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1. 发明申请

WO2013127255A1 PROCESS FOR MANUFACTURE OF HIGHLY ENRICHED EXTRACT CONTAINING ZEAXANTHIN AND/OR ITS ESTERS 审中-公开
标题翻译：含有高锰酸盐和/或其酯的高效提取物的制备方法
公开(公告)号：WO2013127255A1
公开(公告)日：2013-09-06
申请号：PCT/CN2013/000176
申请日：2013-02-22
申请人： DSM IP ASSETS B.V. , HE, Qing , ZHAO, Hai Ning , HUGENTOBLER, Max
发明人： HE, Qing , ZHAO, Hai Ning , HUGENTOBLER, Max
IPC分类号： C09B61/00 , A23L1/30 , A23L1/275 , A61K31/07
CPC分类号： C09B61/00 , A23L5/44 , A23L33/105 , A61K31/07
摘要： A process for the manufacture of an extract of Goji berries containing zeaxanthin and/or its esters is provided, comprising the following steps: a) obtaining dried Goji berries or size reduced pieces thereof; and b) treating the dried Goji berries or the size reduced pieces thereof with an alkali solution; and c) extracting the Goji berries or the size reduced pieces thereof obtained in step b) with a solvent selected from the group consisting of ethyl acetate, hexane, heptane, petroleum ether, acetone, butane, ethyl methyl ketone, methanol, propan-2-ol and mixtures thereof; and d) removing the solvent from the extracts obtained in step c); and e) optionally cleaving the esters in the dried extracts obtained in step d); and f) optionally crystallizing the dried extracts obtained in step d) or e) in an aliphatic straight or branched C 1-4 alcohol. Preferably the process consists only of the steps a) to f) given above.
摘要翻译：提供了一种制备含有玉米黄质和/或其酯的枸杞浆果提取物的方法，包括以下步骤：a）获得干燥的枸杞子或其尺寸减小的片; 和b）用碱溶液处理干燥的枸杞或其大小减少的块; 和c）用选自乙酸乙酯，己烷，庚烷，石油醚，丙酮，丁烷，乙基甲基酮，甲醇，丙-2-醇的溶剂提取步骤b）中获得的枸杞或其大小减少的片醇及其混合物; 和d）从步骤c）中获得的提取物中除去溶剂; 和e）任选地将步骤d）中获得的干燥提取物中的酯裂解; 和f）任选地将步骤d）或e）中获得的干燥提取物结晶在脂肪族直链或支链C 1-4醇中。优选地，该方法仅由上述步骤a）至f）组成。

2. 发明申请

WO2013123618A1 PROCESS FOR MANUFACTURE OF EXTRACT CONTAINING ZEAXANTHIN AND/OR ITS ESTERS 审中-公开
标题翻译：含有ZEAXANTHIN和/或其酯的提取物的制备方法
公开(公告)号：WO2013123618A1
公开(公告)日：2013-08-29
申请号：PCT/CN2012/000230
申请日：2012-02-22
申请人： DSM IP Assets B.V. , HE, Qing , ZHAO, Hai-ning , HUGENTOBLER, Max
发明人： HE, Qing , ZHAO, Hai-ning , HUGENTOBLER, Max
IPC分类号： A61K36/815 , A61K31/047 , C07C403/24 , A61P27/02 , A61P35/00 , A61P39/06 , A23L1/27 , A23L1/29 , A61K131/00
CPC分类号： C07C403/24 , A23L33/105 , A61K31/047 , A61K36/815 , A61K2236/00
摘要： A process for the manufacture of an extract of the skin of Goji berries containing zeaxanthin and/or its esters, comprises the following steps: a) obtaining dried skin of Goji berries or the size reduced pieces thereof; and b) extracting the dried skin of Goji berries or the size reduced pieces thereof obtained in step a) with a solvent selected from the group consisting of ethyl acetate, hexane, heptane, petroleum ether, acetone, butane, ethyl methyl ketone, methanol, propan-2-ol and mixtures thereof; and c) removing the solvent from the extracts obtained in step b); and d) optionally cleaving the esters in the dried extracts obtained in step c); and e) optionally crystallizing the dried extracts obtained in step c) or d) in an aliphatic straight or branched CH alcohol. Preferably the process consists only of the step a) to e) given above.
摘要翻译：制备含有玉米黄质和/或其酯的枸杞浆果皮提取物的方法包括以下步骤：a）获得枸杞干燥的皮肤或其尺寸减小的片; 以及b）用选自乙酸乙酯，己烷，庚烷，石油醚，丙酮，丁烷，乙基甲基酮，甲醇的溶剂萃取步骤a）中获得的枸杞干燥的干燥皮肤或其尺寸减小的片，丙-2-醇及其混合物; 和c）从步骤b）中获得的提取物中除去溶剂; 和d）任选地将步骤c）中获得的干燥提取物中的酯切割; 和e）任选地将步骤c）或d）中获得的干燥提取物结晶在脂族直链或支链CH醇中。优选地，该方法仅由上述步骤a）至e）组成。

3. 发明申请

WO2007017168A1 PROCESS FOR THE PREPARATION OF UBIHYDROQUINONES AND UBIQUINONES 审中-公开
标题翻译：制备UBIHYDROQUINONES和UBIQUINONES的方法
公开(公告)号：WO2007017168A1
公开(公告)日：2007-02-15
申请号：PCT/EP2006/007645
申请日：2006-08-02
申请人： DSM IP ASSETS B.V. , AQUINO, Fabrice , BONRATH, Werner , BOHRER, Patrick , HUGENTOBLER, Max , NETSCHER, Thomas , RADSPIELER, Alexander
发明人： AQUINO, Fabrice , BONRATH, Werner , BOHRER, Patrick , HUGENTOBLER, Max , NETSCHER, Thomas , RADSPIELER, Alexander
IPC分类号： C07C46/06 , C07C50/28 , C07C41/30 , C07C43/23
CPC分类号： C07C46/02 , C07C41/30 , C07C50/28 , C07C43/215 , C07C43/23
摘要： A process for the preparation of ubihydroquinones and ubiquinones by condensation of a prenol or isoprenol with a hydroquinone or derivative thereof in the presence of 0.005 - 1.0 mol% of a catalyst which is a Broensted-acid, a Lewis-acid from the group consisting of a derivative of Bi or In or an element of group 3 of the periodic table of the elements, a heteropolyacid, an NH- or a CH-acidic compound, and optionally oxidizing the ubihydroquinone obtained.
摘要翻译：一种在0.005-1.0摩尔％的催化剂（Broensted-acid），路易斯酸（Lewis酸）的存在下，由Prenol或异戊二烯醇与氢醌或其衍生物缩合制备二氢醌和泛醌的方法， Bi或In的衍生物或元素周期表第3族的元素，杂多酸，NH-或CH-酸性化合物，以及任选地氧化所获得的二氢醌。

4. 发明申请

WO2012025591A1 PROCESS FOR THE MANUFACTURE OF A HIGHLY ENRICHED EXTRACT CONTAINING ZEAXANTHIN AND/OR ITS ESTERS 审中-公开
标题翻译：含有高锰酸盐和/或其酯的高效提取物的制备方法
公开(公告)号：WO2012025591A1
公开(公告)日：2012-03-01
申请号：PCT/EP2011/064630
申请日：2011-08-25
申请人： DSM IP Assets B.V. , BUSS, Axel , HUGENTOBLER, Max
发明人： BUSS, Axel , HUGENTOBLER, Max
IPC分类号： C09B61/00 , A23L1/275 , A23L1/30 , A61K31/07
CPC分类号： C09B61/00 , A23L5/44 , A23L33/105
摘要： The present invention is directed to a process for the manufacture of an extract of Goji berries containing zeaxanthin and/or its esters, comprising the following steps: a) obtaining reduced sized pieces of dried Goji berries; and b) extracting the smaller Goji berries obtained in step a) with a solvent selected from the group consisting of ethyl acetate, hexane, heptane, petroleum ether and mixtures thereof; and c) removing the solvent from the extracts obtained in step b); and d) optionally cleaving the esters in the dried extracts obtained in step c); and e) crystallizing the dried extracts obtained in step c) or d) in an aliphatic straight or branched C 1-4 alcohol. Preferably the process according to the present invention consists only of the steps a) to e) given above.
摘要翻译：本发明涉及一种制备含有玉米黄质和/或其酯的枸杞浆果提取物的方法，包括以下步骤：a）获得减小尺寸的干枸杞子片; 和b）用选自乙酸乙酯，己烷，庚烷，石油醚及其混合物的溶剂萃取步骤a）中获得的较小的枸杞浆果; 和c）从步骤b）中获得的提取物中除去溶剂; 和d）任选地将步骤c）中获得的干燥提取物中的酯切割; 和e）使步骤c）或d）中获得的干燥提取物在脂肪族直链或支链C 1-4醇中结晶。优选地，根据本发明的方法仅由上述步骤a）至e）组成。

5. 发明申请

WO2010079123A2 PROCESS FOR RESVERATROL INTERMEDIATE 审中-公开
标题翻译： RESVERATROL INTERMEDIATE过程
公开(公告)号：WO2010079123A2
公开(公告)日：2010-07-15
申请号：PCT/EP2010/000021
申请日：2010-01-06
申请人： DSM IP ASSETS B.V. , BONRATH, Werner , LETINOIS, Ulla , HUGENTOBLER, Max , KARGE, Reinhard , LEHMANN, Hajo
发明人： BONRATH, Werner , LETINOIS, Ulla , HUGENTOBLER, Max , KARGE, Reinhard , LEHMANN, Hajo
IPC分类号： C07C39/215 , C07C69/017 , C07C67/28
CPC分类号： C07C67/29 , C07C69/017 , C07C69/18
摘要： A process for the preparation of 1-(3,5-diacetoxyphenyl)-ethanol by catalytic hydrogenation of 3,5-diacetoxy-acetophenone in the presence of a Ni-alloy as catalyst in a C 1-3 -carboxylic acid ester as solvent.
摘要翻译：在作为溶剂的C 3-羧酸酯中的Ni合金作为催化剂存在下，通过3,5-二乙酰氧基 - 苯乙酮的催化氢化制备1-（3,5-二乙酰氧基苯基） - 乙醇的方法。

6. 发明申请

WO2007128574A1 PROCESS FOR THE PREPARATION OF ASTAXANTHIN 审中-公开
标题翻译：制备ASTAXANTHIN的方法
公开(公告)号：WO2007128574A1
公开(公告)日：2007-11-15
申请号：PCT/EP2007/004071
申请日：2007-05-08
申请人： DSM IP ASSETS B.V. , BERG, Michael , ESSL, Stefan , HUGENTOBLER, Max
发明人： BERG, Michael , ESSL, Stefan , HUGENTOBLER, Max
IPC分类号： C07C403/24
CPC分类号： C07C403/24
摘要： The invention therefore relates to a process for the preparation of astaxanthin of the formula I by reacting 2 mol of the triphenylphosphonium salt of the general formula II in which X represents chlorine, bromine or the (HSO 4 ) radical, preferably bromine, in a Wittig reaction with one mol of the C 10 -dialdehyde of the formula III which is characterized in that a) the starting compounds of the formulae II and III are taken up in a solvent, the mixture is cooled to a temperature of not more than 10°C, preferably -18°C to +5°C, b) about 0.9 to 1.5, preferably 0.9 to 1.2, mol of a base per mole of triphenylphosphonium salt are added to the resulting reaction mixture at a temperature of not more than 10°C, preferably -18°C to +5°C, c) the base is metered and mixed in over a predetermined reaction time T so that at least a ½ base equivalent is added to the reaction mixture continuously or quasicontinuously within a timespan T'
摘要翻译：因此，本发明涉及通过使2摩尔通式II的三苯基鏻盐（其中X表示氯，溴或（HSO 4））基团，制备式I的虾青素的方法，优选溴，在与一摩尔式III的C 10-20二甲醛的Wittig反应中，其特征在于a）将式II和III的起始化合物溶于溶剂，将混合物冷却至不高于10℃，优选-18℃至+ 5℃的温度，b）加入每摩尔三苯基鏻盐约0.9至1.5摩尔，优选0.9至1.2摩尔的碱在不高于10℃，优选-18℃至+ 5℃的温度下将所得反应混合物加入到所得反应混合物中，c）将碱在预定的反应时间T内进行计量和混合，使得至少1/2碱基当量在时间段T'<3T内连续或准连续加入到反应混合物中，剩余的碱在剩余的反应时间内。

7. 发明申请

WO2011032936A1 NITROOXYESTERS, THEIR PREPARATION AND USE 审中-公开
标题翻译：硝酸盐，他们的制备和使用
公开(公告)号：WO2011032936A1
公开(公告)日：2011-03-24
申请号：PCT/EP2010/063462
申请日：2010-09-14
申请人： DSM IP ASSETS B.V. , HUGENTOBLER, Max , RUF, Steffen , WUESTENBERG, Bettina
发明人： HUGENTOBLER, Max , RUF, Steffen , WUESTENBERG, Bettina
IPC分类号： C07C203/04 , C10L1/22
CPC分类号： C07C203/04 , C10L1/238
摘要： The present invention relates to the novel compounds of the formula (I), as well as to their manufacture and use and compositions comprising them. The invention also relates to a change in oxidation reactions of hydrocarbons admixed to these compounds. Furthermore the invention relates to (bio)diesel fuel comprising such compounds.
摘要翻译：本发明涉及式（I）的新化合物及其制备和用途以及包含它们的组合物。本发明还涉及与这些化合物混合的烃的氧化反应的变化。此外，本发明涉及包含这种化合物的（生物）柴油燃料。

8. 发明申请

WO2009112506A1 NOVEL USE OF CAROTENOID (ESTER)S 审中-公开
标题翻译： CARETENOID（ESTER）的新用途
公开(公告)号：WO2009112506A1
公开(公告)日：2009-09-17
申请号：PCT/EP2009/052826
申请日：2009-03-11
申请人： DSM IP ASSETS B.V. , HUGENTOBLER, Max , RUF, Steffen , WUESTENBERG, Bettina
发明人： HUGENTOBLER, Max , RUF, Steffen , WUESTENBERG, Bettina
IPC分类号： C10L1/19 , C10L1/182 , C10L1/18 , C10L3/00 , C10L1/14 , C10L10/02 , C10L9/10
CPC分类号： C10L1/1826 , C10L1/14 , C10L1/1608 , C10L1/1811 , C10L1/183 , C10L1/1852 , C10L1/1881 , C10L1/19 , C10L1/191 , C10L1/223 , C10L1/231 , C10L1/232 , C10L1/2456 , C10L1/2641 , C10L10/02
摘要： The present invention relates to a composition comprising a) a substance selected from the group of astaxanthinmonoalkanoylesters, astaxanthindialkanoylesters, isozeaxanthin, isozeaxanthinmonoalkanoylesters, isozeaxanthindialkanoylesters and mixtures thereof; and b) a substance selected from the group of alkyl nitrates, nitrooxy esters of alkoxy substituted aliphatic alcohols and organic peroxides; as well as to a change in oxidation reactions of hydrocarbons, especially fuels, admixed to these compositions. The invention also relates to a composition comprising a) a compound selected from the group consisting of astaxanthinmonoalkanoylesters, astaxanthindialkanoylesters, iso-zeaxanthin, iso-zeaxanthinmonoalkanoylesters, iso¬ zeaxanthindialkanoylesters and mixtures thereof; and c) a fuel. Furthermore, the present invention relates to a composition comprising a) a compound selected from the group consisting of astaxanthinmonoalkanoylesters, astaxanthindialkanoylesters, isozeaxanthin, isozeaxanthinmonoalkanoylesters, isozeaxanthindialkanoylesters and mixtures thereof; and b) a compound selected from the group of alkyl nitrates, nitrooxy esters of alkoxy substituted aliphatic alcohols, organic peroxides and mixtures thereof; and d) a stabilizing compound; and e) optionally a solvent.
摘要翻译：本发明涉及一种组合物，该组合物包含：a）选自虾青素单烷基酯，虾青素烷基酯，亚甲基黄豆蛋白，异山莨菪碱单烷酰基酯，异葎草酮烷酰基酯及其混合物的物质; 和b）选自硝酸烷基酯，烷氧基取代的脂族醇的硝基氧基酯和有机过氧化物的物质; 以及与这些组合物混合的烃，特别是燃料的氧化反应的变化。本发明还涉及一种组合物，其包含a）选自虾青素单烷酰基酯，虾青素烷基酯，异玉米黄质，异玉米黄质单烷酰基酯，异葎草酮烷酰基酯及其混合物的化合物; 和c）燃料。此外，本发明涉及一种组合物，其包含：a）选自虾青素单烷基酯，虾青素烷基酯，次黄豆蛋白，异山莨菪碱单烷酰基酯，异葎草酮烷酰基酯及其混合物的化合物; 和b）选自硝酸烷基酯，烷氧基取代的脂族醇的硝基氧基酯，有机过氧化物及其混合物的化合物; 和d）稳定化合物; 和e）任选的溶剂。

9. 发明授权

EP1915333B1 PROCESS FOR THE PREPARATION OF UBIHYDROQUINONES AND UBIQUINONES 有权
标题翻译：工艺用于生产和UBIHYDROCHINONEN泛醌
公开(公告)号：EP1915333B1
公开(公告)日：2015-06-03
申请号：EP06776559.4
申请日：2006-08-02
申请人： DSM IP Assets B.V.
发明人： AQUINO, Fabrice , BONRATH, Werner , BOHRER, Patrick , HUGENTOBLER, Max , NETSCHER, Thomas , RADSPIELER, Alexander
IPC分类号： C07C46/02 , C07C46/06 , C07C50/28 , C07C41/30 , C07C43/23
CPC分类号： C07C46/02 , C07C41/30 , C07C50/28 , C07C43/215 , C07C43/23

10. 发明公开

EP2373611A2 PROCESS FOR RESVERATROL INTERMEDIATE 审中-公开
标题翻译：方法，产生中间白藜芦醇
公开(公告)号：EP2373611A2
公开(公告)日：2011-10-12
申请号：EP10700481.4
申请日：2010-01-06
申请人： DSM IP Assets B.V.
发明人： BONRATH, Werner , LETINOIS, Ulla , HUGENTOBLER, Max , KARGE, Reinhard , LEHMANN, Hajo
IPC分类号： C07C69/157 , C07C67/29
CPC分类号： C07C67/29 , C07C69/017 , C07C69/18
摘要： A process for the preparation of 1-(3,5-diacetoxyphenyl)-ethanol by catalytic hydrogenation of 3,5-diacetoxy-acetophenone in the presence of a Ni-alloy as catalyst in a C
1-3 -carboxylic acid ester as solvent.

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