：2013-08-06
申请号：US12297298
申请日：2007-04-12
申请人： Markus Schubert , Ulrich Müller , Natalia Trukhan
发明人： Markus Schubert , Ulrich Müller , Natalia Trukhan
IPC分类号： C01F7/02 , C01B13/14
CPC分类号： B01J20/0211 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/28042 , B01J20/28057 , C01F5/02 , C01F7/30 , C01G1/02 , C01G9/02 , C01G23/047 , C01G25/00 , C01G25/02 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C01P2006/13 , C07C51/418 , Y10T428/2982 , C07C63/38 , C07C63/26 , C07C57/15
摘要： The present invention relates to a method for producing a metal oxide by heating a porous metal-organic framework material, the framework material comprising at least one at least bidentate organic compound bound to at least one metal ion by coordination, and the metal ion being selected from the metals comprising groups 2 to 4 and 13 of the Periodic Table of the Elements, above the complete decomposition temperature of the framework material, and also to metal oxides obtainable by this method, and to the use thereof.
摘要翻译：本发明涉及通过加热多孔金属 - 有机骨架材料来生产金属氧化物的方法，所述骨架材料包含至少一种至少二齿有机化合物，其通过配位与至少一种金属离子结合，并且选择金属离子包括元素周期表第2至4和13族的金属，高于骨架材料的完全分解温度，以及可通过该方法获得的金属氧化物及其用途。

6. 发明申请

US20110105776A1 METHOD FOR ELECTROCHEMICAL PRODUCTION OF A CRYSTALLINE POROUS METAL ORGANIC SKELETON MATERIAL 有权
标题翻译：电铸多孔金属有机硅材料的电化学生产方法
公开(公告)号：US20110105776A1
公开(公告)日：2011-05-05
申请号：US12987548
申请日：2011-01-10
申请人： Ulrich Müller , Hermann Pütter , Michael Hesse , Markus Schubert , Helge Wessel , Jürgen Huff , Marcus Guzmann
发明人： Ulrich Müller , Hermann Pütter , Michael Hesse , Markus Schubert , Helge Wessel , Jürgen Huff , Marcus Guzmann
IPC分类号： C07F1/08 , C07F3/06 , C07F15/06 , C07C229/34 , C07F3/02 , C25B3/12
CPC分类号： C25B3/12 , B01D53/02 , B01D2253/204 , B01J20/226 , B01J20/28014 , B01J20/28042 , B01J31/1691 , B01J31/1805 , B01J31/1815 , B01J31/2239 , B01J31/226 , B01J2531/16 , B01J2531/26 , B01J2531/842 , C01B3/0015 , C01B21/0455 , C01B23/0057 , F17C11/005 , H01M8/04216 , Y02C10/08 , Y02E60/327 , Y02E60/328 , Y02P20/133 , Y02P70/56 , Y10S95/90 , Y10S502/526
摘要： A method of electrochemically preparing a crystalline, porous, metal-organic framework material comprising at least one at least bidentate organic compound coordinately bound to at least one metal ion, in a reaction medium comprising the at least one bidentate organic compound, wherein at least one metal ion is provided in the reaction medium by the oxidation of one anode comprising the corresponding metal.
摘要翻译：一种在包含至少一种二齿有机化合物的反应介质中电化学制备结晶多孔的金属 - 有机骨架材料的方法，其包含与至少一种金属离子配位结合的至少二齿有机化合物，其中至少一种金属离子通过包含相应金属的一个阳极的氧化在反应介质中提供。

7. 发明申请

US20090183996A1 POROUS METAL ORGANIC FRAMEWORK BASED ON PYRROLES AND PYRIDINONES 审中-公开
标题翻译：基于PYRROLES和PYRIDINONES的多孔金属有机框架
公开(公告)号：US20090183996A1
公开(公告)日：2009-07-23
申请号：US12300942
申请日：2007-05-11
申请人： Ingo Richter , Markus Schubert , Ulrich Müller
发明人： Ingo Richter , Markus Schubert , Ulrich Müller
IPC分类号： C25B3/02
CPC分类号： C07D233/54 , B01J20/226 , C07D235/22 , C25B3/12
摘要： Processes comprising: (i) providing an anode comprising zinc; and (ii) oxidizing the anode in a reaction medium in the presence of at least one organic compound to form a porous metal organic framework comprising the least one organic compound coordinated to at least one zinc ion; wherein the at least one organic compound comprises a ring system selected from the group consisting of compounds corresponding to the following structures wherein the ring system optionally bears one or more substituents selected independently from the group consisting of halogens, C1-6-alkyls, phenyl, NH2, NH(C1-6-alkyls), N(C1-6-alkyls)2, OH, O-phenyl and O—C1-6-alkyls, and wherein each C1-6-alkyl and phenyl substituent may independently and optionally bear one or more substituents selected independently from the group consisting of halogens, NH2, NH(C1-6-alkyls), N(C1-6-alkyls)2, OH, O-phenyl and O—C1-6-alkyls.
摘要翻译：方法包括：（i）提供包含锌的阳极; 和（ii）在至少一种有机化合物的存在下在反应介质中氧化阳极以形成包含与至少一种锌离子配位的至少一种有机化合物的多孔金属有机骨架; 其中所述至少一种有机化合物包括选自对应于以下结构的化合物的环系统，其中所述环系统任选地带有一个或多个独立地选自卤素，C 1-6 - 烷基，苯基， NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，O-苯基和O-C 1-6 - 烷基，其中每个C 1-6 - 烷基和苯基取代基可以独立地和任选地含有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，O-苯基和O-C 1-6 - 烷基的取代基。

8. 发明授权

US09688700B2 Metal-organic frameworks based on on 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid 有权
公开(公告)号：US09688700B2
公开(公告)日：2017-06-27
申请号：US13512637
申请日：2010-11-25
申请人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
发明人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
IPC分类号： C07F1/00 , C07F15/02 , C07F5/06 , C07F3/00
CPC分类号： C07F1/005 , C07F3/003 , C07F5/069 , C07F15/025
摘要： The present invention relates to porous metallic frameworks comprising at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the at least one at least bidentate organic compound is derived from 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid. The present invention further relates to shaped bodies comprising these frameworks, processes for producing them and their use, in particular for the storage and separation of gases.

9. 发明申请

US20120251438A1 Metal-Organic Frameworks Based on On 2,5-Furandicarboxylic Acid Or 2,5-Thiophenedicarboxylic Acid 有权
标题翻译：基于2,5-呋喃二羧酸或2,5-噻吩二羧酸的金属有机骨架
公开(公告)号：US20120251438A1
公开(公告)日：2012-10-04
申请号：US13512637
申请日：2010-11-25
申请人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
发明人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
IPC分类号： C07F5/06 , C07F3/06 , C01B3/56 , C07F3/02
CPC分类号： C07F1/005 , C07F3/003 , C07F5/069 , C07F15/025
摘要： The present invention relates to porous metallic frameworks comprising at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the at least one at least bidentate organic compound is derived from 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid. The present invention further relates to shaped bodies comprising these frameworks, processes for producing them and their use, in particular for the storage and separation of gases.
摘要翻译：本发明涉及包含与至少一种金属离子配位的至少一种至少二齿有机化合物的多孔金属骨架，其中所述至少一种至少二齿有机化合物衍生自2,5-呋喃二甲酸或2,5-噻吩二羧酸酸。本发明还涉及包括这些框架的成形体，其制造方法及其用途，特别是用于气体的储存和分离。

10. 发明申请

US20120070353A1 Process For Separating Off Acidic Gases By Means Of Metal-Organic Frameworks Impregnated With Amines 审中-公开
标题翻译：通过用胺浸渍的金属有机骨架分离酸性气体的方法
公开(公告)号：US20120070353A1
公开(公告)日：2012-03-22
申请号：US13257830
申请日：2010-03-18
申请人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
发明人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
IPC分类号： B01D53/40 , C09K3/00 , B01D53/56 , B01D53/52 , B01D53/62 , B01D53/50
CPC分类号： C10L3/10 , B01D53/025 , B01D53/40 , B01D53/62 , B01D2252/2023 , B01D2252/20405 , B01D2252/2041 , B01D2252/20421 , B01D2252/20426 , B01D2252/20431 , B01D2252/20436 , B01D2252/20484 , B01D2253/204 , B01D2253/25 , B01D2256/16 , B01D2256/24 , B01D2257/302 , B01D2257/304 , B01D2257/404 , B01D2257/504 , B01D2258/05 , B01D2258/06 , B01J20/226 , B01J20/2803 , B01J20/28042 , B01J20/28057 , B01J20/3007 , B01J20/3206 , B01J20/3248 , B01J20/3255 , C07F1/005 , C07F3/003 , C07F5/003 , C07F15/025 , C07F15/045 , C07F15/065 , C10L3/102 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a process for separating off at least one acidic gas from a gas mixture comprising at least one acidic gas, which comprises the step of contacting of the gas mixture with a porous metal-organic framework, where the framework adsorbs the at least one acidic gas and the framework comprises at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the porous metal-organic framework is impregnated with an amine suitable for a gas scrub. The invention further provides such impregnated metal-organic frameworks.
摘要翻译：本发明涉及一种从包含至少一种酸性气体的气体混合物中分离出至少一种酸性气体的方法，该方法包括使气体混合物与多孔金属 - 有机骨架接触的步骤，其中框架吸附在至少一种酸性气体和骨架包含与至少一种金属离子配位的至少一种至少二齿的有机化合物，其中多孔金属 - 有机骨架用适于气体洗涤的胺浸渍。本发明还提供了这种浸渍的金属 - 有机骨架。

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