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1. 发明申请

WO2012104858A1 ONLINE ANALYSIS METHOD FOR CRUDE OILS USING SPECTROSCOPY 审中-公开
标题翻译：使用光谱法分析原油的在线分析方法
公开(公告)号：WO2012104858A1
公开(公告)日：2012-08-09
申请号：PCT/IN2011/000222
申请日：2011-03-30
申请人： RELIANCE INDUSTRIES LTD. , HARENDER, Bisht , NISHA, Preschilla , CHANDRA, Saravanan , SUKUMAR, Mandal , ASIT, Das
发明人： HARENDER, Bisht , NISHA, Preschilla , CHANDRA, Saravanan , SUKUMAR, Mandal , ASIT, Das
IPC分类号： G01N21/35
CPC分类号： G01N33/2823 , G01N21/3577
摘要： An improved method for online IR analysis of hydrocarbon mixture, particularly crude oil is provided for determining its several physico-chemical properties, wherein the oil sample is diluted with IR transparent solvent, particularly carbon tetrachloride and IR absorption is evaluated. The invention uses a method wherein sample cells of less than 0.2mm can be utilized and full IR spectrum from 800 cm -1 to 400 cm -1 can be used for predicting the properties of oil.
摘要翻译：提供了一种用于烃混合物，特别是原油的在线IR分析的改进方法，用于确定其几种物理化学性质，其中用IR透明溶剂，特别是四氯化碳稀释油样品并评估IR吸收。本发明使用其中可以使用小于0.2mm的样品池的方法，并且可以使用800cm -1至400cm -1的全部IR光谱来预测油的性质。

2. 发明申请

WO2013011517A1 FCC CATALYST ADDITIVE AND PREPARATION METHOD THEREOF 审中-公开
标题翻译： FCC催化剂及其制备方法
公开(公告)号：WO2013011517A1
公开(公告)日：2013-01-24
申请号：PCT/IN2011/000599
申请日：2011-09-02
申请人： RELIANCE INDUSTRIES LTD. , GOPAL, Ravichandran , PRAVEEN, Kumar, Chinthala , TEJAS, Doshi , ARUN, Kumar, D. , AMIT, Gohel , SUKUMAR, Mandal , ASIT, Kumar, Das , SRIKANTA, Dinda , AMITKUMAR, Parekh
发明人： GOPAL, Ravichandran , PRAVEEN, Kumar, Chinthala , TEJAS, Doshi , ARUN, Kumar, D. , AMIT, Gohel , SUKUMAR, Mandal , ASIT, Kumar, Das , SRIKANTA, Dinda , AMITKUMAR, Parekh
IPC分类号： B01J29/82 , C10G11/02 , B01J37/00
CPC分类号： B01J29/40 , B01J29/06 , B01J29/08 , B01J29/084 , B01J29/18 , B01J29/7007 , B01J29/80 , B01J35/0006 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J37/0045 , B01J37/10 , B01J2229/186 , B01J2229/36 , B01J2229/42 , C10G11/05 , C10G11/18 , C10G2300/104 , C10G2300/1044
摘要： The present invention relates to a Fluid Catalytic Cracking (FCC) additive and its preparation process. The FCC additive has high efficiency in the production of light olefins C2, C3 and C4 hydrocarbons, especially propylene. The present invention discloses the stabilization of medium pore zeolite especially ZSM-5 using optimum phosphate salts at a pH in the range of 7-9 with synergetic combination of silica rich binder to produce FCC additive with excellent stability under severe hydrothermal conditions.
摘要翻译：本发明涉及流化催化裂化（FCC）添加剂及其制备方法。 FCC添加剂在轻质烯烃C2，C3和C4烃，特别是丙烯的生产中具有高效率。本发明公开了使用最佳磷酸盐在7-9的pH范围内稳定中孔沸石，特别是ZSM-5，与富二氧化硅粘合剂的协同组合产生FCC添加剂，并在严苛的水热条件下具有优异的稳定性。

3. 发明申请

US20110240523A1 FLUID CATALYTIC CRACKING (FCC) PROCESS FOR MANUFACTURING PROPYLENE AND ETHYLENE IN INCREASED YIELD 有权
标题翻译：流化床催化裂化（FCC）在增加乙烯和乙烯中制备丙烯和乙烯的方法
公开(公告)号：US20110240523A1
公开(公告)日：2011-10-06
申请号：US13133759
申请日：2009-12-08
申请人： Sukumar Mandal , Asit Kumar Das , Ashwani Yadav , Manoj Yadav , Akhilesh Bhatnagar , Rajeshwar Dongara , Veera Venkata satya Bhaskara sita Rama Murthy Katravulapalli
发明人： Sukumar Mandal , Asit Kumar Das , Ashwani Yadav , Manoj Yadav , Akhilesh Bhatnagar , Rajeshwar Dongara , Veera Venkata satya Bhaskara sita Rama Murthy Katravulapalli
IPC分类号： C10G11/04
CPC分类号： C10G11/18 , C10G11/05 , C10G2400/20
摘要： A fluid catalytic cracking (FCC) process for manufacturing propylene and ethylene in increased yield. The process comprises cracking an olefinic naphtha stream and main hydrocarbon stock in combination with an olefinic C4 hydrocarbon stream in different zones of one or more risers of an FCC unit. Each FCC riser comprises an acceleration zone at the lower portion thereof, a lift stream feed nozzle at the bottom of the acceleration zone, a main hydrocarbon stock feed nozzle above the acceleration zone and an olefinic naphtha feed nozzle at a location along the acceleration zone between the lift stream feed nozzle and main hydrocarbon stock feed nozzle. The cracking is carried out on a mixed FCC catalyst comprising at least 2 percent by weight pentasil zeolite and at least 10 percent by weight Y-zeolite. The catalyst is injected at the bottom of each FCC riser, the olefinic naptha is injected through the olefinic feed nozzle, the main hydrocarbon stock is injected through the main hydrocarbon stock feed nozzle and the lift stream is injected through the lift stream feed nozzle at the bottom of the acceleration zone. The lift stream comprises the olefinic C4 hydrocarbon stream with or without steam and/or a fuel gas. The olefinic C4 hydrocarbon steam is cracked in the acceleration zone at 600 to 8000° C. and pressure of 0.8 to 5 kg/cm up 2 (gauge) and weight hourly space velocity (WHSV) of 0.2 to 100 hr up 1 and vapour residence time of 0.2 to 5 seconds.
摘要翻译：用于以增加的产率制造丙烯和乙烯的流化催化裂化（FCC）方法。该方法包括在FCC单元的一个或多个立管的不同区域中与烯属烃石脑油流和主要烃类物料一起裂化。每个FCC提升管包括其下部的加速区，加速区底部的升力流进料喷嘴，加速区上方的主烃储料供给喷嘴和沿加速区的位置处的烯烃石脑油进料喷嘴，升降机进料喷嘴和主油料进料喷嘴。裂化在包含至少2重量百分比的pentasil沸石和至少10重量％Y-沸石的混合FCC催化剂上进行。在每个FCC提升管的底部注入催化剂，通过烯烃进料喷嘴注入烯烃萘，主要烃类原料通过主要烃类原料进料喷嘴注入，提升流通过提升料流进料喷嘴注入底部的加速区。提升流包括具有或不具有蒸汽和/或燃料气体的烯烃C4烃流。烯烃C4烃蒸汽在600-8000℃的加速区裂化，压力为0.8-5kg / cm 2（表压），重时空速（WHSV）为0.2〜100小时-1，蒸汽停留时间为0.2〜5秒。

4. 发明授权

US06613710B2 Process for preparation of bi-functional fluid catalytic cracking catalyst composition 失效
公开(公告)号：US06613710B2
公开(公告)日：2003-09-02
申请号：US09961384
申请日：2001-09-25
申请人： Sanjay Kumar Ray , Mohan Prabhu Kuvettu , Venkatchalam Krishnan , Gopal Ravichandran , Kamlesh Gupta , Sukumar Mandal , Satish Makhija , Sobhan Ghosh , Arumugam Velayutham Karthikeyani , Mitra Bhanu Patel
发明人： Sanjay Kumar Ray , Mohan Prabhu Kuvettu , Venkatchalam Krishnan , Gopal Ravichandran , Kamlesh Gupta , Sukumar Mandal , Satish Makhija , Sobhan Ghosh , Arumugam Velayutham Karthikeyani , Mitra Bhanu Patel
IPC分类号： B01J2116
CPC分类号： B01J37/0045 , B01J21/04 , B01J21/16 , B01J29/40 , B01J29/7007 , B01J35/002 , B01J2229/42 , C10G11/05
摘要： A process for preparing bi-functional catalyst for Fluid Catalytic Cracking (FCC), that comprises molecular sieves, modified clay and semi-basic alumina and the catalyst for highly effective cracking of high boiling petroleum feedstock to provide simultaneously, enhanced yields of Liquefied Petroleum Gas (LPG) and reduction of undesirable bottoms.

5. 发明授权

US06267873B1 Fluidized catalytic cracking process 有权
标题翻译：流化催化裂化工艺
公开(公告)号：US06267873B1
公开(公告)日：2001-07-31
申请号：US09201896
申请日：1998-11-30
申请人： Asit Kumar Das , Debasis Bhattacharyya , Sukumar Mandal , Vutukuru Lakshmi Narasimha Murthy , Sanjeev Singh , Marri Rama Rao , Sobhan Ghosh
发明人： Asit Kumar Das , Debasis Bhattacharyya , Sukumar Mandal , Vutukuru Lakshmi Narasimha Murthy , Sanjeev Singh , Marri Rama Rao , Sobhan Ghosh
IPC分类号： C10G1100
CPC分类号： C10G11/187 , C10G11/18 , Y10S585/91
摘要： A fluidized catalytic cracking process for catalytically cracking a feed to lighter products includes introducing a heated catalyst and the feed into a bottom riser of a fluidized catalytic cracking apparatus and allowing the heated catalyst and the feed to preaccelerate upwardly within the bottom riser as a mixture; flowing the mixture upwardly from the bottom riser through a plurality of microriser tubes disposed within a regenerator under conditions effective to cause a cracking reaction of the hydrocarbons and result in a mixture including coked catalyst and hydrocarbon vapors; passing the mixture from the microriser tubes through a catalyst separator for separating the coked catalyst from the hydrocarbon vapors; collecting coked catalyst in a stripper for stripping out hydrocarbon vapors carried along with the coked catalyst and introducing the coked catalyst collected into a regenerator; simultaneous with flowing the mixture, combusting the coked catalyst within the regenerator under conditions effective to cause regeneration of the catalyst so that hot regenerated catalyst is produced and heat transferred to the microriser tubes; introducing the hot regenerated catalyst from the regenerator into the bottom riser for facilitating continuous operation; and directing hydrocarbon vapors from the catalyst separator and from the stripper to a fractionator for separation of products.
摘要翻译：将进料催化裂化成较轻产物的流化催化裂化方法包括将加热的催化剂和进料引入流化催化裂化装置的底部提升管中，并允许加热的催化剂和进料作为混合物在底部提升管内向前预加速; 在有效引起烃的裂解反应并产生包括焦化催化剂和烃蒸汽的混合物的条件下，将混合物从底部提升管向上流过设置在再生器内的多个微型管; 将混合物从微循环管通过催化剂分离器，用于将焦化的催化剂与烃蒸气分离; 在汽提器中收集焦化的催化剂，用于汽提与焦炭催化剂一起携带的烃蒸气并将收集的焦化催化剂引入再生器中; 同时使混合物流动，在有效使催化剂再生的条件下在再生器内燃烧焦化催化剂，使得产生热再生催化剂并将热量传递至微型管; 将热再生催化剂从再生器引入底部提升管，以便于连续操作; 并将碳氢化合物蒸汽从催化剂分离器和汽提器引导至用于分离产物的分馏器。

6. 发明授权

US5846402A Process for catalytic cracking of petroleum based feed stocks 失效
标题翻译：石油基原料催化裂化工艺
公开(公告)号：US5846402A
公开(公告)日：1998-12-08
申请号：US855946
申请日：1997-05-14
申请人： Sukumar Mandal , Suresh Kumarshah , Debasis Bhattacharyya , Vutukuru Lakshmi Narasimha Murthy , Asit Kumar Das , Sanjeev Singh , Ram Mohan Thakur , Shankar Sharma , Jagdev Kumar Dixit , Sobhan Ghosh , Satyen Kumar Das , Manoranjan Santra , Latoor Lal Saroya , Marri Rama Rao , Ganga Shanker Mishra , Satish Makhija
发明人： Sukumar Mandal , Suresh Kumarshah , Debasis Bhattacharyya , Vutukuru Lakshmi Narasimha Murthy , Asit Kumar Das , Sanjeev Singh , Ram Mohan Thakur , Shankar Sharma , Jagdev Kumar Dixit , Sobhan Ghosh , Satyen Kumar Das , Manoranjan Santra , Latoor Lal Saroya , Marri Rama Rao , Ganga Shanker Mishra , Satish Makhija
IPC分类号： B01J29/80 , C10G11/05 , C10G11/18 , C10G11/00
CPC分类号： B01J29/80 , C10G2400/20 , C10G2400/28
摘要： A process for selective catalytic cracking of a petroleum-based feedstock to produce a product having a high yield of liquified petroleum gas (LPG) and light olefins having 3 to 4 carbons includes providing a fluidized bed reactor which is a high velocity riser, continuously circulating fluidized bed reactor; providing a solid acidic catalyst comprised of: from 1 to 6% by wt. of ultra stable Y-zeolite; from 8-25% by wt. of Pentasil zeolite which is shape selective; from 0-8% by wt. of an active material which is bottom selective; from 0-1% by wt. of rare earth constituents; and from 91 to 60% by wt. of nonacidic constituents and binder; charging the fluidized bed reactor with the solid acidic catalyst and the petroleum-based feedstock; and cracking the petroleum-based feedstock in the presence of the solid acidic catalyst in the fluidized bed reactor. The reactor is operated at a Weight Hourly Space Velocity (WHSV) ranging from 40 to 120 hr.sup.-1, a ratio of solid acidic catalyst to petroleum-based feedstock ranging from 15 to 25, a temperature at the top of the high velocity riser ranging from 530.degree. C. to 600.degree. C., recycled riser products ranging from 0 to 40%, a pressure in the fluidized bed reactor ranging from 1.0 to 4.0 kg/cm.sup.2 g, and an amount of steam for dilution and quenching of hydrocarbons ranging from 3 to 50 wt. % of the petroleum-based feedstock. The Pentasil zeolite has a pore size ranging from 5 to 6 .ANG. so that the catalyst is highly selective for LPG and C.sub.4 light olefins with minimum dry gas and coke make, and so that the vanadium tolerance of the catalyst is increased and ranges up to 21,000 PPM. The process produces a LPG yield ranging up to 40 to 65 wt. % of the fresh petroleum-based feedstock, a selectivity for the light olefins of at least 40 wt. %, and a selectivity for the LPG of at least 45 wt.
摘要翻译：选择性催化裂化石油基原料以生产具有高产率的液化石油气（LPG）和具有3至4个碳原子的轻质烯烃的产物的方法包括提供流化床反应器，其为高速提升管，连续循环流化床反应器; 提供固体酸性催化剂，其包含：1至6重量％的超稳定Y型沸石; 8-25重量％。具有形状选择性的pentasil沸石; 0-8重量％的底部选择性活性物质; 0-1重量％的稀土成分; 和91〜60重量％。的非酸成分和粘合剂; 用固体酸性催化剂和石油基原料装入流化床反应器; 并在流化床反应器中在固体酸性催化剂存在下裂化石油基原料。反应器以40至120小时-1的重量小时空间速度（WHSV）运行，固体酸性催化剂与石油基原料的比例为15至25，高速提升管顶部的温度范围从530℃至600℃，循环的提升产品的范围为0至40％，流化床反应器的压力范围为1.0至4.0kg / cm2g，以及用于稀释和猝灭烃的蒸汽量 3〜50重量％％的石油基原料。 Pentasil沸石的孔径范围为5至6安格姆，使得催化剂对于具有最少干燥气体和焦炭的LPG和C4轻质烯烃具有高选择性，并且使得催化剂的耐钒性增加并且范围高达21,000 PPM。该方法产生高达40至65重量％的LPG产率。％的新鲜石油基原料，轻质烯烃的选择性至少为40wt。％，并且LPG的选择性至少为45wt。

7. 发明授权

US09446384B2 Adiabatic regeneration of sulfur capturing adsorbents 有权
标题翻译：硫捕获吸附剂的绝热再生
公开(公告)号：US09446384B2
公开(公告)日：2016-09-20
申请号：US13982862
申请日：2011-12-14
申请人： Asit Das , Ajay Gupta , Bharat Kumar Vaja , Govind Tulsi , Harender Bisht , Jeyavel Sinha , Shubhangi Jagutse , Sukumar Mandal
发明人： Asit Das , Ajay Gupta , Bharat Kumar Vaja , Govind Tulsi , Harender Bisht , Jeyavel Sinha , Shubhangi Jagutse , Sukumar Mandal
IPC分类号： B01J20/34 , C10G25/12
CPC分类号： B01J20/3466 , B01J20/3433 , B01J20/3458 , C10G25/12 , C10G2300/202 , C10G2300/807
摘要： The present invention provides a process for regeneration of the sulfur capturing spent adsorbents after sulfur capturing using a hydrolyzing agent under adiabatic conditions. In accordance with the process of the present invention hydrolyzing agent is introduced to the spent adsorbent in a controlled manner such that the exothermic heat generated within the adsorbent bed does not rise above the predetermined temperature limit.
摘要翻译：本发明提供一种在绝热条件下使用水解剂硫捕集后的硫捕获废吸附剂的再生方法。根据本发明的方法，以受控的方式将水解剂引入废吸附剂，使得在吸附床内产生的放热不会升高到预定温度极限以上。

8. 发明授权

US07462275B2 Process for conversion of hydrocarbons to saturated LPG and high octane gasoline 有权
标题翻译：将碳氢化合物转化为饱和LPG和高辛烷值汽油的方法
公开(公告)号：US07462275B2
公开(公告)日：2008-12-09
申请号：US10894341
申请日：2004-07-20
申请人： Asit Kumar Das , Debasis Bhattacharyya , Gadari Saidulu , Satayen Kumar Das , Bandaru Venkata Hari P. Gupta , Ramakrishnan Ramanarayanan , Latoor Lal Saroya , Konduri Lakshminarayana , Marri Rama Rao , Vinod Ramchandra Upadhyay , Sukumar Mandal , Deepa Meghavathu , Arumugam Velayutham Karthikeyani , Wadharwa Ram Kalsi , Arvind Pratap Singh , Veena Bansal , Ashok Kumar Tiwari , Venkatachalam Krishnan , Satish Makhija , Sobhan Ghosh , Niranjan Raghunath Raje
发明人： Asit Kumar Das , Debasis Bhattacharyya , Gadari Saidulu , Satayen Kumar Das , Bandaru Venkata Hari P. Gupta , Ramakrishnan Ramanarayanan , Latoor Lal Saroya , Konduri Lakshminarayana , Marri Rama Rao , Vinod Ramchandra Upadhyay , Sukumar Mandal , Deepa Meghavathu , Arumugam Velayutham Karthikeyani , Wadharwa Ram Kalsi , Arvind Pratap Singh , Veena Bansal , Ashok Kumar Tiwari , Venkatachalam Krishnan , Satish Makhija , Sobhan Ghosh , Niranjan Raghunath Raje
IPC分类号： C10G67/00
CPC分类号： C10G11/05 , C10G2400/28
摘要： The present invention relates to a process for the conversion of hydrocarbon streams with 95% true boiling point less than 400° C. to very high yield of liquefied petroleum gas in the range of 45-65 wt % of feed and high octane gasoline, the said process comprises catalytic cracking of the hydrocarbons using a solid fluidizable catalyst comprising a medium pore crystalline alumino-silicates with or without Y-zeolite, non crystalline acidic materials or combinations thereof in a fluidized dense bed reactor operating at a temperature range of 400 to 550° C., pressure range of 2 to 20 kg/cm2 (g) and weight hourly space velocity in range of 0.1 to 20 hour−1, wherein the said dense bed reactor is in flow communication to a catalyst stripper and a regenerator for continuous regeneration of the coked catalyst in presence of air and or oxygen containing gases, the catalyst being continuously circulated between the reactor-regenerator system.
摘要翻译：本发明涉及一种将95％真实沸点低于400℃的烃流转化成非常高产率的进料和高辛烷值汽油的45-65重量％的液化石油气的方法，所述方法包括使用固体可流化催化剂催化裂化烃，所述固体可流化催化剂包含具有或不具有Y-沸石的中孔结晶铝硅酸盐，非结晶酸性物质或其组合，其在400至550℃的温度范围内操作的流化密床反应器 ℃，压力范围为2至20kg / cm2（g）和0.1至20小时-1范围内的重时空速，其中所述致密床反应器与用于连续的催化剂汽提塔和再生器流动连通在存在空气和/或含氧气体的情况下再生焦化的催化剂，催化剂在反应器 - 再生器系统之间连续循环。

9. 发明申请

US20060096890A1 Resid cracking apparatus with catalyst and adsorbent regenerators and a process thereof 有权
公开(公告)号：US20060096890A1
公开(公告)日：2006-05-11
申请号：US11266233
申请日：2005-11-04
申请人： Kawliwal Pankaj , Rama Marri , Dixit Kumar , Saroya Lal , Sukumar Mandal , Satish Makhija , Sobhan Ghosh
发明人： Kawliwal Pankaj , Rama Marri , Dixit Kumar , Saroya Lal , Sukumar Mandal , Satish Makhija , Sobhan Ghosh
IPC分类号： C10G11/00
CPC分类号： C10G55/06 , C10G11/18 , C10G25/05 , C10G25/08
摘要： This invention provides a resid cracking apparatus comprising a riser, reactor, stripper cum separator with adjustable outlets in flow communication with adsorbent and catalyst regenerators for converting hydrocarbon residues containing higher concentration of conradson carbon content, poisonous metals such as nickel & vanadium and basic nitrogen etc., into lighter and valuable products and a process thereof.

10. 发明授权

US06540904B1 Process for the upgradation of petroleum residue 有权
标题翻译：石油残渣升级过程
公开(公告)号：US06540904B1
公开(公告)日：2003-04-01
申请号：US09518413
申请日：2000-03-03
申请人： Suhas Ranjan Gun , Priya Bandhu Chowdhury , Kashi Nath Bhattacharya , Achinta Kumar Roy , Umanand Sharma , Swapan Kumar Ghosh , Awadhesh Kumar Sinha , Santosh Kumar Chanda , Sukumar Mandal , Sanjay Kumar Ray , Asit Kumar Das , Satish Makhija , Sobhan Ghosh , Akhilesh Kumar Bhatnagar
发明人： Suhas Ranjan Gun , Priya Bandhu Chowdhury , Kashi Nath Bhattacharya , Achinta Kumar Roy , Umanand Sharma , Swapan Kumar Ghosh , Awadhesh Kumar Sinha , Santosh Kumar Chanda , Sukumar Mandal , Sanjay Kumar Ray , Asit Kumar Das , Satish Makhija , Sobhan Ghosh , Akhilesh Kumar Bhatnagar
IPC分类号： C10G1102
CPC分类号： C10G11/02 , C10G2300/107
摘要： The present invention provides a process for the upgradation of petroleum residue into useful fractions by subjecting petroleum residue in the presence of a solvent and ferrous sulphate catalyst to a pressure in the range of 10 atm. to 120 atm., temperature in the range of 380-420° C., for a period in the range of 0-120 minutes, in a reactor vessel, in an inert atmosphere. The charge is then cooled to room temperature and the product gas released through scrubbers. The residue is re-heated, if required, for free flow of liquid product. The resulting liquid product is distilled to obtain useful fractions.
摘要翻译：本发明提供了一种通过在溶剂和硫酸亚铁催化剂存在下将石油残余物在10atm范围内的压力下将石油残渣升级为有用级分的方法。温度在380-420℃的范围内，在0-120分钟的时间内，在反应器容器中，在惰性气氛中。然后将电荷冷却至室温，并通过洗涤器释放产物气体。如果需要，残余物被重新加热，用于液体产品的自由流动。将所得液体产物蒸馏以获得有用的级分。

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