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1. 发明授权

US5403801A Process for producing .epsilon.-caprolactam and activating solid catalysts therefor 失效
标题翻译：制备ε-己内酰胺和活化固体催化剂的方法
公开(公告)号：US5403801A
公开(公告)日：1995-04-04
申请号：US10791
申请日：1993-01-29
申请人： Masaru Kitamura , Hiroshi Ichihashi , Hideto Tojima
发明人： Masaru Kitamura , Hiroshi Ichihashi , Hideto Tojima
IPC分类号： B01J29/035 , B01J29/86 , B01J29/87 , B01J29/88 , B01J29/90 , B01J38/12 , B01J38/66 , C07D201/04 , B01J37/00 , B01J29/28
CPC分类号： B01J29/90 , B01J29/035 , B01J29/86 , B01J29/87 , B01J29/88 , B01J38/12 , B01J38/66 , C07D201/04 , Y02P20/52 , Y02P20/584
摘要： In the production of .epsilon.-caprolactam from cyclohexanon oxime in gaseous phase in the presence of solid catalysts, the catalysts, no matter whether they may have worked, are brought into contact with either aqueous solution of ammonium salts and at least one basic material or ammonia water.
摘要翻译：在固体催化剂存在下，在气相中从环己酮肟制备ε-己内酰胺时，催化剂无论是否可能已经起作用，都与铵盐水溶液和至少一种碱性物质或氨水。

2. 发明授权

US5071802A Regeneration of catalysts by burning in the presence of alcohols 失效
标题翻译：酒精存在催化剂的再生
公开(公告)号：US5071802A
公开(公告)日：1991-12-10
申请号：US489952
申请日：1990-03-07
申请人： Shinkichi Shimizu , Takayasu Niwa , Nobuyuki Abe , Masanori Doba , Akira Iguchi , Hiroshi Ichihashi , Masaru Kitamura
发明人： Shinkichi Shimizu , Takayasu Niwa , Nobuyuki Abe , Masanori Doba , Akira Iguchi , Hiroshi Ichihashi , Masaru Kitamura
IPC分类号： B01J23/90 , B01J29/90 , B01J38/52 , C07D201/04 , C07D213/10
CPC分类号： C07D213/10 , B01J23/90 , B01J29/90 , B01J38/52 , C07D201/04 , Y02P20/584
摘要： Carbonaceous materials deposited on solid catalysts and produced, for example, in Beckmann rearrangement in a gaseous phase are burned off by effecting the treatment in the presence of alcohols such as methanol or ethanol together with molecular oxygen-containing gas in order to regenerate the catalyst activity.

3. 发明授权

US4565801A Heteropoly-acids and their production and use 失效
标题翻译：杂多酸及其生产和使用
公开(公告)号：US4565801A
公开(公告)日：1986-01-21
申请号：US371223
申请日：1982-04-23
申请人： Shinkichi Shimizu , Hiroshi Ichihashi , Koichi Nagai
发明人： Shinkichi Shimizu , Hiroshi Ichihashi , Koichi Nagai
IPC分类号： C07C57/05 , B01J27/00 , B01J27/19 , B01J27/199 , C01B25/16 , C01B25/24 , C07C51/00 , C07C51/25 , C07C67/00 , B01J27/14
CPC分类号： C07C51/252 , B01J23/002 , B01J27/19 , B01J27/199 , C01B25/16 , B01J2523/00
摘要： A heteropoly-acid of the formula:H.sub.3+x (PMo.sub.12-x V.sub.x O.sub.40).nH.sub.2 Owherein x and n are numbers satisfying respectively the equations: 0.ltoreq.x.ltoreq.3 and n.ltoreq.6, and comprising phosphorus as the central atom and molybdenum or molybdenum and vanadium as the coordinating atoms, or its reduction-form product, which is in a cubic crystal structure having diffraction lines at lattice spacings (d) of at least 8.4, 6.8, 5.9, 4.8, 4.2 and 3.4 in the X-ray powder diffraction. The heteropoly-acid is useful as a catalyst, especially as a catalyst in the production of methacrylic acid by the gas-phase catalytic oxidation of methacrolein.
摘要翻译：具有下式的杂多酸：H3 + x（PMo12-xVxO40）·nH2O其中x和n分别满足等式：0≤x≤3和n≤6，并且包含磷作为中心原子和钼或钼和钒作为配位原子，或其还原形式的产物，其在晶格间距（d）处具有至少8.4,6.8,5.9,4.8,4.2和3.4的衍射线的立方晶体结构在X射线粉末衍射中。杂多酸可用作催化剂，特别是通过甲基丙烯醛的气相催化氧化生产甲基丙烯酸时的催化剂。

4. 发明授权

US4010238A Proces for selective removal of nitrogen oxides from waste gases 失效
标题翻译：处理从废气中选择性除去氮氧化物的程序
公开(公告)号：US4010238A
公开(公告)日：1977-03-01
申请号：US452659
申请日：1974-03-19
申请人： Tatsuo Shiraishi , Shinkichi Shimizu , Hiroshi Ichihashi , Tadashi Shindo
发明人： Tatsuo Shiraishi , Shinkichi Shimizu , Hiroshi Ichihashi , Tadashi Shindo
IPC分类号： B01D53/94 , B01J23/22 , B01J23/26 , B01J23/84 , B01J23/847 , B01J27/198 , B01J27/199 , B01J8/00 , C01B21/00
CPC分类号： B01J23/8472 , B01D53/9418 , B01J23/22 , B01J23/26 , B01D2251/2062 , B01D2255/20707 , B01D2255/20723 , B01D2255/20738 , B01D2255/20746 , B01D2255/20753 , B01D2255/20761 , B01D2255/20784 , B01D2255/2094
摘要： A process for the selective removal of nitrogen oxides from waste gases containing nitrogen oxides, which comprises contacting the waste gases with a metal oxide catalyst having the following formula:V.sub.x A.sub.y O.sub.zwherein V is vanadium; A is at least one element selected from the group consisting of copper, zinc, tin, lead, titanium, phosphorus, chromium, iron, cobalt and nickel; x and y are each a numeral of 0.5 to 12; and z is a numeral of 1 to 60, at a temperature of 150.degree. to 800.degree. C in the presence of ammonia.
摘要翻译：一种用于从含有氮氧化物的废气中选择性除去氮氧化物的方法，其包括使废气与具有下式的金属氧化物催化剂接触：

5. 发明申请

US20070198005A1 Coagulating cutter 有权
标题翻译：凝结切割机
公开(公告)号：US20070198005A1
公开(公告)日：2007-08-23
申请号：US11359535
申请日：2006-02-22
申请人： Hiroshi Ichihashi , Ryoji Sakai , Masaru Imoto , Masami Oshida , Katsumi Sasaki
发明人： Hiroshi Ichihashi , Ryoji Sakai , Masaru Imoto , Masami Oshida , Katsumi Sasaki
IPC分类号： A61B18/04
CPC分类号： A61B17/320092 , A61B18/1445
摘要： A coagulating cutter according to the present invention comprises: a transmitting member for transmitting energy, for treating living body tissue, to the living body tissue; an outer sheath through which the transmitting member is passed; and a grasping section supported at the tip end portion of the outer sheath so as to be capable of turning with respect to the transmitting member, which allows the living body tissue to be grasped against the transmitting member. With such an arrangement, upon turning the grasping section toward the transmitting member to be in a closed state, the faces of the transmitting member and the grasping section, which face each other, provide a contact portion, where the transmitting member and the grasping section are in contact with each other over a predetermined length, for incising the living body tissue grasped between the transmitting member and the grasping section, and a non-contact portion, where the transmitting member and the grasping section are provided with a predetermined interval on both sides of the axis extending in the direction of the predetermined length of the contact portion so as not to be in contact with each other, for coagulating the living body tissue.
摘要翻译：根据本发明的凝结切割机包括：传送部件，用于将生物体组织的能量传递给生物体组织; 传递构件通过的外护套; 以及抓握部，其支撑在所述外护套的前端部，以能够相对于所述传递部件转动，所述抓持部使得所述生物体组织能够抵靠所述传递部件。通过这样的布置，当将把持部朝向传递部件转动到关闭状态时，传递部件和把持部分彼此面对的面设置有接触部分，在该接触部分处，传递部件和把持部分彼此接触预定长度，用于切割夹持在传递部件和把持部之间的生物体组织和非接触部分，其中传递部件和把持部分在两者上设置有预定间隔所述轴线沿着所述接触部分的预定长度的方向延伸以不彼此接触，以使所述生物体组织凝结。

6. 发明授权

US06531595B2 Method for producing &egr;-caprolactam and reactor for the method 失效
标题翻译：用于该方法生产ε-己内酰胺和反应器的方法
公开(公告)号：US06531595B2
公开(公告)日：2003-03-11
申请号：US09963603
申请日：2001-09-27
申请人： Wolfgang F. Hölderich , Gerd Dahlhoff , Hiroshi Ichihashi , Keisuke Sugita
发明人： Wolfgang F. Hölderich , Gerd Dahlhoff , Hiroshi Ichihashi , Keisuke Sugita
IPC分类号： C07D20104
CPC分类号： C07D201/04
摘要： A method is provided for producing &egr;-caprolactam from cyclohexanone oxime by using a zeolite or non-zeolitic material as a catalyst under gas phase reaction conditions. The method comprises a reaction step converting cyclohexanone oxime into &egr;-caprolactam in the presence of the zeolite or non-zeolitic material; and a regeneration step of treating the zeolite or non-zeolitic material with a non-oxidizing gas at a temperature of from about 100°C. to about 600° C.
摘要翻译：提供了一种通过在气相反应条件下使用沸石或非沸石材料作为催化剂从环己酮肟生产ε-己内酰胺的方法。该方法包括在沸石或非沸石材料存在下将环己酮肟转化成ε-己内酰胺的反应步骤; 以及在约100℃的温度下用非氧化性气体处理沸石或非沸石材料的再生步骤。至约600℃

7. 发明授权

US06482945B2 Process for producing epsilon-caprolactam and apparatus for the process 失效
标题翻译：用于生产ε-己内酰胺的方法和该方法的装置
公开(公告)号：US06482945B2
公开(公告)日：2002-11-19
申请号：US09964424
申请日：2001-09-28
申请人： Wolfgang F. Hölderich , Gerd Dahlhoff , Andre Sbresny , Hiroshi Ichihashi
发明人： Wolfgang F. Hölderich , Gerd Dahlhoff , Andre Sbresny , Hiroshi Ichihashi
IPC分类号： C07D20104
CPC分类号： C07D201/06 , C07D201/04
摘要： A process is provided for producing &egr;-caprolactam from cyclohexanone oxime. The process comprises a evaporation step of a mixture of cyclohexanone oxime and a solvent by introducing the mixture into a fluidized bed in which inert particles is fluidized by an inert gas, the particles having heat enough to evaporate the mixture; and a rearrangement step of cyclohexanone oxime in the evaporated mixture into &egr;-caprolactam by a gas phase Beckmann rearrangement reaction using a solid catalyst, excluding a catalyst consisting of a boric acid or a boron oxide.
摘要翻译：提供了从环己酮肟生产ε-己内酰胺的方法。该方法包括通过将混合物引入流化床中的环己酮肟和溶剂的混合物的蒸发步骤，其中惰性颗粒通过惰性气体流化，该颗粒具有足以蒸发混合物的热量; 和通过使用固体催化剂的气相贝克曼重排反应将蒸发的混合物中的环己酮肟重排成ε-己内酰胺，不包括由硼酸或氧化硼组成的催化剂。

8. 发明授权

US4992252A Method for production of hydroxylammonium salt 失效
标题翻译：羟基铵盐的生产方法
公开(公告)号：US4992252A
公开(公告)日：1991-02-12
申请号：US446665
申请日：1989-12-06
申请人： Hiroshi Ichihashi , Kikuo Takeda , Hiroshi Yoshioka
发明人： Hiroshi Ichihashi , Kikuo Takeda , Hiroshi Yoshioka
IPC分类号： C01C1/00 , B01J23/42 , B01J27/02 , C01B21/14
CPC分类号： C01B21/1418 , B01J23/42
摘要： A process for producing hydroxylammonium salts of hydrogenating nitrogen monoxide in an acidic medium in the presence of a catalyst which is prepared by subjecting a platinum compound to a first reductive treatment with a thiosulfate or a thiosulfate combined with an alkali metal sulfide in the presence of a catalyst carrier, and a second reductive treatment with a reductant selected from the group consisting of formic acid, hydrogen, hydrazine and sodium borohydride at a temperature of 50.degree. C. to 150.degree. C.

9. 发明授权

US4665274A Method for producing cycloolefins 失效
标题翻译：环烯烃的制备方法
公开(公告)号：US4665274A
公开(公告)日：1987-05-12
申请号：US900846
申请日：1986-08-27
申请人： Hiroshi Ichihashi , Hiroshi Yoshioka
发明人： Hiroshi Ichihashi , Hiroshi Yoshioka
IPC分类号： B01J27/00 , B01J27/053 , B01J27/055 , C07B61/00 , C07C1/00 , C07C5/11 , C07C13/02 , C07C13/20 , C07C67/00
CPC分类号： B01J27/053 , C07C5/11 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2523/46 , C07C2523/50 , C07C2523/72 , C07C2523/745 , C07C2523/75 , C07C2523/89 , C07C2527/053
摘要： A method for producing cycloolefins, useful as an intermediate for lysine, caprolactam, adipic acid etc., by the partial hydrogenation of corresponding aromatic hydrocarbons with a hydrogen gas in the presence of water and a catalyst comprising barium sulfate as a carrier and ruthenium and one or more metals selected from the group consisting of iron, cobalt, silver and copper supported on the carrier, characterized by incorporating one or more metal oxides selected from the group consisting of silicon dioxide, titanium dioxide and aluminum oxide in the reaction system.
摘要翻译：一种生产环烯烃的方法，可用作赖氨酸，己内酰胺，己二酸等的中间体，通过在水和含有硫酸钡作为载体的催化剂和钌和一种催化剂的存在下，用氢气对相应的芳烃进行部分氢化，或更多选自负载在载体上的铁，钴，银和铜的金属，其特征在于在反应体系中掺入一种或多种选自二氧化硅，二氧化钛和氧化铝的金属氧化物。

10. 发明授权

US4058547A Catalytic process for the production of acrylonitrile 失效
标题翻译：用于生产丙烯腈的催化工艺
公开(公告)号：US4058547A
公开(公告)日：1977-11-15
申请号：US302882
申请日：1972-11-01
申请人： Tatsuo Shiraishi , Shinkichi Shimizu , Hiroshi Ichihashi
发明人： Tatsuo Shiraishi , Shinkichi Shimizu , Hiroshi Ichihashi
IPC分类号： B01J23/887 , B01J27/192 , C07C120/14
CPC分类号： C07C253/26 , B01J23/8876 , B01J27/192 , Y02P20/52
摘要： In the production of acrylonitrile by a vapor phase reaction of propylene, ammonia and oxygen at an elevated temperature, a process which comprises contacting propylene, ammonia and oxygen with a catalyst composition comprising a catalyst system of the formula: Tl.sub.a P.sub.b Mo.sub.c Fe.sub.d Bi.sub.e X.sub.f O.sub.g wherein X represents one or more of the metals, Ni, Mg and Co, and a, b, c, d, e, f and g represent respectively the relative number of atoms of each component; provided that when c is 12, a is 2 or less, but not 0; b is 0 to 5; d is 0.1 to 5; e is 0.1 to 5; f is 2 to 15; and the value of g depends on the number of the other atoms and is usually from 38.3 to 81.5.
摘要翻译：在通过丙烯，氨和氧在升高的温度下的气相反应生产丙烯腈的过程中，包括使丙烯，氨和氧与包含下式催化剂体系的催化剂组合物接触的方法：其中X代表一个或多个更多的金属，Ni，Mg和Co，以及a，b，c，d，e，f和g分别表示各成分的相对原子数。条件是当c为12时，a为2或更小，但不为0; b为0〜5; d为0.1〜5; e为0.1〜5; f为2〜15; g的值取决于其他原子的数量，通常为38.3〜81.5。

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