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1. 发明申请

WO2007045457A1 FLUID MIXING DEVICE INSERTED IN OR COMBINED WITH A REACTOR 审中-公开
标题翻译：流体混合装置插入或与反应器组合
公开(公告)号：WO2007045457A1
公开(公告)日：2007-04-26
申请号：PCT/EP2006/010049
申请日：2006-10-18
申请人： ENI S.P.A. , BARTOLINI, Andrea , BASINI, Luca , GUARINONI, Alessandra , BENNARDO, Antonio , ONORATI, Nicola
发明人： BARTOLINI, Andrea , BASINI, Luca , GUARINONI, Alessandra , BENNARDO, Antonio , ONORATI, Nicola
IPC分类号： B01J8/02 , B01F5/06 , C01B3/38
CPC分类号： B01F5/0453 , B01F5/0456 , B01J8/009 , B01J8/0278 , B01J2208/00849 , B01J2219/00265 , C01B3/386 , C01B2203/0261 , C01B2203/1276 , Y02P20/52 , Y10T137/87652
摘要： A device is described for mixing two fluids, inserted in or combined with a reactor, which can also be used for catalytic partial oxidation, substantially consisting of the following zones : - a first feeding zone equipped with means for allowing a first fluid, possibly gaseous under the operating conditions, to enter in an axial direction; - an underlying distribution zone containing a bundle of pipes preferably parallel to the axis inside which said fluid is uniformly distributed; - a second feeding zone equipped with means for allowing a second fluid to enter the distribution zone containing the bundle of preferably parallel pipes and to be uniformly distributed outside said parallel pipes; - a mixing zone separated from the distribution zone by a pipe-plate supporting said parallel pipes, said pipe-plate having slits or openings in order to uniformly discharge the second fluid in an axial direction into the mixing area, and said parallel pipes extending beyond said pipe -plate into the mixing zone.
摘要翻译：描述了一种装置，用于混合两个流体，其插入反应器中或与反应器组合，该反应器也可用于催化部分氧化，基本由以下区域组成： - 第一进料区，其配备有允许第一流体在操作条件下，沿轴向进入; - 底层分布区，其包含优选平行于所述流体均匀分布的轴线的管束; - 第二进料区，其具有用于允许第二流体进入包含优选平行管束的分配区并且均匀分布在所述平行管外部的装置; - 通过支撑所述平行管的管板与分配区分离的混合区，所述管板具有狭缝或开口，以便将第二流体沿轴向均匀地排放到混合区域中，并且所述平行管延伸超过所述管板进入混合区。

2. 发明申请

WO2005023710A3 CATALYTIC PARTIAL OXIDATION PROCESS FOR PRODUCING SYNTHESIS GAS 审中-公开
公开(公告)号：WO2005023710A3
公开(公告)日：2005-03-17
申请号：PCT/EP2004/010169
申请日：2004-09-09
申请人： ENI S.P.A. , ENITECNOLOGIE S.P.A. , BASINI, Luca , BARTOLINI, Andrea , LUPI, Giancarlo , CLERICI, Gabriele, Carlo, Ettore
发明人： BASINI, Luca , BARTOLINI, Andrea , LUPI, Giancarlo , CLERICI, Gabriele, Carlo, Ettore
IPC分类号： C01B3/38
摘要： Partial oxidation process of liquid fuels, selected from hydrocarbon and/or oxygenated compounds, together with gaseous fuels, selected from hydrocarbon compounds, natural gas and LPG, by means of a suitable catalytic system comprising the following steps: premixing the reagents and possibly heating them to temperatures ranging from 25 to 400 °C, said reagents consisting of said liquid fuels, said gaseous fuels and oxygen or air or oxygen enriched air, optionally in the presence of vapour and/or CO 2 ; reacting the mixture of reagents in the catalytic zone, at inlet temperatures ranging from 50 to 500 °C and space velocities ranging from 1,000 to 1,000,000 Nl reagents/L cat x h, reaching temperatures ranging from 450 to 1350 °C.

3. 发明申请

WO2006034868A1 EQUIPMENT FOR THE ATOMISATION OF A LIQUID STREAM BY MEANS OF A DISPERSING GASEOUS STREAM AND FOR MIXING THE ATOMISED PRODUCT WITH A FURTHER SUITABLE GASEOUS STREAM IN EQUIPMENT FOR EFFECTING CATALYTIC PARTIAL OXIDATIONS AND RELATIVE CATALYTIC PARTIAL OXIDATION PROCESS 审中-公开
标题翻译：用于通过分散式气体流引起的液体流的设备，以及用于混合原始产品与在设备中进一步适用气体流的效应用于催化部分氧化和相对催化部分的设备
公开(公告)号：WO2006034868A1
公开(公告)日：2006-04-06
申请号：PCT/EP2005/010574
申请日：2005-09-26
申请人： ENI S.P.A. , ENITECNOLOGIE S.P.A , BARTOLINI, Andrea , BASINI, Luca , LUPI, Giancarlo
发明人： BARTOLINI, Andrea , BASINI, Luca , LUPI, Giancarlo
IPC分类号： B01J8/02 , B01J19/26 , C01B3/38 , B05B7/04 , B01J19/24
CPC分类号： B01J19/26 , B01B1/005 , B01J4/002 , B01J8/008 , B01J8/0264 , B01J8/0278 , B01J19/248 , B01J27/24 , B05B7/0458 , B05B7/08 , B05B7/0861 , C01B3/382 , C01B3/386 , C01B2203/0244 , C01B2203/0261 , C01B2203/0844 , C01B2203/1064 , C01B2203/1247 , C01B2203/1276 , C01B2203/142 , C01B2203/82 , Y02P20/52
摘要： Equipment for the atomisation of a liquid stream by means of a dispersing gaseous stream and for mixing the atomised product with a further suitable gaseous stream, characterized in that it comprises: a feeding zone (A) equipped with means suitable for feeding the liquid stream, the gaseous dispersing stream and further gaseous stream; one or more two-stage atomisation zones (N) of the liquid stream by means of the gaseous dispersing stream; a distribution zone (D) of the further gaseous stream; the first stage of the atomisation zone (N1) essentially consisting of a tubular core (2), through which the liquid stream passes, equipped with an appropriate series of nozzles (5), situated at the same height, and an outer jacket (4) coaxial to said core, through which the gaseous dispersing stream passes, wherein said nozzles (5) allow the gaseous dispersing stream to enter the tubular core, perpendicularly to the axis of said tubular core (2), effecting a first atomisation of the liquid stream, the second stage of the atomisation zone (N2) essentially consisting of one or more nozzles (6) positioned at the end of the tubular core (2), parallel to the axis of said tubular core, to increase the atomisation degree, the distribution zone (D) essentially consisting of a further jacket (8), through which the further gaseous stream passes, external and coaxial to the jacket (4) of the first atomisation stage, and a series of nozzles (9) situated at the bottom of said further jacket, all positioned at. the same height and parallel or inclined with an alpha angle lower than 40° with respect to the axis of the tubular core.
摘要翻译：用于通过分散气流使液体流雾化并用于将雾化产物与另外合适的气流混合的设备，其特征在于，其包括：装有适于供给液体流的装置的进料区（A）气态分散流和另外的气流; 液态物流的一个或多个两级雾化区（N），通过气态分散物流; 进一步气流的分配区（D）; 雾化区（N1）的第一阶段基本上由管状芯（2）组成，液体流通过管状核心（2）配备有位于相同高度的适当系列的喷嘴（5），外护套（4））与气体分散流通过的所述核共轴，其中所述喷嘴（5）允许气态分散流垂直于所述管状芯（2）的轴线进入管状芯，从而实现液体的第一雾化流，基本上由位于管状芯（2）的端部的一个或多个喷嘴（6）组成的雾化区（N2）的第二阶段，平行于所述管状芯的轴线，以增加雾化度，分布区（D），其基本上由另外的护套（8）组成，另外的气体流通过该外部气流与第一雾化级的护套（4）外部并同轴，并且位于底部的一系列喷嘴（9）所说的另外一件夹克位于。相同的高度并且相对于管状芯的轴线平行或倾斜成α角小于40°。

4. 发明申请

WO2012069625A1 PROCESS FOR THE SELECTIVE REMOVAL OF MOLYBDENUM FROM A SOLUTION CONTAINING IT 审中-公开
标题翻译：从含有它的溶液中选择性去除莫来石的方法
公开(公告)号：WO2012069625A1
公开(公告)日：2012-05-31
申请号：PCT/EP2011/071011
申请日：2011-11-25
申请人： ENI S.P.A. , BARTOLINI, Andrea , SENTIMENTI, Emilio
发明人： BARTOLINI, Andrea , SENTIMENTI, Emilio
IPC分类号： C22B3/26 , C22B3/20 , C22B7/00 , C22B34/22 , C22B34/34 , C01G39/00 , C01G39/06
CPC分类号： C22B34/34 , C01G39/003 , C22B3/0031 , C22B3/20 , C22B7/007 , C22B7/009 , C22B34/225 , C22B34/345 , Y02P10/214 , Y02P10/23 , Y02P10/234 , Y10S210/912
摘要： The present invention relates to a process for selectively removing molybdenum from a solution which contains molybdenum, said process comprising the following steps: ■ bringing the solution to an acid pH lower than or equal to 3, preferably lower than or equal to 2, even more preferably lower than or equal to 0.5, by the addition of an inorganic acid; ■ adding at least one organic solvent, preferably toluene or xylene, to the solution and stirring continuously so as to create a water-organic emulsion; ■ adding to the water-organic emulsion at least one alkaline metal xanthate having the general formula MeRX, wherein R is a linear or branched alkyl group having a number of carbon atoms higher than or equal to 2, Me is an alkaline metal selected from Li, Na, K, Rb, Cs and Fr, and X is the xanthate group, so as to form a complex with molybdenum wherein the molar ratio molybdenum/alkaline metal xanthate ranges from 1/6 to 1/2, keeping the emulsion at an acid pH by the addition of an inorganic acid, and interrupting the stirring so as to allow the separation of the aqueous phase from the organic phase. The linear or branched alkyl group R preferably has a number of carbon atoms higher than or equal to 2 and lower than or equal to 12. A reductant is optionally added to the starting solution which comprises Mo and V.
摘要翻译：本发明涉及从含有钼的溶液中选择性除去钼的方法，所述方法包括以下步骤：使该溶液的酸pH低于或等于3，优选低于或等于2，甚至更多优选低于或等于0.5，通过加入无机酸; |向溶液中加入至少一种有机溶剂，优选甲苯或二甲苯，并连续搅拌，以产生水 - 有机乳液; 向水 - 有机乳液中加入至少一种具有通式MeRX的碱金属黄原酸盐，其中R是碳原子数高于或等于2的直链或支链烷基，Me是选自Li ，Na，K，Rb，Cs和Fr，X是黄原酸酯基，以便与钼形成络合物，其中钼/碱金属黄原酸酯的摩尔比为1/6至1/2，将乳液保持在通过加入无机酸的酸性pH，并且中断搅拌以使水相与有机相分离。直链或支链烷基R优选具有高于或等于2且低于或等于12的碳原子数。还原剂任选地加入到包含Mo和V的起始溶液中。

5. 发明申请

WO2011072841A1 PROCESS FOR RECOVERING METALS FROM A STREAM RICH IN HYDROCARBONS AND CARBONACEOUS RESIDUES 审中-公开
标题翻译：从碳氢化合物和碳氢化合物中回收金属的方法
公开(公告)号：WO2011072841A1
公开(公告)日：2011-06-23
申请号：PCT/EP2010/007627
申请日：2010-12-13
申请人： ENI S.P.A. , BARTOLINI, Andrea , POLLESEL, Paolo , SENTIMENTI, Emilio , CHECCHIN, Michele
发明人： BARTOLINI, Andrea , POLLESEL, Paolo , SENTIMENTI, Emilio , CHECCHIN, Michele
IPC分类号： C22B7/00
CPC分类号： C10G21/06 , C10G21/28 , C10G2300/205 , C22B3/22 , C22B7/008 , C22B7/009 , C22B23/026 , C22B34/225 , Y02P10/214 , Y02P10/224 , Y02P10/23 , Y02P10/234 , Y02W30/54
摘要： A process for recovering metals from a stream rich in hydrocarbons and carbonaceous residues by means of a treatment section characterized in that it comprises the following steps : • sending said stream to an extraction by mixing said stream with a suitable hydrophilizing agent, i.e. being capable of removing the hydrophobic qualities of said stream; • sending the mixture consisting of said stream and said hydrophilizing agent to separation, separating a liquid phase containing most of the hydrophilizing agent and hydrocarbons dissolved from a "solid" phase; • preferably subjecting the "solid" phase separated to drying effected at a maximum temperature of 3500C in order to remove the medium- light hydrocarbon components from the "solid" phase; • sending the "solid" phase separated, preferably dried, to leaching with an alkaline solution in the presence of air and/or oxygen and possibly in the presence of an emulsifying agent or its precursor; • sending the leached mixture to separation, separating the solid residue from the liquor.
摘要翻译：一种通过处理部分从富含烃和碳质残渣的物流中回收金属的方法，其特征在于其包括以下步骤：将所述物流与合适的亲水剂混合，将所述物流与所述物流混合，去除所述流的疏水性质; 将由所述流和所述亲水剂组成的混合物发送到分离，分离含有大部分亲水剂的液相和从“固体”相中溶解的烃; 优选在350℃的最高温度下对分离的“固体”相进行干燥，以从“固体”相除去中轻烃成分; °的“固体”相分离，优选干燥，在空气和/或氧气存在下并可能在乳化剂或其前体存在下用碱性溶液浸出; °将该沥滤混合物送入分离，将固体残渣与液体分离。

6. 发明申请

WO2010142397A2 PROCESS FOR RECOVERING METALS FROM A STREAM RICH IN HYDROCARBONS AND CARBONACEOUS RESIDUES 审中-公开
标题翻译：从碳氢化合物和碳氢化合物中回收金属的方法
公开(公告)号：WO2010142397A2
公开(公告)日：2010-12-16
申请号：PCT/EP2010/003345
申请日：2010-06-01
申请人： ENI S.P.A. , BARTOLINI, Andrea , CORNARO, Ugo , POLLESEL, Paolo , OUDENNE, Paul, Dominique
发明人： BARTOLINI, Andrea , CORNARO, Ugo , POLLESEL, Paolo , OUDENNE, Paul, Dominique
IPC分类号： C10G47/26
CPC分类号： C10G47/26 , B01J23/28 , B01J23/92 , B01J38/02 , B01J38/72 , C10G49/12 , C10G49/22 , C10G2300/1025 , C10G2300/205 , C10G2300/301 , C10G2300/4006 , C10G2300/4081 , C22B3/20 , C22B7/001 , Y02P10/214 , Y02P10/234
摘要： A process for recovering metals from a stream rich in hydrocarbons and carbonaceous residues by means of a treatment section, characterized in that it comprises the following steps: sending said stream to a primary treatment, effected in one or more steps, wherein said stream is treated in the presence of a fluxant agent in a suitable apparatus, at a temperature ranging from 80 to 180°C, preferably from 100 to 160°C, and subjected to liquid/solid separation in order to obtain a clarified product essentially consisting of liquids and a cake (oilcake); possibly subjecting the separated cake to drying, in order to remove the hydrocarbon component having a boiling point lower than a temperature ranging from 300 to 350°C from the cake; sending the cake, possibly dried, to a secondary thermal treatment comprising: a flameless pyrolysis of the cake effected between 400 and 800°C, preferably between 500 and 670°C; an oxidation of the pyrolysis residue effected in an oxidizing environment and at temperatures ranging from 400 to 800°C, preferably from 500 to 700°C.
摘要翻译：一种通过处理部分从富含烃和碳质残余物的物流中回收金属的方法，其特征在于其包括以下步骤：将一个或多个步骤中的所述物流送入初级处理，其中所述物流被处理在合适的装置中，在80至180℃，优选100至160℃的温度范围内，存在助剂，并进行液/固分离，以获得基本上由液体和一块蛋糕（油饼）; 可能使分离的饼干经历干燥，以便从饼中除去沸点低于300-350℃的沸点的烃成分; 将可能干燥的蛋糕送到二次热处理中，其包括：在400和800℃之间，优选在500和670℃之间进行无蛋白质的热解; 在氧化环境和400至800℃，优选500至700℃的温度范围内进行热解残留的氧化。

7. 发明申请

WO2003053567A2 CATALYTIC COMPOSITION FOR THE DEHYDROGENATION OF ALKYLAROMATIC HYDROCARBONS 审中-公开
标题翻译：用于脱氢烷基碳氢化合物的催化组合物
公开(公告)号：WO2003053567A2
公开(公告)日：2003-07-03
申请号：PCT/EP2002/014816
申请日：2002-12-18
申请人： SNAMPROGETTI S.p.A. , BARTOLINI, Andrea , SANFILIPPO, Domenico , IEZZI, Rodolfo
发明人： BARTOLINI, Andrea , SANFILIPPO, Domenico , IEZZI, Rodolfo
IPC分类号： B01J23/34
CPC分类号： B01J23/96 , B01J23/34 , B01J23/6562 , C07C5/3332 , C07C2521/04 , C07C2523/04 , C07C2523/08 , C07C2523/34 , C07C2523/42 , Y02P20/584 , C07C15/46
摘要： Process for the catalytic dehydrogenation of alkylaromatic hydrocarbons optionally mixed with ethane which comprises: A) dehydrogenating the hydrocarbon stream, optionally mixed with an inert gas, in a fluid bed reactor in the presence of a catalytic composition based on gallium and manganese supported on alumina modified with silica, at a temperature ranging from 400 to 700°C, at a total pressure ranging from 0.1 to 3 ata and with a GHSV (Gas Hourly Space Velocity) ranging from 50 to 10,000 h -1 ; and B) regenerating and heating the catalyst, by means of the catalytic oxidation of a fuel, in a fluid bed regenerator at a temperature higher than 400°C.
摘要翻译：用于任选与乙烷混合的烷基芳烃的催化脱氢方法，其包括：在流化床反应器中，在基于负载在氧化铝上的载体上的载体上的镓和锰的催化组合物存在下，将烃流任选地与惰性气体混合，二氧化硅，温度范围为400-700℃，总压力为0.1至3ata，GHSV气体小时空速为50至10,000h-1，B为催化剂再生和加热，借助于在高于400℃的温度下在流化床再生器中催化氧化燃料。

8. 发明申请

WO2017109728A1 PROCESS FOR THE TREATMENT OF REFINERY PURGE STREAMS 审中-公开
标题翻译：炼油厂净化流程的处理
公开(公告)号：WO2017109728A1
公开(公告)日：2017-06-29
申请号：PCT/IB2016/057891
申请日：2016-12-21
申请人： ENI S.P.A.
发明人： BARTOLINI, Andrea
IPC分类号： C10G31/06 , C10G31/10 , C10G21/00 , C10G21/12 , C10G21/14
CPC分类号： C10G31/06 , C10G21/003 , C10G21/12 , C10G21/14 , C10G31/10
摘要： The present invention relates to a process for the treatment of refinery purge streams, containing a hydrocarbon component in slurry phase having a boiling point higher than or equal to 140°C, characterized by the presence of quantities of asphaltenes higher than or equal to 5% by weight and characterized by the presence of a solid content higher than or equal to 5% by weight. The process provides that said purge be mixed with a suitable fluxing agent according to appropriate ratios and under certain conditions, forming a suspension with a content higher than or equal to 10% by weight of compounds having a boiling point TbP lower than or equal to 350°C. After mixing, the suspension is sent to a liquid/solid separation step which operates under suitable conditions, separating a solid phase containing a residual organic component and a solid component, called cake, and a liquid phase containing residual solids. The solid phase obtained is cooled to below 60°C, including the upper extreme, forming a granular solid which is stored and maintained at a temperature lower than or equal to 60°C.
摘要翻译：本发明涉及一种处理炼油厂吹扫气流的方法，所述方法包含在沸点高于或等于140℃的淤浆相中的烃组分，其特征在于存在沥青质高于或等于5重量％，其特征在于存在高于或等于5重量％的固体含量。该方法规定，所述吹扫按照合适的比例和在某些条件下与合适的助熔剂混合，形成含量高于或等于10重量％的沸点TbP低于或等于350℃的化合物 ;C。混合后，将悬浮液送入在合适条件下操作的液体/固体分离步骤，分离含有残余有机组分和称为滤饼的固体组分的固相和含有残余固体的液相。将所获得的固相冷却至低于60℃（包括上限），形成粒状固体，将其储存并保持在低于或等于60℃的温度。

9. 发明公开

EP1954386A1 FLUID MIXING DEVICE INSERTED IN OR COMBINED WITH A REACTOR 审中-公开
标题翻译：方法和反应器，流体混合器
公开(公告)号：EP1954386A1
公开(公告)日：2008-08-13
申请号：EP06806365.0
申请日：2006-10-18
申请人： ENI S.p.A.
发明人： BARTOLINI, Andrea , BASINI, Luca , GUARINONI, Alessandra , BENNARDO, Antonio , ONORATI, Nicola
IPC分类号： B01J8/02 , B01F5/06 , C01B3/38
CPC分类号： B01F5/0453 , B01F5/0456 , B01J8/009 , B01J8/0278 , B01J2208/00849 , B01J2219/00265 , C01B3/386 , C01B2203/0261 , C01B2203/1276 , Y02P20/52 , Y10T137/87652
摘要： A device is described for mixing two fluids, inserted in or combined with a reactor, which can also be used for catalytic partial oxidation, substantially consisting of the following zones : - a first feeding zone equipped with means for allowing a first fluid, possibly gaseous under the operating conditions, to enter in an axial direction; - an underlying distribution zone containing a bundle of pipes preferably parallel to the axis inside which said fluid is uniformly distributed; - a second feeding zone equipped with means for allowing a second fluid to enter the distribution zone containing the bundle of preferably parallel pipes and to be uniformly distributed outside said parallel pipes; - a mixing zone separated from the distribution zone by a pipe-plate supporting said parallel pipes, said pipe-plate having slits or openings in order to uniformly discharge the second fluid in an axial direction into the mixing area, and said parallel pipes extending beyond said pipe -plate into the mixing zone.

10. 发明授权

EP1796825B1 EQUIPMENT FOR THE ATOMISATION OF A LIQUID STREAM BY MEANS OF A DISPERSING GASEOUS STREAM AND FOR MIXING THE ATOMISED PRODUCT WITH A FURTHER SUITABLE GASEOUS STREAM IN EQUIPMENT FOR EFFECTING CATALYTIC PARTIAL OXIDATIONS AND RELATIVE CATALYTIC PARTIAL OXIDATION PROCESS 有权
标题翻译： DEVICE用于喷射的流体流USING A气体流量和分散混合雾化产物，在该装置另一种合适的气体流动具体实施催化部分氧化AND ASSOCIATED METHODS催化部分氧化
公开(公告)号：EP1796825B1
公开(公告)日：2009-01-14
申请号：EP05796839.8
申请日：2005-09-26
申请人： ENI S.p.A.
发明人： BARTOLINI, Andrea , BASINI, Luca , LUPI, Giancarlo
IPC分类号： B01J8/02 , B01J19/26 , C01B3/38 , B05B7/04 , B01J19/24
CPC分类号： B01J19/26 , B01B1/005 , B01J4/002 , B01J8/008 , B01J8/0264 , B01J8/0278 , B01J19/248 , B01J27/24 , B05B7/0458 , B05B7/08 , B05B7/0861 , C01B3/382 , C01B3/386 , C01B2203/0244 , C01B2203/0261 , C01B2203/0844 , C01B2203/1064 , C01B2203/1247 , C01B2203/1276 , C01B2203/142 , C01B2203/82 , Y02P20/52

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