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61. 发明授权

EP1713764B1 HOMOGENE ISOMERISIERUNG VON CIS-2-PENTENNITRIL ZU 3-PENTENNITRIL 有权
标题翻译： CIS 2戊烯腈均相异构化为3-戊烯
公开(公告)号：EP1713764B1
公开(公告)日：2007-08-29
申请号：EP05701200.7
申请日：2005-01-27
申请人： BASF Aktiengesellschaft
发明人： SCHEIDEL, Jens , MILLER, Christian , BAUMANN, Robert , JUNGKAMP, Tim , BARTSCH, Michael , HADERLEIN, Gerd , LUYKEN, Hermann , SIEGEL, Wolfgang , BASSLER, Peter
IPC分类号： C07C253/30 , C07C255/07
CPC分类号： C07C253/30 , Y02P20/127 , C07C255/07
摘要： The invention relates to a method for isomerization of pentene nitrile in an educt flow, wherein isomerization is performed on a homogeneously dissolved catalyst.

62. 发明公开

EP1716102A2 VERFAHREN ZUR HERSTELLUNG VON PENTENNITRILEN AUS N-BUTAN 有权
标题翻译：用于生产戊烯腈由正丁烷
公开(公告)号：EP1716102A2
公开(公告)日：2006-11-02
申请号：EP05701202.3
申请日：2005-01-27
申请人： BASF Aktiengesellschaft
发明人： BARTSCH, Michael , BAUMANN, Robert , HADERLEIN, Gerd , SCHINDLER, Götz-Peter , JUNGKAMP, Tim , LUYKEN, Hermann , SCHEIDEL, Jens , BRODHAGEN, Andreas
IPC分类号： C07C253/00
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for hydrocyanating 1,3-butadiene over at least one nickel(0) complex having phosphorus ligands as a catalyst, wherein the 1,3-butadiene is used in a mixture with n-butane and the mixture contains from 60 to 90% by volume of 1,3-butadiene and from 40 to 10% by volume of n-butane.

63. 发明公开

EP1682269A1 VERFAHREN ZUR HERSTELLUNG VON NICKEL(0)-PHOSPHORLIGAND-KOMPLEXEN 审中-公开
标题翻译：用于生产镍（0） - 磷络合物
公开(公告)号：EP1682269A1
公开(公告)日：2006-07-26
申请号：EP04790952.8
申请日：2004-10-28
申请人： BASF Aktiengesellschaft
发明人： HADERLEIN, Gerd , BAUMANN, Robert , BARTSCH, Michael , JUNGKAMP, Tim , LUYKEN, Hermann , SCHEIDEL, Jens , SIEGEL, Wolfgang
IPC分类号： B01J37/16 , B01J31/18 , B01J31/30 , C07F15/04 , C07C253/10
CPC分类号： C07F15/045 , B01J31/185 , B01J31/1865 , B01J31/1875 , B01J31/24 , B01J2231/323 , B01J2231/52 , B01J2531/847 , C07C253/10 , C07F15/04 , C07C255/04
摘要： The invention relates to a method for producing nickel(0)/phosphorus ligand complexes, which comprise at least one nickel(0) central atom and at least one phosphorus-containing ligand. Said method is characterised in that a nickel(II) source, containing nickel bromide, nickel iodide or mixtures thereof, is reduced in the presence of at least one phosphorus-containing ligand.

64. 发明授权

EP1521722B1 VERFAHREN ZUR ENTFERNUNG VON WASSER AUS EINER MISCHUNG, DIE WASSER UND ZINKCHLORID ENTH LT 有权
标题翻译：程序中除水从混合物中水和氯化锌ABST LT
公开(公告)号：EP1521722B1
公开(公告)日：2006-04-05
申请号：EP03738116.7
申请日：2003-07-04
申请人： BASF Aktiengesellschaft
发明人： JUNGKAMP, Tim , SCHEIDEL, Jens , LUYKEN, Hermann , BARTSCH, Michael , BAUMANN, Robert , HADERLEIN, Gerd
IPC分类号： C01G9/04 , B01D3/36 , C07C253/34
CPC分类号： C01G9/04 , B01D3/36 , F26B5/005 , F26B7/00
摘要： The invention relates to a method for removing water from a mixture containing water and zinc chloride. The invention is characterized in that said mixture containing water and zinc chloride is mixed with an aprotic, polar diluting agent whose boiling point, in the event of non-azeotropic formation of said diluting agent with water under the pressure conditions of the distillation mentioned below, is higher than the boiling point of water and is liquid at the boiling point of water or one azeotrope or heteroazeotrope with water is formed under the pressure and temperature conditions of the distillation mentioned below, and the mixture containing water, zinc chloride and the diluting agent is distilled while removing water or said azeotrope or said heteroazeotrope from this mixture while obtaining a water-free mixture containing zinc chloride and said diluting agent.

65. 发明公开

EP1610893A1 ALS KATALYSATOR FÜR DIE HYDROCYANIERUNG VON OLEFINISCH UNGESÄTTIGTEN VERBINDUNGEN GEEIGNETES SYSTEM 有权
标题翻译： AS烯属不饱和化合物FIT系统的催化剂的氢氰化
公开(公告)号：EP1610893A1
公开(公告)日：2006-01-04
申请号：EP04722843.2
申请日：2004-03-24
申请人： BASF Aktiengesellschaft
发明人： BARTSCH, Michael , BAUMANN, Robert , HADERLEIN, Gerd , FLORES, Miguel Angel , JUNGKAMP, Tim , LUYKEN, Hermann , SCHEIDEL, Jens , SIEGEL, Wolfgang , MOLNAR, Ferenc
IPC分类号： B01J27/14
CPC分类号： B01J31/185 , B01J23/755 , B01J31/0212 , B01J31/143 , B01J31/1865 , B01J2231/32 , B01J2531/847 , C07C253/10 , C07C255/04
摘要： A system suitable for use as a catalyst for the hydrocyanation of olefinically unsaturated compounds, containing a) Ni(0), b) Ni(0) as a ligand complex-fixing compound containing trivalent phosphorus, c) a Lewis acid and d) a compound of formula MRn wherein M = AI or Ti, R= identical or different monovalent alkoxyl radicals, wherein several alkoxy radicals can be interbridged, also in the case where M = AI, R = identical or different alkyl radicals wherein several alkyl radicals can be interbridged or one or several alkyl radicals can be bridged by one or several of the above-mentioned alkoxy radicals, n = valency of M. The invention also relates to methods for the hydrocyanation of an olefinically unsaturationed compound in the presence of said system.

66. 发明公开

EP1565435A1 VERFAHREN ZUR REINIGUNG VON CAPROLACTAM 有权
标题翻译：程序对清洁己内酰胺
公开(公告)号：EP1565435A1
公开(公告)日：2005-08-24
申请号：EP03789024.1
申请日：2003-11-11
申请人： BASF Aktiengesellschaft
发明人： LUYKEN, Hermann , ANSMANN, Andreas , BENISCH, Christoph , BASSLER, Peter , FISCHER, Rolf-Hartmuth , MAIXNER, Stefan , MELDER, Johann-Peter
IPC分类号： C07D201/16 , C07D201/08
CPC分类号： C07D201/16
摘要： The invention relates to a method for purifying crude caprolactam that has been obtained by: 1) reacting a mixture (I) containing 6-aminocapronitrile and water to form a mixture (II) containing caprolactam, ammonia, water, high boilers and low boilers in the presence of a catalyst followed by; 2) removing ammonia from mixture (II) while obtaining a mixture (III) that contains caprolactam, water, high boilers and low boilers, after which; 3) water is entirely or partially removed from mixture (III) while obtaining a crude caprolactam (IV) that contains caprolactam, high boilers and low boilers. The inventive method is characterized in that: a) the crude caprolactam and an inorganic acid, which has a boiling point higher that that of caprolactam under distillation conditions in accordance with subsequent steps b) to h), are fed to a first distillation device K1; b) the crude caprolactam and the inorganic acid are distilled in the first distillation device K1 during which a first partial flow in the bottom area and a second partial flow in the top area are withdrawn from the distillation device K1; c) the second partial flow from step b) is fed to a second distillation device K2; d) the second partial flow from step b) is distilled in the second distillation device K2 during which a first partial flow in the bottom area and a second partial flow in the top area are withdrawn from the distillation device K2; e) a first partial flow from step d) is fed to a third distillation device K3; f) the first partial flow from step d) is distilled in the third distillation device K3 during which a first partial flow in the bottom area and purified caprolactam in the top area are withdrawn from the distillation device K3, and; g) the first partial flow from step f) is fed to the first distillation device K1.

67. 发明授权

EP1299347B1 VERFAHREN ZUR ABTRENNUNG VON AMMONIAK 有权
标题翻译：用于分离氨
公开(公告)号：EP1299347B1
公开(公告)日：2005-04-27
申请号：EP01957948.1
申请日：2001-07-10
申请人： BASF AKTIENGESELLSCHAFT
发明人： LUYKEN, Hermann
IPC分类号： C07C231/24 , C07D201/16
CPC分类号： C07C231/24 , C07D201/16
摘要： The invention relates to a method for separating ammoniac (I) from mixtures (II) containing ammoniac (I) and an amide (IV) is obtained by reacting educts (III) selected from the group consisting of nitriles (IIIa), amines (IIIb), aminonitriles (IIIc) and aminoamides (IIId) with water. The method is characterised in that a) the educt (III) is reacted with water in liquid phase in the presence of an organic liquid diluting agent (V) to form a mixture (II) containing amide (IV) and ammoniac (I), b) the mixture (II) is transformed under conditions of mass, pressure and temperature - under which the diluting agent (V) and the water are in a liquid state and exhibit a miscibility gap - in order to obtain a two phase system consisting of a phase (VII), c) phase (VII) is separated from phase (VIII), d) the ammoniac present in phase (VII) is separated by extraction (a) by means of a mixture (IX) containing water in order to obtain a mixture (XI) which contains less ammoniac than phase (VII), and e) the diluting agent (V) is separated from the mixture (XI) in order to obtain the amide (IV).

68. 发明授权

EP1058677B1 VERFAHREN ZUR HYDRIERUNG VON ALIPHATISCHEN ALPHA, OMEGA-DINITRILEN 有权
标题翻译： PROCESS加氢脂肪族α，ω-二腈
公开(公告)号：EP1058677B1
公开(公告)日：2003-01-08
申请号：EP99915533.6
申请日：1999-02-23
申请人： BASF AKTIENGESELLSCHAFT
发明人： VOIT, Guido , OHLBACH, Frank , LUYKEN, Hermann , MERGER, Martin , REHFINGER, Alwin , FISCHER, Rolf, Hartmuth , BASSLER, Peter , ANSMANN, Andreas
IPC分类号： C07C209/00
CPC分类号： C07C253/30 , B01J23/02 , B01J23/78 , C07C209/48 , C07C211/12 , C07C255/24

69. 发明授权

EP0927157B1 VERFAHREN ZUR GLEICHZEITIGEN HERSTELLUNG VON 6-AMINOCAPRONITRIL UND HEXAMETHYLENDIAMIN 失效
公开(公告)号：EP0927157B1
公开(公告)日：2001-12-05
申请号：EP97940102.3
申请日：1997-08-21
申请人： BASF AKTIENGESELLSCHAFT
发明人： LUYKEN, Hermann , VOIT, Guido , BASSLER, Peter , REHFINGER, Alwin , FISCHER, Rolf
IPC分类号： C07C253/34 , C07C209/84 , C07C255/24 , C07C211/12
CPC分类号： C07C253/30 , C07C209/48
摘要： The invention concerns a process for simultaneously preparing 6-aminocapronitrile and hexamethylene diamine proceeding from adipodinitrile. The process is characterized in that: (1) adipodinitrile is partially hydrogenated in the presence of a catalyst in order to obtain a mixture containing 6-aminocapronitrile, hexamethylene diamine and adipodinitrile; (2) 6-aminocapronitrile and hexamethylene diamine are separated from the mixture; (3) between 0.01 and 10 wt %, relative to adipodinitrile, of an acid or an acidic ion exchanger is added to the part substantially containing adipodinitrile, and the adipodinitrile is separated from the mixture; and (4) the adipodinitrile is returned to step (1).

70. 发明授权

EP0801643B1 VERFAHREN ZUR KONTINUIERLICHEN REINIGUNG VON AUS 6-AMINOCAPRONITRIL HERGESTELLTEM ROH-CAPROLACTAM 失效
标题翻译：用于连续清洁方法OUT 6-氨基己腈生产ROH己内酰胺
公开(公告)号：EP0801643B1
公开(公告)日：2001-07-25
申请号：EP95942729.5
申请日：1995-12-22
申请人： BASF AKTIENGESELLSCHAFT
发明人： RITZ, Josef , FISCHER, Rolf , SCHNURR, Werner , ACHHAMMER, Günther , LUYKEN, Hermann , FUCHS, Eberhard
IPC分类号： C07D201/16 , C07D201/08 , C07B63/02
CPC分类号： C07D201/16 , Y02P20/52

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