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41. 发明授权

US07812086B2 Fluorinated elastomer latex, its production method, fluorinated elastomer and fluororubber molded product 有权
标题翻译：氟化弹性体胶乳，其生产方法，氟化弹性体和氟橡胶成型产品
公开(公告)号：US07812086B2
公开(公告)日：2010-10-12
申请号：US11291812
申请日：2005-12-02
申请人： Hiroshi Funaki , Ryuji Seki , Kazuya Oharu , Hiroki Kamiya
发明人： Hiroshi Funaki , Ryuji Seki , Kazuya Oharu , Hiroki Kamiya
IPC分类号： C08L27/12
CPC分类号： C08F214/265 , C08F214/262 , C08K5/09 , C08L27/12
摘要： The current invention relates to a fluorinated elastomer latex containing an aqueous medium, a fluorinated elastomer dispersed in the aqueous medium in an amount of from 10 to 60 mass % and a fluorinated emulsifier represented by the formula (1): C2F5O(CF2CF2O)mCF2COOA (wherein A is a hydrogen atom, an alkali metal or NH4, and m is an integer of from 1 to 3), which employs no perfluorooctanoate emulsifier and which is excellent in dispersion stability of the fluorinated elastomer.
摘要翻译：本发明涉及含有水性介质，分散在水性介质中的氟化弹性体，含量为10〜60质量％的氟化弹性体胶乳和由式（1）表示的氟化乳化剂：C2F5O（CF2CF2O）mCF2COOA（其中A为氢原子，碱金属或NH 4，m为1至3的整数），其不使用全氟辛酸酯乳化剂，并且氟化弹性体的分散稳定性优异。

42. 发明授权

US07408019B2 Fluorinated ether compound 失效
标题翻译：氟化醚化合物
公开(公告)号：US07408019B2
公开(公告)日：2008-08-05
申请号：US11410896
申请日：2006-04-26
申请人： Masao Iwaya , Kazuya Oharu , Hirokazu Takagi , Hidekazu Okamoto
发明人： Masao Iwaya , Kazuya Oharu , Hirokazu Takagi , Hidekazu Okamoto
IPC分类号： C08G73/24 , C07C43/11
CPC分类号： C09K5/00
摘要： A novel fluorinated ether compound useful as an inert medium is provided.The compound is represented by the following formula (1) such as the compound represented by the following formula (1a) or the compound represented by the following formula (1b): RF1OCFRF2CFRF2ORF1 (1) F(CF2)4OCF(CF3)CF(CF3)O(CF2)4F (1a) F(CF2)6OCF(CF3)CF(CF3)O(CF2)6F (1b) wherein the symbols have the following meanings: RF1 is a C4-7 linear perfluoroalkyl group; and RF2 is a fluorine atom or a trifluoromethyl group.
摘要翻译：提供了可用作惰性介质的新型氟化醚化合物。该化合物由下式（1a）表示的化合物或下式（1b）表示的化合物表示：＆lt;线内配方说明=“在线式” 结束=“引导”→>> F1> > > <？in-line-formula description =“In-line Formulas”end =“lead”？> F（CF < 4）OCF（CF 3）CF（CF 3 O）O（CF 2）4 F（1a）<？in-line-formula description =“In-line Formulas”end =“tail”？> <？in-line-formula description =“In-line Formulas”end =“lead” CF（CF 3）O（CF 3）2 CFF（CF 3 3）O（CF 3） F（1b）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中符号具有以下含义： R F1是直链全氟烷基的C 4-7直链; R F2是氟原子或三氟甲基。

43. 发明授权

US07193119B2 Process for producing fluorinated alkyl ether 有权
标题翻译：制备氟化烷基醚的方法
公开(公告)号：US07193119B2
公开(公告)日：2007-03-20
申请号：US11348490
申请日：2006-02-07
申请人： Masazumi Nagai , Hidekazu Okamoto , Kazuya Oharu
发明人： Masazumi Nagai , Hidekazu Okamoto , Kazuya Oharu
IPC分类号： C07C41/00
CPC分类号： C07C41/06 , C07C43/123
摘要： To provide a process for producing a fluorinated alkyl ether, whereby a sufficient reaction rate can be attained even under mild reaction conditions, and a post-process such as distillation after the reaction can be efficiently carried out.A process for producing a fluorinated alkyl ether, which comprises introducing an aprotic polar solvent, a fluorinated ether, a catalyst, a fluorinated alkyl alcohol and a fluorinated olefin into a reactor, and then, reacting the fluorinated alkyl alcohol with the fluorinated olefin, characterized in that the ratio of the two components of the aprotic polar solvent and the fluorinated ether introduced into the reactor is the aprotic polar solvent/the fluorinated ether=5/95 to 80/20 by mass ratio.
摘要翻译：为了提供氟化烷基醚的制造方法，即使在温和的反应条件下也能够得到充分的反应速度，能够有效地进行反应后的蒸馏等后处理。一种制备氟化烷基醚的方法，包括将非质子极性溶剂，氟化醚，催化剂，氟化烷基醇和氟化烯烃引入反应器中，然后使氟化烷基醇与氟化烯烃反应，其特征在于引入到反应器中的非质子极性溶剂和氟化醚的两种组分的比例是非质子极性溶剂/氟化醚= 5/95〜80/20质量比。

44. 发明授权

US07193118B2 Method for producing fluoroalkyl ether 有权
标题翻译：氟烷基醚的制备方法
公开(公告)号：US07193118B2
公开(公告)日：2007-03-20
申请号：US11293200
申请日：2005-12-05
申请人： Hidekazu Okamoto , Masazumi Nagai , Kazuya Oharu
发明人： Hidekazu Okamoto , Masazumi Nagai , Kazuya Oharu
IPC分类号： C07C41/06
CPC分类号： C07C41/06 , C07C43/123
摘要： A method for producing a fluoroalkyl ether, which comprises reacting a fluoroalkyl alcohol with a fluorinated olefin in the presence of a solvent and a catalyst, wherein the fluoroalkyl alcohol and the fluorinated olefin are continuously supplied into a reactor, a reaction product containing the fluoroalkyl ether is continuously withdrawn from the reactor, and the reaction is carried out while the concentration of the fluoroalkyl alcohol present in the reactor is maintained to be at most 7 mass % based on the total organic component present in the reactor. According to the present invention, a fluoroalkyl ether having a high purity can be produced in an industrial scale and at a high reaction rate.
摘要翻译：一种制备氟烷基醚的方法，其包括在溶剂和催化剂存在下使氟代烷基醇与氟化烯烃反应，其中将氟代烷基醇和氟化烯烃连续地供入反应器中，将含有氟代烷基醚从反应器中连续取出，反应进行，同时反应器中存在的氟代烷基醇的浓度维持在反应器中存在的总有机成分的7质量％以下。根据本发明，可以以工业规模和高反应速度制备高纯度的氟烷基醚。

45. 发明申请

US20060199979A1 Fluorinated ether compound 失效
标题翻译：氟化醚化合物
公开(公告)号：US20060199979A1
公开(公告)日：2006-09-07
申请号：US11410896
申请日：2006-04-26
申请人： Masao Iwaya , Kazuya Oharu , Hirokazu Takagi , Hidekazu Okamoto
发明人： Masao Iwaya , Kazuya Oharu , Hirokazu Takagi , Hidekazu Okamoto
IPC分类号： C07C43/11
CPC分类号： C09K5/00
摘要： A novel fluorinated ether compound useful as an inert medium is provided. The compound is represented by the following formula (1) such as the compound represented by the following formula (1a) or the compound represented by the following formula (1b): RF1OCFRF2CFRF2ORF1 (1) F(CF2)4OCF(CF3)CF(CF3)O(CF2)4F (1a) F(CF2)6OCF(CF3)CF(CF3)O(CF2)6F (1b) wherein the symbols have the following meanings: RF1 is a C4-7 linear perfluoroalkyl group; and RF2 is a fluorine atom or a trifluoromethyl group.
摘要翻译：提供了可用作惰性介质的新型氟化醚化合物。该化合物由下式（1a）表示的化合物或下式（1b）表示的化合物表示：＆lt;线内配方说明=“在线式” 结束=“引导”→>> F1> > > <？in-line-formula description =“In-line Formulas”end =“lead”？> F（CF < 4）OCF（CF 3）CF（CF 3 O）O（CF 2）4 F（1a）<？in-line-formula description =“In-line Formulas”end =“tail”？> <？in-line-formula description =“In-line Formulas”end =“lead” CF（CF 3）O（CF 3）2 CFF（CF 3 3）O（CF 3） F（1b）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中符号具有以下含义： R F1是直链全氟烷基的C 4-7直链; R F2是氟原子或三氟甲基。

46. 发明授权

US07102031B2 Method for producing diene compound 有权
标题翻译：生产二烯化合物的方法
公开(公告)号：US07102031B2
公开(公告)日：2006-09-05
申请号：US10864497
申请日：2004-06-10
申请人： Masao Iwaya , Hidekazu Okamoto , Kazuya Oharu
发明人： Masao Iwaya , Hidekazu Okamoto , Kazuya Oharu
IPC分类号： C07C41/18
CPC分类号： C08F36/20 , C07C17/361 , C07C41/44 , C07C51/58 , C08F16/32 , C07C21/18 , C07C57/76 , C07C57/66 , C07C43/17
摘要： It is an object to obtain from a mixture of a specific diene compound (1) and a compound (2) with the same molecular weight and molecular formula hard to separate by distillation, the diene compound (1) in high purity without using any special reagent or complicated technique.Namely, the present invention provides a method of inducing the Claisen rearrangement reaction of the compound (2) in a mixture containing CR1R2═CR3CFR4CR5R6OCR7═CR8R9 (1) and CFR1R2CR3═CR4CR5R6OCR7═CR8R9 (2), and separating the diene compound (1) from a Claisen rearrangement reaction product; or converting the Claisen rearrangement reaction product into a derivative and then separating the diene compound (1) from the derivative of the Claisen rearrangement reaction product. Wherein, R1 to R9 each represent a fluorine atom or the like.
摘要翻译：本发明的目的是从具有相同分子量和分子式的特定二烯化合物（1）和化合物（2）的混合物中获得，其难以通过蒸馏分离，高纯度的二烯化合物（1）不使用任何特殊的试剂或复杂技术。也就是说，本发明提供了一种诱导化合物（2）在混合物中的Claisen重排反应的方法，该混合物包含CR 1，R 2，R 2， SUP> CFR 9（1）和CFR 1

47. 发明授权

US06903230B2 Process for producing a fluorine-containing compound 有权
标题翻译：含氟化合物的制造方法
公开(公告)号：US06903230B2
公开(公告)日：2005-06-07
申请号：US10629710
申请日：2003-07-30
申请人： Shuzhong Wang , Kazuhiko Hayashi , Shinsuke Kaga , Kazuya Oharu
发明人： Shuzhong Wang , Kazuhiko Hayashi , Shinsuke Kaga , Kazuya Oharu
IPC分类号： C07B39/00 , C07C17/04 , C07C17/18 , C07C67/307 , C07C19/08 , C07C25/13 , C07D69/76
CPC分类号： C07C17/18 , C07B39/00 , C07C17/04 , C07C67/307 , C07C69/75
摘要： It is to provide a process for synthesizing an intended fluorine-containing compound having a geminal difluoro structure with a high yield, by subjecting a carbonyl compound which is readily available to a two-stage reaction.A compound (1) such as ethyl 4-oxocyclohexanecarboxylate is reacted with a compound of the formula X-Z or a compound of the formula Z2O (wherein Z is a monovalent group which gives a leaving group of the structure —OZ, and X is a chlorine atom, a bromine atom or an iodine atom) such as phosphorus pentachloride, and then a fluorinating agent which generates fluorine anions such as HF is acted thereon to obtain a fluorine-containing compound (2) such as ethyl 4,4-difluorocyclohexanecarboxylate
摘要翻译：通过使容易获得的羰基化合物进行两步反应来提供通过高收率合成具有偕二氟结构的目标含氟化合物的方法。使化合物（1）如4-氧代环己烷羧酸乙酯与式XZ化合物或式Z 2 O 2化合物（其中Z是一价基团，使得结构-OZ，X是氯原子，溴原子或碘原子）如五氯化磷，然后将产生氟等阴离子的氟化物如HF用作获得含氟化合物（2），例如作为4,4-二氟环己烷羧酸乙酯

48. 发明授权

US06860926B2 Fluorine-containing compound, and water and oil repellent composition 失效
标题翻译：含氟化合物，防水防油组合物
公开(公告)号：US06860926B2
公开(公告)日：2005-03-01
申请号：US09976435
申请日：2001-10-15
申请人： Minako Ishikawa , Takashige Maekawa , Ryuji Seki , Shoji Furuta , Kazuya Oharu
发明人： Minako Ishikawa , Takashige Maekawa , Ryuji Seki , Shoji Furuta , Kazuya Oharu
IPC分类号： C03C17/28 , C03C17/32 , C03C25/24 , C03C25/26 , C07C69/62 , C07C69/63 , C07C311/09 , C09K3/18 , D06M13/236 , D06M15/277 , C07C311/24
CPC分类号： D06M15/277 , C03C17/28 , C03C17/32 , C03C25/25 , C03C25/26 , C07C69/62 , C07C69/63 , C07C311/09 , C09K3/18 , D06M13/236 , D06M2200/10 , D06M2200/11 , D06M2200/12
摘要： The following fluorine-containing compound is presented which is capable of providing dry soil resistance when incorporated to a water and oil repellent.Rf1R2OCOCH2CHR1COOR3Rf2 (wherein each of Rf1 and Rf2 which are independent of each other, is a C3-22 polyfluoroalkyl group, R1 is a hydrogen atom or a C1-10 alkyl group, and each of R2 and R3 which are independent of each other, is a C1-4 alkylene group, etc.).
摘要翻译：提供以下含氟化合物，其在掺入拒水拒油剂时能够提供干性土壤抗性。R 1 R 2 OCOCH 2 CHR 1 COOR 3 R f（其中每个R 彼此独立的和R f2是C3-22多氟烷基，R 1是氢原子或C 1-10烷基，R 2和R 3中的每一个 >彼此独立，是C 1-4亚烷基等）。

49. 发明授权

US06315822B1 Phosphate type water and oil repellent composition 失效
标题翻译：磷酸类防水斥油剂组合物
公开(公告)号：US06315822B1
公开(公告)日：2001-11-13
申请号：US09435208
申请日：1999-11-05
申请人： Kazuya Oharu , Minako Shindo
发明人： Kazuya Oharu , Minako Shindo
IPC分类号： C09K318
CPC分类号： D21H21/16 , C09K3/18 , C14C9/00 , D21H17/10 , D21H17/11 , Y10T428/31993
摘要： A water and oil repellent composition comprising, as essential components, a phosphate of the following formula 1, a nonionic surfactant made of a compound containing at least one carbon-carbon triple bond and at least one hydroxyl group in its molecule and an aqueous medium: (Rf—Q—O—)mPO(OH)n(O−)3−m−n.(Y+)3−m−n Formula 1 wherein Rf is a polyfluoroalkyl group, Q is a bivalent organic group, Y+ is a monovalent counter ion, m is an integer of from 1 to 3, and n is an integer of from 0 to 2, provided that (m+n) is 1, 2 or 3.
摘要翻译：一种拒水拒油剂组合物，其包含作为必要成分的下式1的磷酸盐，由分子中含有至少一个碳 - 碳三键和至少一个羟基的化合物和水性介质组成的非离子表面活性剂：其中Rf是多氟烷基，Q是二价有机基团，Y +是一价抗衡离子，m是1至3的整数，n是0-2的整数，条件是（m + n）是 1，2或3。

50. 发明授权

US5728903A Method for producing flourine-containing silicone compound 失效
标题翻译：生产含氟化硅化合物的方法
公开(公告)号：US5728903A
公开(公告)日：1998-03-17
申请号：US779370
申请日：1997-01-06
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
IPC分类号： C08G77/385 , C07C17/15
CPC分类号： C08G77/385
摘要： A method for producing a fluorine-containing silicone compound, which comprises subjecting a compound of the following formula (I) and a hydrosilicone compound having at least one hydrogen atom bonded to a silicon atom to hydrosilylation to obtain a fluorine-containing silicone compound having a R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 HCR.sup.4 R.sup.5 -- group bonded to the silicon atom: R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 .dbd.CR.sup.4 R.sup.5(I) wherein R.sup.f is a monovalent fluorine-containing organic group, Q is a single bond or a bivalent organic group containing no fluorine atom, and each of R.sup.1 to R.sup.5 which are independent of one another, is a hydrogen atom or a monovalent organic group.
摘要翻译：一种含氟硅氧烷化合物的制造方法，其特征在于，使下述式（I）的化合物与具有至少一个与硅原子键合的氢原子的氢硅氧烷化合物进行氢化硅烷化，得到具有 Rf-Q-CR1R2CR3HCR4R5-键合到硅原子上：Rf-Q-CR1R2CR3 = CR4R5（Ⅰ）其中Rf是一价含氟有机基团，Q是单键或不含氟原子的二价有机基团，和彼此独立的R 1至R 5中的每一个为氢原子或一价有机基团。

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