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1. 发明授权

US06610793B1 Modified poly(ethylene oxide), method of making same and articles using same 有权
标题翻译：改性聚（环氧乙烷），其制备方法和使用其的制品
公开(公告)号：US06610793B1
公开(公告)日：2003-08-26
申请号：US09579843
申请日：2000-05-26
申请人： Dave A. Soerens , Eric D. Johnson , Gregory J. Wideman , James Hongxue Wang
发明人： Dave A. Soerens , Eric D. Johnson , Gregory J. Wideman , James Hongxue Wang
IPC分类号： C08F28300
CPC分类号： C08F283/00 , C08F283/06
摘要： A method for making modified poly(ethylene oxide) by graft polymerizing thereto organic monomers containing a trialkoxy silane functional group or a moiety that reacts with water to form a silanol group, such as methacryloxypropyl trimethoxy silane, onto the poly(ethylene oxide) is disclosed. The graft polymerization is accomplished by mixing the poly(ethylene oxide), the silane-containing monomer(s) and an initiator and applying heat. Preferably, the method is a reactive-extrusion process. The resulting modified poly(ethylene oxide) has improved water absorption characteristics and melt processabilities and may be used to make thermally processed articles, such as fibers, films and foams, that have improved properties over articles similarly processed from unmodified poly(ethylene oxide).
摘要翻译：公开了一种通过接枝聚合含有三烷氧基硅烷官能团的有机单体或与水反应以形成硅烷醇基的部分（例如甲基丙烯酰氧基丙基三甲氧基硅烷）到聚（环氧乙烷）上的改性聚环氧乙烷的方法）。接枝聚合通过将聚（环氧乙烷），含硅烷的单体和引发剂混合并施加热量来实现。优选地，该方法是反应挤出方法。所得到的改性聚环氧乙烷具有改善的吸水特性和熔融加工性能，并且可用于制造类似于未改性的聚（环氧乙烷）加工的制品具有改进性能的热处理制品，例如纤维，膜和泡沫。

2. 发明授权

US06790519B1 Moisture-induced poly(ethylene oxide) gel, method of making same and articles using same 失效
标题翻译：水分诱导的聚（环氧乙烷）凝胶，制备方法和使用相同的制品
公开(公告)号：US06790519B1
公开(公告)日：2004-09-14
申请号：US09579842
申请日：2000-05-26
申请人： Eric D. Johnson , Gregory J. Wideman , James Hongxue Wang
发明人： Eric D. Johnson , Gregory J. Wideman , James Hongxue Wang
IPC分类号： B32B518
CPC分类号： C08G65/336 , A61L15/26 , B32B7/12 , B32B27/06 , B32B27/12 , C08F283/06 , Y10T428/249953 , C08L71/02 , C08L83/10 , C08F230/08 , C08F220/36
摘要： A method for making modified poly(ethylene oxide) by graft polymerizing thereto organic monomers containing a trialkoxy silane functional group or a moiety that reacts with water to form a silanol group, such as methacryloxypropyl trimethoxy silane, onto the poly(ethylene oxide) is disclosed. The graft polymerization is accomplished by mixing the poly(ethylene oxide), the silane-containing monomer(s) and an initiator and applying heat. Preferably, the method is a reactive-extrusion process. After graft polymerization, the modified poly(ethylene oxide) may be exposed or subjected to relatively high moisture conditions, thereby causing crosslinking and formation of a structure that is capable of absorbing relatively large amounts of saline. The resulting modified poly(ethylene oxide) has improved properties over articles similarly processed from unmodified poly(ethylene oxide).
摘要翻译：公开了一种通过接枝聚合含有三烷氧基硅烷官能团的有机单体或与水反应以形成硅烷醇基的部分（例如甲基丙烯酰氧基丙基三甲氧基硅烷）到聚（环氧乙烷）上的改性聚环氧乙烷的方法）。接枝聚合通过将聚（环氧乙烷），含硅烷的单体和引发剂混合并施加热量来实现。优选地，该方法是反应挤出方法。接枝聚合后，改性聚（环氧乙烷）可能被暴露或经历相对高的水分条件，从而引起交联和形成能够吸收相对大量盐水的结构。所得到的改性聚（环氧乙烷）对于类似于未改性聚（环氧乙烷）加工的制品具有改进的性能。

3. 发明授权

US07012116B1 Blend compositions of an unmodified poly vinyl alcohol and a thermoplastic elastomer 有权
标题翻译：未改性的聚乙烯醇和热塑性弹性体的混合组合物
公开(公告)号：US07012116B1
公开(公告)日：2006-03-14
申请号：US09629678
申请日：2000-08-01
申请人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
发明人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
IPC分类号： C08L29/04
CPC分类号： C08J5/18 , C08J2329/04 , D01F6/14 , Y10T428/31504 , Y10T428/31551 , Y10T428/31725 , Y10T428/31786 , Y10T428/31826 , Y10T428/31855 , Y10T428/31931 , Y10T428/31935 , Y10T428/31938
摘要： This invention relates, in general, to blend compositions of an unmodified poly vinyl alcohol and a thermoplastic elastomer and thermoplastic film and fiber structures comprising these blend compositions. More specifically, this invention relates to substantially water-free films and fibers comprising unmodified polyvinyl alcohol and a thermoplastic elastomer.
摘要翻译：本发明一般涉及未改性的聚乙烯醇和热塑性弹性体的共混组合物和包含这些共混组合物的热塑性薄膜和纤维结构。更具体地，本发明涉及基本上无水的膜和包含未改性的聚乙烯醇和热塑性弹性体的纤维。

4. 发明授权

US06355347B1 Methods of making blend compositions of an unmodified polyvinyl alcohol and metallocene polyolefin or a grafted metallocene polyolefin 有权
标题翻译：制备未改性聚乙烯醇和茂金属聚烯烃或接枝茂金属聚烯烃的共混组合物的方法
公开(公告)号：US06355347B1
公开(公告)日：2002-03-12
申请号：US09629379
申请日：2000-08-01
申请人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
发明人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
IPC分类号： C08L2904
CPC分类号： C08J5/18 , C08J2329/04 , D01F6/14 , Y10T428/29 , Y10T428/2913 , Y10T428/298 , Y10T428/31504
摘要： This invention relates, in general, to methods of making blend compositions of an unmodified polyvinyl alcohol and a metallocene polyolefin or grafted metallocene polyolefin and thermoplastic film and fiber structures comprising these blend compositions. More specifically, this invention relates to methods of making substantially water-free films and fibers comprising unmodified polyvinyl alcohol and a metallocene polyolefin or grafted metallocene polyolefin.
摘要翻译：本发明一般涉及制备未改性的聚乙烯醇和茂金属聚烯烃或接枝金属茂聚烯烃和包含这些共混组合物的热塑性薄膜和纤维结构的共混组合物的方法。更具体地，本发明涉及制备基本上无水的膜和包含未改性的聚乙烯醇和茂金属聚烯烃或接枝茂金属聚烯烃的纤维的方法。

5. 发明授权

US06350518B1 Methods of making blend compositions of an unmodified poly vinyl alcohol and a thermoplastic elastomer 有权
标题翻译：制备未改性聚乙烯醇和热塑性弹性体的共混组合物的方法
公开(公告)号：US06350518B1
公开(公告)日：2002-02-26
申请号：US09630267
申请日：2000-08-01
申请人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
发明人： David Michael Schertz , James Hongxue Wang , Gregory J. Wideman , William S. Pomplun
IPC分类号： C08L2904
CPC分类号： C08J5/18 , C08J2329/04 , D01F6/14 , Y10T428/29 , Y10T428/2913 , Y10T428/298 , Y10T428/31504
摘要： This invention relates, in general, to methods of making blend compositions of an unmodified poly vinyl alcohol and a thermoplastic elastomer and thermoplastic film and fiber structures comprising these blend compositions. More specifically, this invention relates to methods of making substantially water-free films and fibers comprising unmodified polyvinyl alcohol and a thermoplastic elastomer.
摘要翻译：本发明一般涉及制备未改性的聚乙烯醇和热塑性弹性体和热塑性薄膜的共混组合物和包含这些共混组合物的纤维结构体的方法。更具体地，本发明涉及制备基本上无水的膜和包含未改性的聚乙烯醇和热塑性弹性体的纤维的方法。

6. 发明授权

US10753023B2 Toughened polylactic acid fibers 有权
公开(公告)号：US10753023B2
公开(公告)日：2020-08-25
申请号：US12855984
申请日：2010-08-13
申请人： Vasily A. Topolkaraev , Peiguang Zhou , Gregory J. Wideman , Tom Eby , Ryan J. McEneany
发明人： Vasily A. Topolkaraev , Peiguang Zhou , Gregory J. Wideman , Tom Eby , Ryan J. McEneany
IPC分类号： D04H3/009 , D01F6/92 , D01F6/62 , C08L67/04 , B29K105/00 , B29K67/00
摘要： Polylactic acid fibers formed from a thermoplastic composition that contains polylactic acid and a polymeric toughening additive are provided. The present inventors have discovered that the specific nature of the components and process by which they are blended may be carefully controlled to achieve a composition having desirable morphological features. More particularly, the toughening additive can be dispersed as discrete physical domains within a continuous phase of the polylactic acid. These domains have a particular size, shape, and distribution such that upon fiber drawing, they absorb energy and become elongated. This allows the resulting composition to exhibit a more pliable and softer behavior than the otherwise rigid polylactic acid. Through selective control over the components and method employed, the present inventors have discovered that the resulting fibers may thus exhibit good mechanical properties, both during and after melt spinning.

7. 发明授权

US09327438B2 Method for forming a thermoplastic composition that contains a plasticized starch polymer 有权
标题翻译：形成含有增塑淀粉聚合物的热塑性组合物的方法
公开(公告)号：US09327438B2
公开(公告)日：2016-05-03
申请号：US13330789
申请日：2011-12-20
申请人： James H. Wang , Gregory J. Wideman , JaeHong Lee
发明人： James H. Wang , Gregory J. Wideman , JaeHong Lee
IPC分类号： B29C47/00 , B29C47/88 , B29B9/06 , B29B7/94 , B29B7/42 , B29B7/90 , B29B9/02 , B29C47/34 , B29K105/00 , B29C47/30 , B29B7/46 , B29B7/72 , B29B9/16
CPC分类号： B29C47/0004 , B29B7/42 , B29B7/46 , B29B7/728 , B29B7/90 , B29B7/94 , B29B9/02 , B29B9/06 , B29B9/16 , B29C47/0011 , B29C47/0014 , B29C47/0021 , B29C47/0066 , B29C47/30 , B29C47/34 , B29C47/8805 , B29C47/8815 , B29C47/884 , B29C47/8845 , B29C47/8895 , B29C2793/009 , B29C2947/92704 , B29C2947/92723 , B29C2947/92923 , B29C2947/92933 , B29C2947/92942 , B29K2003/00 , B29K2105/0038 , B29K2995/0056 , B29K2995/006
摘要： A method and system for melt processing a thermoplastic composition that contains a starch and plasticizer is provided. The composition is melt blended and extruded through a die to form an extrudate, which is thereafter cooled using a multi-stage system of the present invention that includes at least one water-cooling stage and at least one air-cooling stage. More particularly, the extrudate is initially contacted with water for a certain period time so that it becomes partially cooled and solidified on its surface. After the water-cooling stage(s), the extrudate is also subjected to at least one air-cooling stage in which a stream of air is placed into contact with the extrudate.
摘要翻译：提供了一种用于熔融加工含有淀粉和增塑剂的热塑性组合物的方法和系统。将组合物熔融共混并通过模头挤出以形成挤出物，然后使用包括至少一个水冷段和至少一个空气冷却段的本发明的多级系统进行冷却。更具体地，挤出物最初与水接触一定时间，使得其在其表面上部分冷却和固化。在水冷却阶段之后，挤出物还经受至少一个空气冷却阶段，其中空气流与挤出物接触。

8. 发明授权

US08841386B2 Fibers formed from aromatic polyester and polyether copolymer 有权
标题翻译：由芳香族聚酯和聚醚共聚物形成的纤维
公开(公告)号：US08841386B2
公开(公告)日：2014-09-23
申请号：US12136090
申请日：2008-06-10
申请人： Aimin He , Vasily A. Topolkaraev , Alan E. Wright , Gregory J. Wideman
发明人： Aimin He , Vasily A. Topolkaraev , Alan E. Wright , Gregory J. Wideman
IPC分类号： C08G65/32 , C08L67/02 , D04H1/56 , C08F283/01 , C08L71/02
CPC分类号： D01F6/62 , C08F283/01 , C08L67/02 , C08L71/02 , D01F6/66 , D04H1/56 , D04H1/565 , Y10T442/60 , Y10T442/68 , Y10T442/681 , Y10T442/696 , C08L2666/22
摘要： A method for forming a fiber is provided. The method comprises supplying at least one aromatic polyester to a melt processing device and modifying the aromatic polyester with at least one polyether copolymer within the device to form a thermoplastic composition having a melt flow rate that is greater than the melt flow rate of the aromatic polyester. The polyether copolymer contains a repeating unit (A) having the following formula: C2H4Ox (A) wherein, x is an integer from 1 to 250, the polyether copolymer further containing a repeating unit (B) having the following formula: CnH2nOy (B) wherein, n is an integer from 3 to 20; and y is an integer from 1 to 150.
摘要翻译：提供了一种形成纤维的方法。该方法包括向熔融加工装置供应至少一种芳族聚酯，并在装置内用至少一种聚醚共聚物改性芳族聚酯以形成熔体流动速率大于芳族聚酯的熔体流动速率的热塑性组合物。聚醚共聚物含有具有下式的重复单元（A）：C 2 H 4 O x（A）其中x为1至250的整数，聚醚共聚物还含有具有下式的重复单元（B）：C n H 2n O y（B）其中n为3至20的整数; y为1〜150的整数。

9. 发明授权

US08445110B2 Water-sensitive film containing thermoplastic polyurethanes 有权
标题翻译：含热塑性聚氨酯的感光膜
公开(公告)号：US08445110B2
公开(公告)日：2013-05-21
申请号：US13432079
申请日：2012-03-28
申请人： Bo Shi , James H. Wang , Gregory J. Wideman
发明人： Bo Shi , James H. Wang , Gregory J. Wideman
IPC分类号： B32B27/40 , B29C47/08 , C09D175/04
CPC分类号： C08L29/04 , A61F13/15211 , A61F13/15731 , A61F13/60 , B29C55/06 , B29C55/08 , B29C55/12 , B29K2075/00 , B29K2105/0088 , B29K2995/0062 , C08J5/18 , C08J2329/04 , C08J2375/08 , C08K5/0016 , C08K5/053 , C08L71/02 , C08L75/04 , C08L2205/03 , C09J7/40 , C09J7/405 , C09J2429/006 , C09J2475/006 , Y10T428/1462 , Y10T428/1476 , Y10T428/31551 , Y10T428/31855 , Y10T428/31935 , C08L2666/20 , C08L2666/14
摘要： A film that contains a thermoplastic polyurethane and water-soluble polymer is provided. The film is both elastic and water-sensitive (e.g., water-soluble, water-dispersible, etc.) in that it loses its integrity over time in the presence of water. The dual attributes of elasticity and water-sensitivity may be achieved by reducing the tendency of the thermoplastic polyurethane and water-soluble polymer to form separate phases. Namely, phase separation may cause the elastomer to act as a barrier and limit the ability of the water-soluble polymer to contact water and thereby disperse. To minimize such phase separation, a variety of aspects of the film construction may be selectively controlled, such as the nature of the thermoplastic polyurethane and water-soluble polymer, the relative amount of each component, and so forth.
摘要翻译：提供含有热塑性聚氨酯和水溶性聚合物的薄膜。该膜既弹性又具有水敏性（例如，水溶性，水分散性等），因为它在水的存在下随着时间的推移失去其完整性。弹性和水敏性的双重属性可以通过降低热塑性聚氨酯和水溶性聚合物形成分离相的趋势来实现。也就是说，相分离可能导致弹性体作为屏障，并限制了水溶性聚合物与水接触从而分散的能力。为了最小化这种相分离，可以选择性地控制膜构造的各种方面，例如热塑性聚氨酯和水溶性聚合物的性质，各组分的相对量等。

10. 发明授权

US08329601B2 Biodegradable and renewable film 有权
标题翻译：可生物降解和再生膜
公开(公告)号：US08329601B2
公开(公告)日：2012-12-11
申请号：US12337779
申请日：2008-12-18
申请人： Bo Shi , Sarah A. Funk , James H. Wang , Gregory J. Wideman , Ross T. Kaufman , Vasily A. Topolkaraev
发明人： Bo Shi , Sarah A. Funk , James H. Wang , Gregory J. Wideman , Ross T. Kaufman , Vasily A. Topolkaraev
IPC分类号： B32B27/00 , B32B27/12 , C08L89/00 , B29C65/00 , B29C47/00
CPC分类号： A61L15/225 , A61L15/425 , A61L15/62 , B29C47/00 , B29C47/0026 , B29C55/005 , B29K2003/00 , B29K2105/04 , B29K2105/16 , B29K2995/006 , B32B5/022 , B32B9/02 , B32B27/08 , B32B27/12 , B32B27/20 , B32B27/22 , B32B27/30 , B32B27/32 , B32B27/36 , B32B27/40 , B32B37/153 , B32B2038/0028 , B32B2262/0238 , B32B2262/0246 , B32B2262/0253 , B32B2262/0261 , B32B2262/0276 , B32B2262/0292 , B32B2262/062 , B32B2305/20 , B32B2307/31 , B32B2307/7145 , B32B2307/7163 , B32B2307/724 , B32B2307/7265 , B32B2555/02 , C08J5/18 , C08J2300/16 , C08J2303/02 , C08L3/02 , C08L89/00 , Y10T428/24504 , Y10T442/282 , Y10T442/674 , C08L2666/26 , C08L89/02
摘要： A biodegradable and renewable film that may be employed in a wide variety of applications is provided. The film is formed from a thermoplastic composition that contains at least one starch and at least one plant protein. Even at a high renewable material content, the present inventors have discovered that films may be readily formed from plant proteins and starches by selectively controlling the individual amount of the starch and plant proteins, the nature of the starch and plant proteins, and other components used in the film. Balancing the amount of starches and plant proteins within a certain range, for instance, can reduce the likelihood of plant protein aggregation and enhance the ability of the composition to be melt processed. The composition also contains at least one plasticizer that improves the thermoplastic nature of the protein and starch components. The selection of the plasticizer may also help reduce the tendency of the plant protein to aggregate during melt processing. For example, a relatively acidic plasticizer (e.g., carboxylic acid) may be employed in certain embodiments to minimize the formation of disulfide bonds in a gluten protein, and thereby decrease its tendency to aggregate.
摘要翻译：提供了可用于各种应用的可生物降解和可再生的膜。该膜由含有至少一种淀粉和至少一种植物蛋白质的热塑性组合物形成。即使在高可再生材料含量下，本发明人也发现，通过选择性地控制淀粉和植物蛋白质的个体数量，淀粉和植物蛋白质的性质以及所使用的其它组分，可以容易地从植物蛋白质和淀粉形成膜在电影里。例如，将一定范围内的淀粉和植物蛋白质的量平衡可以降低植物蛋白质聚集的可能性并增加组合物被熔融加工的能力。该组合物还含有至少一种改善蛋白质和淀粉组分的热塑性质的增塑剂。增塑剂的选择也有助于降低植物蛋白质在熔融加工过程中聚集的趋势。例如，在某些实施方案中可以使用相对酸性的增塑剂（例如羧酸）以最小化谷蛋白中二硫键的形成，从而降低其聚集趋势。

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