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1. 发明申请

US20090171107A1 PROCESS FOR PREPARING POROUS METAL ORGANIC FRAMEWORKS 有权
标题翻译：制备多孔金属有机框架的方法
公开(公告)号：US20090171107A1
公开(公告)日：2009-07-02
申请号：US12300902
申请日：2007-05-11
申请人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
发明人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
IPC分类号： C07F1/08
CPC分类号： C25B3/12
摘要： The present invention relates to a process for preparing a porous metal organic framework comprising at least two organic compounds coordinated to at least one metal ion, which comprises the steps (a) oxidation of at least one anode comprising the metal corresponding to at least one metal ion in a reaction medium in the presence of at least one first organic compound which is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbons have been replaced by heteroatoms selected from the group consisting of N, O and S to form a reaction intermediate comprising the at least one metal ion and the first organic compound; and (b) reaction of the reaction intermediate at a prescribed temperature with at least one second organic compound which coordinates to the at least one metal ion, with the second organic compound being derived from a dicarboxylic, tricarboxylic or tetracarboxylic acid.
摘要翻译：本发明涉及一种制备多孔金属有机骨架的方法，所述多孔金属有机骨架包括与至少一种金属离子配位的至少两种有机化合物，其包括以下步骤：（a）至少一个阳极的氧化，所述至少一个阳极包含对应于至少一种金属在至少一种第一有机化合物存在下的反应介质中，所述第一有机化合物是任选取代的单环，双环或多环饱和或不饱和烃，其中至少两个环碳已经被选自N，O 和S形成包含所述至少一种金属离子和所述第一有机化合物的反应中间体; 和（b）将反应中间体在规定温度下与至少一种与至少一种金属离子配位的第二有机化合物反应，第二有机化合物衍生自二羧酸，三羧酸或四羧酸。

2. 发明授权

US07879221B2 Process for preparing porous metal organic frameworks 有权
标题翻译：制备多孔金属有机骨架的方法
公开(公告)号：US07879221B2
公开(公告)日：2011-02-01
申请号：US12300902
申请日：2007-05-11
申请人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
发明人： Hermann Pütter , Markus Schubert , Ingo Richter , Ulrich Müller , Natalia Trukhan
IPC分类号： C25B3/12 , C07F15/00 , C07F3/00
CPC分类号： C25B3/12
摘要： The present invention relates to a process for preparing a porous metal organic framework comprising at least two organic compounds coordinated to at least one metal ion, which comprises the steps (a) oxidation of at least one anode comprising the metal corresponding to at least one metal ion in a reaction medium in the presence of at least one first organic compound which is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbons have been replaced by heteroatoms selected from the group consisting of N, O and S to form a reaction intermediate comprising the at least one metal ion and the first organic compound; and (b) reaction of the reaction intermediate at a prescribed temperature with at least one second organic compound which coordinates to the at least one metal ion, with the second organic compound being derived from a dicarboxylic, tricarboxylic or tetracarboxylic acid.
摘要翻译：本发明涉及一种制备多孔金属有机骨架的方法，所述多孔金属有机骨架包括与至少一种金属离子配位的至少两种有机化合物，其包括以下步骤：（a）至少一个阳极的氧化，所述至少一个阳极包含对应于至少一种金属在至少一种第一有机化合物存在下的反应介质中，所述第一有机化合物是任选取代的单环，双环或多环饱和或不饱和烃，其中至少两个环碳已经被选自N，O 和S形成包含所述至少一种金属离子和所述第一有机化合物的反应中间体; 和（b）将反应中间体在规定温度下与至少一种与至少一种金属离子配位的第二有机化合物反应，第二有机化合物衍生自二羧酸，三羧酸或四羧酸。

3. 发明申请

US20090305040A1 METAL OXIDES FROM METAL-ORGANIC FRAMEWORK MATERIALS 失效
标题翻译：金属有机骨架材料的金属氧化物
公开(公告)号：US20090305040A1
公开(公告)日：2009-12-10
申请号：US12297298
申请日：2007-04-12
申请人： Markus Schubert , Ulrich Müller , Natalia Trukhan
发明人： Markus Schubert , Ulrich Müller , Natalia Trukhan
IPC分类号： C01F7/30 , C01F5/06 , C01G25/02
CPC分类号： B01J20/0211 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/28042 , B01J20/28057 , C01F5/02 , C01F7/30 , C01G1/02 , C01G9/02 , C01G23/047 , C01G25/00 , C01G25/02 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C01P2006/13 , C07C51/418 , Y10T428/2982 , C07C63/38 , C07C63/26 , C07C57/15
摘要： The present invention relates to a method for producing a metal oxide by heating a porous metal-organic framework material, the framework material comprising at least one at least bidentate organic compound bound to at least one metal ion by coordination, and the metal ion being selected from the metals comprising groups to 4 and 13 of the Periodic Table of the Elements, above the complete decomposition temperature of the framework material, and also to metal oxides obtainable by this method, and to the use thereof.
摘要翻译：本发明涉及通过加热多孔金属 - 有机骨架材料来生产金属氧化物的方法，所述骨架材料包含至少一种至少二齿有机化合物，其通过配位与至少一种金属离子结合，并且选择金属离子从元素周期表中的4至13的金属组成，高于骨架材料的完全分解温度，以及可通过该方法获得的金属氧化物及其用途。

4. 发明授权

US08501150B2 Metal oxides from metal-organic framework materials 失效
标题翻译：金属 - 有机骨架材料的金属氧化物
公开(公告)号：US08501150B2
公开(公告)日：2013-08-06
申请号：US12297298
申请日：2007-04-12
申请人： Markus Schubert , Ulrich Müller , Natalia Trukhan
发明人： Markus Schubert , Ulrich Müller , Natalia Trukhan
IPC分类号： C01F7/02 , C01B13/14
CPC分类号： B01J20/0211 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/28042 , B01J20/28057 , C01F5/02 , C01F7/30 , C01G1/02 , C01G9/02 , C01G23/047 , C01G25/00 , C01G25/02 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C01P2006/13 , C07C51/418 , Y10T428/2982 , C07C63/38 , C07C63/26 , C07C57/15
摘要： The present invention relates to a method for producing a metal oxide by heating a porous metal-organic framework material, the framework material comprising at least one at least bidentate organic compound bound to at least one metal ion by coordination, and the metal ion being selected from the metals comprising groups 2 to 4 and 13 of the Periodic Table of the Elements, above the complete decomposition temperature of the framework material, and also to metal oxides obtainable by this method, and to the use thereof.
摘要翻译：本发明涉及通过加热多孔金属 - 有机骨架材料来生产金属氧化物的方法，所述骨架材料包含至少一种至少二齿有机化合物，其通过配位与至少一种金属离子结合，并且选择金属离子包括元素周期表第2至4和13族的金属，高于骨架材料的完全分解温度，以及可通过该方法获得的金属氧化物及其用途。

5. 发明授权

US09688700B2 Metal-organic frameworks based on on 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid 有权
公开(公告)号：US09688700B2
公开(公告)日：2017-06-27
申请号：US13512637
申请日：2010-11-25
申请人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
发明人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
IPC分类号： C07F1/00 , C07F15/02 , C07F5/06 , C07F3/00
CPC分类号： C07F1/005 , C07F3/003 , C07F5/069 , C07F15/025
摘要： The present invention relates to porous metallic frameworks comprising at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the at least one at least bidentate organic compound is derived from 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid. The present invention further relates to shaped bodies comprising these frameworks, processes for producing them and their use, in particular for the storage and separation of gases.

6. 发明申请

US20120251438A1 Metal-Organic Frameworks Based on On 2,5-Furandicarboxylic Acid Or 2,5-Thiophenedicarboxylic Acid 有权
标题翻译：基于2,5-呋喃二羧酸或2,5-噻吩二羧酸的金属有机骨架
公开(公告)号：US20120251438A1
公开(公告)日：2012-10-04
申请号：US13512637
申请日：2010-11-25
申请人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
发明人： Natalia Trukhan , Ulrich Müller , Jens Heimann , Alois Kindler
IPC分类号： C07F5/06 , C07F3/06 , C01B3/56 , C07F3/02
CPC分类号： C07F1/005 , C07F3/003 , C07F5/069 , C07F15/025
摘要： The present invention relates to porous metallic frameworks comprising at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the at least one at least bidentate organic compound is derived from 2,5-furandicarboxylic acid or 2,5-thiophenedicarboxylic acid. The present invention further relates to shaped bodies comprising these frameworks, processes for producing them and their use, in particular for the storage and separation of gases.
摘要翻译：本发明涉及包含与至少一种金属离子配位的至少一种至少二齿有机化合物的多孔金属骨架，其中所述至少一种至少二齿有机化合物衍生自2,5-呋喃二甲酸或2,5-噻吩二羧酸酸。本发明还涉及包括这些框架的成形体，其制造方法及其用途，特别是用于气体的储存和分离。

7. 发明申请

US20120070353A1 Process For Separating Off Acidic Gases By Means Of Metal-Organic Frameworks Impregnated With Amines 审中-公开
标题翻译：通过用胺浸渍的金属有机骨架分离酸性气体的方法
公开(公告)号：US20120070353A1
公开(公告)日：2012-03-22
申请号：US13257830
申请日：2010-03-18
申请人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
发明人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
IPC分类号： B01D53/40 , C09K3/00 , B01D53/56 , B01D53/52 , B01D53/62 , B01D53/50
CPC分类号： C10L3/10 , B01D53/025 , B01D53/40 , B01D53/62 , B01D2252/2023 , B01D2252/20405 , B01D2252/2041 , B01D2252/20421 , B01D2252/20426 , B01D2252/20431 , B01D2252/20436 , B01D2252/20484 , B01D2253/204 , B01D2253/25 , B01D2256/16 , B01D2256/24 , B01D2257/302 , B01D2257/304 , B01D2257/404 , B01D2257/504 , B01D2258/05 , B01D2258/06 , B01J20/226 , B01J20/2803 , B01J20/28042 , B01J20/28057 , B01J20/3007 , B01J20/3206 , B01J20/3248 , B01J20/3255 , C07F1/005 , C07F3/003 , C07F5/003 , C07F15/025 , C07F15/045 , C07F15/065 , C10L3/102 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a process for separating off at least one acidic gas from a gas mixture comprising at least one acidic gas, which comprises the step of contacting of the gas mixture with a porous metal-organic framework, where the framework adsorbs the at least one acidic gas and the framework comprises at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the porous metal-organic framework is impregnated with an amine suitable for a gas scrub. The invention further provides such impregnated metal-organic frameworks.
摘要翻译：本发明涉及一种从包含至少一种酸性气体的气体混合物中分离出至少一种酸性气体的方法，该方法包括使气体混合物与多孔金属 - 有机骨架接触的步骤，其中框架吸附在至少一种酸性气体和骨架包含与至少一种金属离子配位的至少一种至少二齿的有机化合物，其中多孔金属 - 有机骨架用适于气体洗涤的胺浸渍。本发明还提供了这种浸渍的金属 - 有机骨架。

8. 发明申请

US20110152375A1 METHOD OF REDUCING THE METHANE GAS LEVEL AND OF INCREASING THE TOTAL GAS YIELD IN ANIMAL FEED 审中-公开
标题翻译：减少甲烷气体水平和增加动物饲料总气量的方法
公开(公告)号：US20110152375A1
公开(公告)日：2011-06-23
申请号：US12688963
申请日：2010-01-18
申请人： Arnulf Tröscher , Michael Koch , Natalia Trukhan , Ulrich Müller
发明人： Arnulf Tröscher , Michael Koch , Natalia Trukhan , Ulrich Müller
IPC分类号： A61K31/19 , A23K1/18 , A23K1/16 , A61P1/00
CPC分类号： A23K50/10 , A23K20/24 , Y02P60/56
摘要： The present invention relates to the use of at least one porous metal-organic framework material (MOF) comprising at least one first and, if appropriate, one second organic compound, where at least the first organic compound binds coordinatively to at least one metal ion in an at least partly bidentate manner, where the at least one metal ion is Mg(II) and where the first organic compound is derived from formic acid and the second organic compound from acetic acid, for reducing the methane level in the total gas produced, and to the use for increasing the total gas formation during feed digestion in ruminants as well as a method for reducing the methane level in the total gas produced and a method for increasing the total gas formation during feed digestion in ruminants.
摘要翻译：本发明涉及至少一种多孔金属 - 有机骨架材料（MOF）的用途，所述多孔金属 - 有机骨架材料（MOF）包含至少一种第一和（如果合适的话）一种第二有机化合物，其中至少第一有机化合物与至少一种金属离子至少部分二齿的方式，其中至少一种金属离子是Mg（II），其中第一有机化合物衍生自甲酸，第二有机化合物来自乙酸，用于降低产生的总气体中的甲烷水平以及用于增加反刍动物饲料消化期间的总气体形成的用途以及降低所产生的总气体中的甲烷水平的方法以及用于增加反刍动物饲料消化过程中的总气体形成的方法。

9. 发明申请

US20130012717A1 Process For Preparing A Porous Metal-Organic Framework Composed Of Zinc Methylimidazolate 有权
标题翻译：制备由甲基咪唑锌组成的多孔金属有机结构的方法
公开(公告)号：US20130012717A1
公开(公告)日：2013-01-10
申请号：US13542971
申请日：2012-07-06
申请人： Natalia Trukhan , Ulrich Müller
发明人： Natalia Trukhan , Ulrich Müller
IPC分类号： C07F3/06
CPC分类号： C07F3/06
摘要： Described is a process for preparing a porous metal-organic framework comprising at least one at least bidentate organic compound coordinated to at least one metal ion, where the at least one metal ion is a zinc ion and the at least one at least bidentate organic compound is based on 2-methylimidazole, which comprises the steps (a) addition of a first water-based solution comprising zinc ions to a second water-based solution comprising 2-methylimidazole, with a suspension being formed after addition of the second solution; (b) addition of a third solution comprising a strong base to the suspension formed in step (a).
摘要翻译：描述了一种制备多孔金属 - 有机骨架的方法，所述多孔金属 - 有机骨架包含至少一种与至少一种金属离子配位的至少二齿有机化合物，其中所述至少一种金属离子是锌离子，并且所述至少一种至少二齿有机化合物是基于2-甲基咪唑，其包括以下步骤：（a）在包含2-甲基咪唑的第二水性溶液中加入包含锌离子的第一水性溶液，在加入第二溶液后形成悬浮液; （b）向步骤（a）中形成的悬浮液中加入包含强碱的第三溶液。

10. 发明申请

US20120049110A1 Process For Producing A Carbon-Comprising Composite 审中-公开
标题翻译：生产含碳复合材料的工艺
公开(公告)号：US20120049110A1
公开(公告)日：2012-03-01
申请号：US13222488
申请日：2011-08-31
申请人： Natalia Trukhan , Ulrich Müller , Emi Leung , Alexander Panchenko , Nicole Janssen
发明人： Natalia Trukhan , Ulrich Müller , Emi Leung , Alexander Panchenko , Nicole Janssen
IPC分类号： H01M4/583 , B01D53/047 , H01M4/04 , C01B31/30 , C01B31/34
CPC分类号： B01D53/02 , B01D53/047 , B01D2253/102 , B01D2253/204 , B01D2255/207 , B01D2257/11 , B01D2257/302 , B01D2257/404 , B01D2257/406 , B01D2257/502 , B01D2257/504 , B01D2257/7022 , B01D2257/7025 , B01D2257/708 , B01D2259/4525 , H01M4/0409 , H01M4/0416 , H01M4/0471 , H01M4/133 , H01M4/583 , H01M10/052 , Y02C10/08 , Y02C20/20
摘要： The present invention relates to a process for producing a carbon-comprising composite, wherein a porous metal-organic framework comprising at least one at least bidentate organic compound coordinated to at least one metal ion is pyrolyzed under a protective gas atmosphere and the at least one at least bidentate organic compound is nitrogen-free. The invention further relates to composites which can be obtained in this way and sulfur electrodes comprising these and also their uses.
摘要翻译：本发明涉及一种生产含碳复合材料的方法，其中包含至少一种与至少一种金属离子配位的至少二齿有机化合物的多孔金属 - 有机骨架在保护气体气氛下热解，并且所述至少一种至少二齿有机化合物是无氮的。本发明还涉及可以以这种方式获得的复合材料和包含这些的硫电极以及它们的用途。

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