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1. 发明申请

WO2012034869A1 PROCESS FOR PRODUCING POLYETHYLENE WITH IMPROVED HOMOGENEITY 审中-公开
标题翻译：生产具有改善的均匀性的聚乙烯的方法
公开(公告)号：WO2012034869A1
公开(公告)日：2012-03-22
申请号：PCT/EP2011/065135
申请日：2011-09-01
申请人： BOREALIS AG , LENTZAKIS, Helen , LYLYKANGAS, Mikko , BERGSTRA, Michiel , VAHTERI, Markku , AHO, Jani
发明人： LENTZAKIS, Helen , LYLYKANGAS, Mikko , BERGSTRA, Michiel , VAHTERI, Markku , AHO, Jani
IPC分类号： C08F10/02
CPC分类号： C08F210/16 , C08F10/00 , C08F2/001 , C08F210/08 , C08F2500/01 , C08F2500/05 , C08F2500/08 , C08F2500/12 , C08F2500/26 , C08F2500/02 , C08F2500/07 , C08F4/6555 , C08F4/6492
摘要： Process for producing polyethylene compositions, like LLDPE, MDPE or HDPE, with a high level of homogeneity which comprises the steps of a) preactivating the total amount of a Ziegler-Natta procatalyst with the total amount of a cocatalyst, which cocatalyst comprises an organoaluminium compound, in order to get a preactivated Ziegler-Natta catalyst system, b) introducing the preactivated Ziegler-Natta catalyst system into a prepolymerisation reactor, wherein the preactivated Ziegler-Natta catalyst system is prepolymerised with at least one C 2 -C 10 -alpha-olefin monomer and optionally one or more C 3 -C 10 -alpha- olefin comonomer, in order to get a prepolymerisation product, c) introducing the prepolymerisation product into a first polymerisation reactor, which comprises a slurry reactor, wherein the prepolymerisation product is further polymerised with ethylene monomers and optionally one or more C 3 -C 10 -alpha-olefin comonomers in order to get a first polymerisation product, d) introducing the first polymerisation product into a second polymerisation reactor, wherein the first polymerisation product is further polymerised with ethylene monomers and optionally one or more C 3 to C 10 -alpha-olefin comonomers in order to get a second polymerisation product, e) optionally performing one or two subsequent polymerisation steps in order to get a third or fourth polymerisation product, f) further processing the obtained polymerisation product into pellets by extrusion; its use for forming articles, especially films with a low gel content.
摘要翻译：用于生产具有高水平均匀性的聚乙烯组合物如LLDPE，MDPE或HDPE的方法，其包括以下步骤：a）预先活化齐格勒 - 纳塔前催化剂的总量与助催化剂的总量，该助催化剂包含有机铝化合物，以便获得预活化的齐格勒 - 纳塔催化剂体系，b）将预活化的齐格勒 - 纳塔催化剂体系引入预聚合反应器，其中预活化的齐格勒 - 纳塔催化剂体系与至少一种C2-C10-α-烯烃单体和任选的一种或多种C 3 -C 10-α-烯烃共聚单体，以获得预聚合产物，c）将预聚合产物引入第一聚合反应器，该反应器包括浆料反应器，其中预聚合产物进一步与乙烯单体和任选的一种或多种C 3 -C 10-α-烯烃共聚单体，以获得第一聚合产物，d）引入t 他将第一聚合产物转化成第二聚合反应器，其中第一聚合产物进一步与乙烯单体和任选的一种或多种C 3 -C 10-α-烯烃共聚单体聚合，以获得第二聚合产物，e）任选地进行一个或两个随后的聚合步骤以获得第三或第四聚合产物，f）通过挤出将所得聚合产物进一步加工成颗粒; 其用于形成制品，特别是具有低凝胶含量的膜。

2. 发明申请

WO2011058091A1 PROCESS FOR OLEFIN POLYMERIZATION 审中-公开
标题翻译：烯烃聚合方法
公开(公告)号：WO2011058091A1
公开(公告)日：2011-05-19
申请号：PCT/EP2010/067268
申请日：2010-11-11
申请人： BOREALIS AG , AUMO, Jeannette , MATIKAINEN, Pasi , BARTKE, Michael , ELOVIRTA, Tom , VIJAY, Sameer , LYLYKANGAS, Mikko , ELO, Pertti , HUHTANEN, Lauri
发明人： AUMO, Jeannette , MATIKAINEN, Pasi , BARTKE, Michael , ELOVIRTA, Tom , VIJAY, Sameer , LYLYKANGAS, Mikko , ELO, Pertti , HUHTANEN, Lauri
IPC分类号： C08F10/00 , C08F4/659
CPC分类号： C08F10/00 , C08F110/06 , C08F2410/01 , C08F4/65912 , C08F4/65927 , C08F2/00 , C08F2500/12 , C08F4/6492
摘要： The present invention aims to provide a process for polymerizing at least one olefin in the presence of a polymerization catalyst comprising the steps of: (A) continuously introducing a first liquid comprising a transition metal compound, an organometallic compound of a metal of Group 13 of Periodic System of Elements and a solvent, and a second liquid which together with said first liquid is capable of forming an emulsion, into an emulsification stage to produce an emulsion comprising said first liquid dispersed in said second liquid; (B) continuously withdrawing an emulsion stream from said emulsification stage and directing it into a solidification stage to form a slurry comprising a solid polymerization catalyst component comprising said transition metal compound and said organometallic compound suspended in said second liquid; (C) continuously recovering said solid polymerization catalyst component from said solidification stage; (D) directing said solid polymerization catalyst component into a first prepolymerization stage together with a monomer and an amount of second liquid wherein the monomer is prepolymerized onto said solid polymerization catalyst component so that the ratio of the weight of the polymer to the weight of said solid polymerization catalyst component is from 0.1:1 to 20:1 to form a slurry of a prepolymerized solid polymerization catalyst component suspended in said second liquid; (E) recovering said prepolymerized solid polymerization catalyst component from said first prepolymerization stage; (F) continuously introducing said prepolymerized solid polymerization catalyst component into a second prepolymerization stage together with an olefin monomer to form a prepolymerized catalyst comprising in average 100 to 1000 g of polymer per 1 gram of said solid polymerization catalyst component; (G) continuously withdrawing said prepolymerized catalyst from said second prepolymerization stage and directing it into a subsequent polymerization stage together with at least one olefin monomer to effect polymerization of the at least one olefin monomer in the presence of said prepolymerized catalyst. The polymerization process produces polymers in high yield. The morphology of the polymer powder is good and the amount of fine particle polymer is low. The process can be operated for long a long period in a stable manner.
摘要翻译：本发明的目的在于提供一种在聚合催化剂存在下聚合至少一种烯烃的方法，包括以下步骤：（A）连续引入包含过渡金属化合物的第一液体，第13族金属的有机金属化合物元素周期性系统和溶剂，以及与所述第一液体一起能够形成乳液的第二液体进入乳化阶段以产生包含分散在所述第二液体中的所述第一液体的乳液; （B）从所述乳化阶段连续抽出乳液流并将其导入固化阶段以形成包含悬浮在所述第二液体中的包含所述过渡金属化合物和所述有机金属化合物的固体聚合催化剂组分的浆料; （C）从所述固化阶段连续回收所述固体聚合催化剂组分; （D）将所述固体聚合催化剂组分与单体和一定量的第二液体一起引导到第一预聚合阶段，其中所述单体预聚合到所述固体聚合催化剂组分上，使得所述聚合物的重量与所述固体聚合催化剂组分为0.1:1至20:1，以形成悬浮在所述第二液体中的预聚合固体聚合催化剂组分的浆液; （E）从所述第一预聚合阶段回收所述预聚固体聚合催化剂组分; （F）将所述预聚合的固体聚合催化剂组分连同烯烃单体一起连续引入第二预聚合阶段，以形成预聚合的催化剂，每克所述固体聚合催化剂组分平均含有100至1000克聚合物; （G）从所述第二预聚合阶段连续地抽出所述预聚合催化剂，并将其引导至随后的聚合阶段与至少一种烯烃单体，以在所述预聚合的催化剂存在下进行至少一种烯烃单体的聚合。聚合过程以高产率生产聚合物。聚合物粉末的形态好，微粒聚合物的量低。该方法可以长时间稳定运行。

3. 发明申请

WO2011058089A1 PROCESS FOR PRODUCING A POLYMERIZATION CATALYST 审中-公开
标题翻译：制备聚合催化剂的方法
公开(公告)号：WO2011058089A1
公开(公告)日：2011-05-19
申请号：PCT/EP2010/067266
申请日：2010-11-11
申请人： BOREALIS AG , VIJAY, Sameer , RÄSÄNEN, Jukka , LYLYKANGAS, Mikko
发明人： VIJAY, Sameer , RÄSÄNEN, Jukka , LYLYKANGAS, Mikko
IPC分类号： C08F4/00 , C08F110/06 , C08F4/6592 , C08F6/00 , B01J37/00
CPC分类号： C08F10/06 , B01J31/143 , B01J31/1608 , B01J31/2295 , B01J37/0072 , B01J37/009 , B01J2531/94 , C07C17/38 , C07C17/383 , C08F4/65912 , C08F6/02 , C08F110/06 , C08L23/10 , C08F4/00 , C08F4/65927 , C08F2500/12
摘要： The present invention aims to provide a process for producing a solid polymerization catalyst component comprising the steps of (A) withdrawing a mixed stream comprising the solid polymerization catalyst component and a mixture of a first liquid comprising a hydrocarbon or halogenated hydrocarbon solvent and a second liquid comprising a liquid capable of forming an emulsion with said first liquid from a catalyst preparation stage; (B) separating said mixed stream into a liquid stream comprising a majority of said mixture of said first liquid and said second liquid and a product stream comprising a majority of said solid polymerization catalyst component; (C) dividing said liquid stream into a first liquid stream comprising a majority of said first liquid and a second liquid stream comprising a majority of said second liquid; (D) forming a purified second liquid stream and a disposable stream; and (E) returning at least a part of said purified second liquid stream into said catalyst preparation stage. The process offers an economical and environmentally attractive method of producing the solid catalyst component. The catalyst is active in polymerization and can be used in industrial processes.
摘要翻译：本发明的目的在于提供一种制备固体聚合催化剂组分的方法，包括以下步骤：（A）将包含固体聚合催化剂组分的混合物和包含烃或卤代烃溶剂的第一液体和第二液体包括能够从催化剂制备阶段与所述第一液体形成乳液的液体; （B）将所述混合物流分离成包含大部分所述第一液体和所述第二液体的所述混合物的液体物流和包含大部分所述固体聚合催化剂组分的产物流; （C）将所述液体流分成包含大部分所述第一液体的第一液体流和包含大部分所述第二液体的第二液体流; （D）形成纯化的第二液体流和一次性流; 和（E）将至少一部分纯化的第二液体物流返回到催化剂制备阶段。该方法提供了生产固体催化剂组分的经济且环境友好的方法。催化剂在聚合反应中有活性，可用于工业过程。

4. 发明申请

WO2007132060A2 FERTILIZER GRANULES AND MANUFACTURING PROCESS THEREOF 审中-公开
标题翻译：肥料颗粒及其制造方法
公开(公告)号：WO2007132060A2
公开(公告)日：2007-11-22
申请号：PCT/FI2007/000134
申请日：2007-05-16
申请人： KEMIRA GROWHOW OYJ , HERO, Heikki , LYLYKANGAS, Mikko
发明人： HERO, Heikki , LYLYKANGAS, Mikko
CPC分类号： C05G3/0088 , C05C1/02 , C05G3/0058 , C05C5/02 , C05C9/00 , C05D9/00
摘要： The invention relates to a fertilizer granule comprising both a nitrate and urea as the main nitrogen source. A mineral added during production is an important component in the composition, said mineral stabilizing these otherwise poorly compatible nitrogen compounds. A high nitrogen content is thus attained with ammonium nitrate concentrations falling below maximum limit values set by international legislation and classification, while at the same time the explosion risk particularly associated with the use of ammonium nitrate is avoided. The invention is also directed to a process for the production of the fertilizer granule of the above type, said process resulting in a fertilizer granule with excellent resistance properties and a high nitrogen content, wherein said granule may be coated by methods typical in the art, if desired.
摘要翻译：本发明涉及包含硝酸盐和尿素作为主要氮源的肥料颗粒。在生产过程中添加的矿物质是组合物中的重要成分，所述矿物稳定化这些其他相容不足的氮化合物。因此，通过国际立法和分类确定的硝酸铵浓度低于最大极限值，从而达到高氮含量，同时避免了与使用硝酸铵特别相关的爆炸危险。本发明还涉及一种生产上述类型的肥料颗粒的方法，所述方法产生具有优异的耐性和高氮含量的肥料颗粒，其中所述颗粒可以通过本领域常规方法进行包衣，如果需要的话。

5. 发明申请

WO2006090007A3 AMMONIUM NITRATE GRANULE AND METHOD FOR THE PREPERATION OF THE SAME 审中-公开
公开(公告)号：WO2006090007A3
公开(公告)日：2006-08-31
申请号：PCT/FI2006/000073
申请日：2006-02-24
申请人： KEMIRA GROWHOW OYJ , LYLYKANGAS, Mikko , KIISKI, Harri , POUKARI, Juhani , MILBORNE, Robert, John
发明人： LYLYKANGAS, Mikko , KIISKI, Harri , POUKARI, Juhani , MILBORNE, Robert, John
IPC分类号： C05C1/02 , C05G1/00
摘要： The invention relates to a fertilizer granule containing ammonium nitrate, comprising a core containing ammonium nitrate and a coating layer containing calcium sulphate. The coating layer consists of a mixture containing calcium sulphate and ammonium nitrate. Such a fertilizer granule is preferably produced by contacting the core with an aqueous ammonium nitrate solution and solid calcium sulphate particles, either as a slurry or separately. The production of the fertilizer granule is safe and easy.

6. 发明申请

WO2022111966A1 CATALYST FEED SYSTEM 审中-公开
公开(公告)号：WO2022111966A1
公开(公告)日：2022-06-02
申请号：PCT/EP2021/080598
申请日：2021-11-04
申请人： BOREALIS AG
发明人： NYFORS, Klaus , KIVELÄ, Jouni , SATTAR, Mubashar , ZITTING, Samuli , ELOVAINIO, Erno , LYLYKANGAS, Mikko , LINDHOLM, Jan , COX, Danny
IPC分类号： B01J8/00
摘要： The present invention relates to a process for feeding a polymerization catalyst into a polymerization reactor, said process comprising the steps of: (i) forming a catalyst slurry comprising oil and a solid catalyst component in a first catalyst preparation vessel; (ii) transferring the catalyst slurry from the first catalyst preparation vessel to a first catalyst feed vessel; (iii) maintaining the catalyst slurry in the first catalyst feed vessel in a homogeneous state; (iv) withdrawing a portion of the catalyst slurry from the first catalyst feed vessel, preferably continuously withdrawing the catalyst slurry from the first catalyst feed vessel, and introducing the withdrawn portion of the catalyst slurry into a polymerization reactor; wherein the oil has a dynamic viscosity of from 25 to 1500 mPa*s at the conditions within the first catalyst preparation vessel and the first catalyst feed vessel, wherein the catalyst slurry is transferred along a substantially vertical path downwards from the first catalyst feed vessel to the reactor.

7. 发明申请

WO2023031201A1 GAS PHASE POLYMERIZATION PROCESS WITH IMPROVED GAS RECYCLING 审中-公开
公开(公告)号：WO2023031201A1
公开(公告)日：2023-03-09
申请号：PCT/EP2022/074089
申请日：2022-08-30
申请人： BOREALIS AG
发明人： KUUSISTO, Mika , ZITTING, Samuli , ELOVAINIO, Erno , LYLYKANGAS, Mikko , MATIKAINEN, Pasi
IPC分类号： B01J8/18 , B01J8/24 , B01J19/18 , C08F10/00 , C08F8/00
摘要： A gas phase polymerization assembly comprising a gas phase polymerization reactor having at least one inlet and at least one outlet, a circulation gas compression unit having an inlet and an outlet, whereby the inlet of the circulation gas compression unit is fluidly connected to the at least one outlet of the gas phase polymerization reactor by an unreacted gas line; a flush gas compression unit having an inlet and an outlet, wherein the inlet of the flush gas compression unit is fluidly connected to the outlet of the circulation gas compression unit by a pressurized unreacted gas line; a circulation line fluidly connecting the pressurized unreacted gas line with the at least one inlet of the gas phase polymerization reactor; a flush gas withdrawal line connected to the outlet of the flush gas compression unit.

8. 发明申请

WO2013075808A1 METHOD FOR RECOVERING POLYMER AND APPARATUS THEREFOR 审中-公开
标题翻译：用于回收聚合物及其装置的方法
公开(公告)号：WO2013075808A1
公开(公告)日：2013-05-30
申请号：PCT/EP2012/004779
申请日：2012-11-16
申请人： BOREALIS AG
发明人： NYFORS, Klaus , ÄÄRILÄ, Jari , HÄTÖNEN, Jari , ANDTSJÖ, Henrik , JOHANSSON, Eira , LYLYKANGAS, Mikko
IPC分类号： B01J8/18 , B01J8/00 , C08F10/00 , C08F2/34
CPC分类号： C08F2/01 , B01J8/003 , B01J8/005 , B01J8/1809 , B01J2208/00548 , B01J2208/0061 , B01J2208/00761 , B01J2219/00247 , B01J2219/00254 , C08F2/34 , C08F10/00 , C08J11/04 , Y10S526/92 , C08F110/06 , C08F2500/12 , C08F210/16 , C08F210/08
摘要： Process and apparatus for recovering polymer from a a gas phase reactor having a distribution plate via an outlet vessel comprising at least one apparatus for the breakup of polymeric agglomerates, the apparatus further comprising a feed pipe connecting the gas phase reactor and the outlet vessel a return gas line connecting the gas phase reactor and the outlet vessel, means for varying the flow rate through the return gas line from the outlet vessel to the gas phase reactor, and means for varying the outlet rate of polymer product from the outlet vessel.
摘要翻译：用于从具有分布板的气相反应器中回收聚合物的方法和装置，所述气相反应器具有经由出口容器的出口容器，所述出口容器包括至少一种用于分解聚合物附聚物的装置，该装置还包括将气相反应器和出口容器连接的回流气体连接气相反应器和出口容器的管线，用于改变通过从出口容器到气相反应器的回气管线的流速的装置，以及用于改变聚合物产物从出口容器的出口速率的装置。

9. 发明公开

EP2499173A1 PROCESS FOR OLEFIN POLYMERIZATION 有权
标题翻译：程序烯烃聚合
公开(公告)号：EP2499173A1
公开(公告)日：2012-09-19
申请号：EP10776683.4
申请日：2010-11-11
申请人： Borealis AG
发明人： AUMO, Jeannette , MATIKAINEN, Pasi , BARTKE, Michael , ELOVIRTA, Tom , VIJAY, Sameer , LYLYKANGAS, Mikko , ELO, Pertti , HUHTANEN, Lauri
IPC分类号： C08F10/00 , C08F4/659
CPC分类号： C08F10/00 , C08F110/06 , C08F2410/01 , C08F4/65912 , C08F4/65927 , C08F2/00 , C08F2500/12 , C08F4/6492
摘要： The present invention aims to provide a process for polymerizing at least one olefin in the presence of a polymerization catalyst comprising the steps of: (A) continuously introducing a first liquid comprising a transition metal compound, an organometallic compound of a metal of Group 13 of Periodic System of Elements and a solvent, and a second liquid which together with said first liquid is capable of forming an emulsion, into an emulsification stage to produce an emulsion comprising said first liquid dispersed in said second liquid; (B) continuously withdrawing an emulsion stream from said emulsification stage and directing it into a solidification stage to form a slurry comprising a solid polymerization catalyst component comprising said transition metal compound and said organometallic compound suspended in said second liquid; (C) continuously recovering said solid polymerization catalyst component from said solidification stage; (D) directing said solid polymerization catalyst component into a first prepolymerization stage together with a monomer and an amount of second liquid wherein the monomer is prepolymerized onto said solid polymerization catalyst component so that the ratio of the weight of the polymer to the weight of said solid polymerization catalyst component is from 0.1:1 to 20:1 to form a slurry of a prepolymerized solid polymerization catalyst component suspended in said second liquid; (E) recovering said prepolymerized solid polymerization catalyst component from said first prepolymerization stage; (F) continuously introducing said prepolymerized solid polymerization catalyst component into a second prepolymerization stage together with an olefin monomer to form a prepolymerized catalyst comprising in average 100 to 1000 g of polymer per 1 gram of said solid polymerization catalyst component; (G) continuously withdrawing said prepolymerized catalyst from said second prepolymerization stage and directing it into a subsequent polymerization stage together with at least one olefin monomer to effect polymerization of the at least one olefin monomer in the presence of said prepolymerized catalyst. The polymerization process produces polymers in high yield. The morphology of the polymer powder is good and the amount of fine particle polymer is low. The process can be operated for long a long period in a stable manner.

10. 发明公开

EP4251312A1 CATALYST FEED SYSTEM 审中-实审
公开(公告)号：EP4251312A1
公开(公告)日：2023-10-04
申请号：EP21801944.6
申请日：2021-11-04
申请人： Borealis AG
发明人： NYFORS, Klaus , KIVELÄ, Jouni , SATTAR, Mubashar , ZITTING, Samuli , ELOVAINIO, Erno , LYLYKANGAS, Mikko , LINDHOLM, Jan , COX, Danny
IPC分类号： B01J8/00

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