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1. 发明授权

US5612442A Phenol novolak condensate and bis(methoxymethyl)biphenyl for production thereof 失效
标题翻译：苯酚酚醛清漆缩合物和双（甲氧基甲基）联苯等
公开(公告)号：US5612442A
公开(公告)日：1997-03-18
申请号：US530735
申请日：1995-09-19
申请人： Katuhiko Okazaki , Mikito Kashima , Yumiki Noda , Hiroshi Jibiki , Takashi Honma
发明人： Katuhiko Okazaki , Mikito Kashima , Yumiki Noda , Hiroshi Jibiki , Takashi Honma
IPC分类号： C07C39/15 , C08G8/08 , C08G59/08 , C08L63/00 , C08G65/38
CPC分类号： C08L63/00 , C07C39/15 , C08G59/08 , C08G8/08
摘要： A bis(methoxymethyl)biphenyl having the formula (I): ##STR1## which is capable of producing by a dehalogenating coupling of a halogenated methoxymethylbenzene and which is useful as an intermediate for a phenol novolak condensate, an epoxy resin curing agent, an epoxy resin composition, or a phenol resin composition.
摘要翻译：具有式（I）的双（甲氧基甲基）联苯：其能够通过卤代甲氧基甲苯的脱卤耦合产生，可用作苯酚酚醛清漆缩合物的中间体，环氧树脂固化剂环氧树脂组合物或酚醛树脂组合物。

2. 发明授权

US4922010A Processes for preparing 2-substituted propionic acid and derivatives thereof 失效
标题翻译：制备2-取代的丙酸及其衍生物的方法
公开(公告)号：US4922010A
公开(公告)日：1990-05-01
申请号：US282024
申请日：1988-12-07
申请人： Mikito Kashima , Hideo Ishikawa , Kouichi Kashiwagi , Yumiki Noda
发明人： Mikito Kashima , Hideo Ishikawa , Kouichi Kashiwagi , Yumiki Noda
IPC分类号： C07C51/367 , C07C51/377 , C07C67/343
CPC分类号： C07C51/377 , C07C51/367 , C07C67/343
摘要： There are disclosed a process for preparing 2-hydroxy-2-(6-methoxy-2-naphthyl)propionic acid or 2-hydroxy-(4-substituted phenyl)propionic acid derivative which comprises reacting 2-methoxynaphthalene or substituted benzene derivatives with pyruvic acid in the presence of a Lewis acid and then, if necessary, hydrolyzing the obtained product, and a process for preparing 2-(6-methoxy-2-naphthyl)propionic acid or 2-(4-substituted phenyl)propionic acid derivative which comprises reducing 2-hydroxy-2-(6-methoxy-2-naphthyl)propionic acid or 2-hydroxy-2-(4-substituted phenyl)propionic acid derivative in a lower aliphatic acid in the presence of an inorganic acid under hydrogen atmosphere by using a metal catalyst.
摘要翻译：公开了2-羟基-2-（6-甲氧基-2-萘基）丙酸或2-羟基 - （4-取代苯基）丙酸衍生物的制备方法，该方法包括使2-甲氧基萘或取代的苯衍生物与丙酮酸反应在路易斯酸存在下，然后如果需要，水解所得产物，以及制备2-（6-甲氧基-2-萘基）丙酸或2-（4-取代苯基）丙酸衍生物的方法，其中包括在氢气氛下在无机酸存在下，在低级脂肪酸中还原2-羟基-2-（6-甲氧基-2-萘基）丙酸或2-羟基-2-（4-取代苯基）丙酸衍生物通过使用金属催化剂。

3. 发明授权

US4539423A Process for preparing diesters of malonic acid 失效
标题翻译：丙二酸二酯的制备方法
公开(公告)号：US4539423A
公开(公告)日：1985-09-03
申请号：US433045
申请日：1982-10-06
申请人： Hiroshi Itatani , Mikito Kashima , Tsutomu Suehiro
发明人： Hiroshi Itatani , Mikito Kashima , Tsutomu Suehiro
IPC分类号： B01J31/00 , C07B61/00 , C07C67/46 , C07C69/38 , C07C67/36
CPC分类号： C07C67/46
摘要： Disclosed is an improved process for preparing diesters of malonic acid by subjecting ketene, carbon monoxide and an ester of nitrous acid to a liquid phase reaction in an organic solvent, in which the reaction is carried out in the presence of a catalyst of a platinum group metal complex represented by the formula:L.sub.2 MX.sub.2wherein, L represents a ligand selected from the group consisting of triorganophosphines, triorganophosphite and triorganoarsines; M represents a platinum group metal; and X represents a halogen or an acetic acid ion.
摘要翻译：公开了一种通过使烯酮，一氧化碳和亚硝酸的酯在有机溶剂中进行液相反应来制备丙二酸二酯的改进方法，其中反应在铂族催化剂存在下进行由式L2MX2表示的金属络合物，其中L表示选自三有机膦，三有机亚磷酸酯和三有机锍的配体; M表示铂族金属; X表示卤素或乙酸离子。

4. 发明授权

US4180607A Epoxy resin composition and method for curing the epoxy resin composition 失效
标题翻译：环氧树脂组合物和环氧树脂组合物的固化方法
公开(公告)号：US4180607A
公开(公告)日：1979-12-25
申请号：US938526
申请日：1978-08-31
申请人： Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima
发明人： Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima
IPC分类号： C09D5/03 , C08G59/00 , C08G59/42
CPC分类号： C08G59/4223
摘要： Disclosed is an epoxy resin composition containing, as an essential curing component, 2,3,3',4'-biphenyltetracarboxylic dianhydride which is highly compatible with epoxy resins at a relatively low temperature and effective for producing cured epoxy resins having an excellent thermal resistance.
摘要翻译：公开了一种环氧树脂组合物，其包含作为必需固化组分的2,3,3'，4'-联苯四羧酸二酐，其在相对低的温度下与环氧树脂高度相容并且有效地制备具有优异耐热性的固化环氧树脂。

5. 发明授权

US4717494A Liquid thermal accumulator composition and thermal accumulation process 失效
标题翻译：液体蓄热器组成和热积累过程
公开(公告)号：US4717494A
公开(公告)日：1988-01-05
申请号：US878317
申请日：1986-06-25
申请人： Hiroshi Itatani , Mikito Kashima , Masami Aikawa
发明人： Hiroshi Itatani , Mikito Kashima , Masami Aikawa
IPC分类号： C09K5/00 , C09K5/06 , C09K5/08
CPC分类号： C09K5/063
摘要： A liquid thermal accumulator composition comprising a dicarboxylic acid anhydride, an alcohol and a monoester of the dicarboxylic acid and the alcohol. A process for accumulation of thermal energy utilizing said composition is also disclosed.
摘要翻译：一种液体蓄热器组合物，其包含二羧酸酐，醇和二羧酸的单酯和醇。还公开了利用所述组合物累积热能的方法。

6. 发明授权

US4048197A 2,3,3',4'-Biphenyltetracarboxylic acid dianhydride 失效
标题翻译： 2,3,3 {40,4 {40-联苯四羧酸二酐
公开(公告)号：US4048197A
公开(公告)日：1977-09-13
申请号：US597789
申请日：1975-07-21
申请人： Hiroshi Itatani , Mikito Kashima , Masaoki Matsuda , Hataaki Yoshimoto , Hiroyuki Yamamoto
发明人： Hiroshi Itatani , Mikito Kashima , Masaoki Matsuda , Hataaki Yoshimoto , Hiroyuki Yamamoto
IPC分类号： C07C51/09 , C07C51/265 , C07C51/27 , C07C51/573 , C07C67/343 , C07D307/89
CPC分类号： C07C51/573 , C07C51/09 , C07C51/265 , C07C51/27 , C07C67/343
摘要： A process for separating and purifying biphenyltetracarboxylic dianhydride isomers from a mixture of these isomers by fractional crystallization in aliphatic acid anhydrides or acetone. The isomeric mixture is obtained by heating biphenyltetracarboxylic acids, optionally in the presence of an aliphatic acid anhydride. The biphenyltetracarboxylic acids are obtained by oxidizing coupling dimers of o-xylene or by hydrolyzing coupling dimers of dimethyl phthalate. 2,3,3',4'-biphenyltetracarboxylic acid dianhydride which can be isolated from the above mixture can be used to form polyimide.
摘要翻译：通过在脂肪酸酐或丙酮中分级结晶从这些异构体的混合物中分离和纯化联苯四羧酸二酐异构体的方法。异构体混合物通过加热联苯四羧酸，任选在脂族酸酐存在下获得。联苯四羧酸是通过氧化邻二甲苯二聚体或通过水解邻苯二甲酸二甲酯的偶联二聚体得到的。可从上述混合物中分离的2,3,3'，4'-联苯四羧酸二酐可用于形成聚酰亚胺。

7. 发明授权

US4042603A Intramolecular cyclization in a fatty acid ester solvent 失效
标题翻译：脂肪酸酯溶剂中的分子内环化
公开(公告)号：US4042603A
公开(公告)日：1977-08-16
申请号：US559065
申请日：1975-03-17
申请人： Hiroshi Itatani , Mikito Kashima , Akinori Shiotani , Hataaki Yoshimoto , Tetuo Kato
发明人： Hiroshi Itatani , Mikito Kashima , Akinori Shiotani , Hataaki Yoshimoto , Tetuo Kato
IPC分类号： C07C69/017 , C07C45/00 , C07C49/587 , C07C49/675 , C07C49/697 , C07C67/00 , C07C69/92 , C07C201/00 , C07C205/45 , C07C253/00 , C07C255/56 , C07D307/91
CPC分类号： C07D307/91 , C07C201/12 , C07C205/45 , C07C45/67 , C07C49/675 , C07C49/697
摘要： A process for preparing substituted dibenzofuran or fluorenone-9 by the intramolecular cyclization of substituted diphenyl ether or benzophenone in the presence of a carboxylic acid salt of palladium and/or palladium organic complex.
摘要翻译：在钯和/或钯有机络合物的羧酸盐存在下，通过取代的二苯基醚或二苯甲酮的分子内环化制备取代的二苯并呋喃或芴酮-9的方法。

8. 发明授权

US4290936A Process for preparing polyimide solution 失效
标题翻译：制备聚酰亚胺溶液的方法
公开(公告)号：US4290936A
公开(公告)日：1981-09-22
申请号：US092508
申请日：1979-11-08
申请人： Yoshikazu Sasaki , Hiroshi Inoue , Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima
发明人： Yoshikazu Sasaki , Hiroshi Inoue , Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima
IPC分类号： C08G73/10 , C08K5/13
CPC分类号： C08G73/1028
摘要： A polyimide solution is prepared by a process wherein a tetracarboxylic acid ingredient containing at least about 80% by mole of 3,3',4,4'-biphenyltetracarboxylic acid or its functional derivative and an aromatic diamine ingredient containing at least about 50% by mole of 4,4'-diaminodiphenyl ether are polymerized at from about 100.degree. to 300.degree. C. in phenol or a halogenated phenolic compound; the amount of the acid and diamine ingredients being approximately equimolar to each other; whereby polymerization of the tetracarboxylic acid ingredient and the aromatic diamine ingredient is effected while being accompanied by imidation. Preferably, the polymerization accompanied by imidation is effected in a manner such that at least a second half of the polymerization is carried out in a closed reaction system. The resulting polyimide solution is suitable for making therefrom shaped articles, such as films, possessing excellent mechanical properties.
摘要翻译：通过以下方法制备聚酰亚胺溶液，其中含有至少约80摩尔％的3,3'，4,4'-联苯四羧酸或其官能衍生物的四羧酸成分和包含至少约50％的芳族二胺成分摩尔的4,4'-二氨基二苯醚在苯酚或卤化酚类化合物中在约100-300℃下聚合; 酸和二胺成分的量彼此近似等摩尔数; 从而在伴随着酰亚胺化的同时进行四羧酸成分和芳香族二胺成分的聚合。优选地，伴随着酰亚胺化的聚合以这样的方式进行，使得聚合的至少一半在闭合反应体系中进行。所得到的聚酰亚胺溶液适用于具有优异机械性能的成型制品如膜。

9. 发明授权

US4247443A Aromatic polyimide resin composition 失效
标题翻译：芳香族聚酰亚胺树脂组合物
公开(公告)号：US4247443A
公开(公告)日：1981-01-27
申请号：US67166
申请日：1979-08-16
申请人： Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima , Hataaki Yoshimoto , Shuji Yamamoto , Yoshikazu Sasaki
发明人： Ichiro Sasaki , Hiroshi Itatani , Mikito Kashima , Hataaki Yoshimoto , Shuji Yamamoto , Yoshikazu Sasaki
IPC分类号： C08J3/09 , C08K5/13
CPC分类号： C08J3/095 , C08J2379/08
摘要： An aromatic polyimide resin composition useful for producing a film or sheet, comprises 2% by weight or more of an imide polymer having at least 90 molar % of a recurring unit of the formula (I): ##STR1## wherein R' is a divalent aromatic radical, and dissolved in an organic polar solvent consisting essentially of one or more halogenated phenol compounds of the formulae (II) or (III): ##STR2## wherein R.sup.2 is a hydrogen atom of a C.sub.1-3 alkyl radical and is a halogen atom, the halogenated phenol compound having a melting point of 100.degree. C. or less and a boiling point of 300.degree. C. or less.
摘要翻译：可用于制备薄膜或片材的芳族聚酰亚胺树脂组合物包含2重量％或更多的具有至少90摩尔％的式（I）的重复单元的酰亚胺聚合物：其中R' 并且溶解在基本上由一种或多种式（II）或（III）的卤代酚化合物组成的有机极性溶剂中：其中R 2是氢原子为C1-3烷基，为卤素原子，该卤代酚化合物的熔点为100℃以下，沸点为300℃以下。

10. 发明授权

US06630561B2 Crystalline polyesterpolyol and hot-melt adhesive 失效
标题翻译：结晶聚酯多元醇和热熔胶
公开(公告)号：US06630561B2
公开(公告)日：2003-10-07
申请号：US09838036
申请日：2001-04-19
申请人： Mikito Kashima , Yumiki Noda , Harutoshi Hoshino , Toshikazu Machida , Hideki Ichihashi , Fumio Adachi , Yukio Kaneko
发明人： Mikito Kashima , Yumiki Noda , Harutoshi Hoshino , Toshikazu Machida , Hideki Ichihashi , Fumio Adachi , Yukio Kaneko
IPC分类号： C09J17506
CPC分类号： C09J175/06 , C08G18/4238 , Y10S528/905
摘要： A crystalline polyesterpolyol having a number average molecular weight of 1,500 to 15,000 and obtainable from a polybasic carboxylic acid component and an aliphatic hydrocarbon diol component comprising 1,10-decanediol and/or 1,12-dodecanediol, and a hot-melt adhesive comprising a reaction product of a polyisocyanate and a polyesterpolyol, which contains a crystalline polyesterpolyol having a number average molecular weight of 1,500 to 15,000 and obtainable from a polybasic carboxylic acid component and an aliphatic hydrocarbon diol component comprising 1,10-decanediol and/or 1,12-dodecanediol are provided.
摘要翻译：数均分子量为1500〜15000的结晶性聚酯多元醇，可由多元羧酸成分和含有1,10-癸二醇和/或1,12-十二烷二醇的脂肪族二醇成分得到，以及含有多异氰酸酯和聚酯多元醇的反应产物，其含有数均分子量为1,500至15,000的结晶聚酯多元醇，并且可由多元羧酸组分和包含1,10-癸二醇和/或12,12-癸二醇的脂族烃二醇组分获得提供了十二烷二醇。

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