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1. 发明授权

US5914422A Method for producing fluorine-containing silicone compound 失效
标题翻译：含氟硅氧烷化合物的制造方法
公开(公告)号：US5914422A
公开(公告)日：1999-06-22
申请号：US966482
申请日：1997-11-07
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
IPC分类号： C08G77/385 , C07F7/08
CPC分类号： C08G77/385
摘要： A method for producing a fluorine-containing silicone compound, which comprises subjecting a compound of the following formula (I) and a hydrosilicone compound having at least one hydrogen atom bonded to a silicon atom to hydrosilylation to obtain a fluorine-containing silicone compound having a R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 HCR.sup.4 R.sup.5 -- group bonded to the silicon atom:R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 .dbd.CR.sup.4 R.sup.5(I)wherein R.sup.f is a monovalent fluorine-containing organic group, Q is a single bond or a bivalent organic group containing no fluorine atom, and each of R.sup.1 to R.sup.5 which are independent of one another, is a hydrogen atom or a monovalent organic group.
摘要翻译：一种含氟硅氧烷化合物的制造方法，其特征在于，使下述式（I）的化合物与具有至少一个与硅原子键合的氢原子的氢硅氧烷化合物进行氢化硅烷化，得到具有 Rf-Q-CR1R2CR3HCR4R5-键合到硅原子上：Rf-Q-CR1R2CR3 = CR4R5（Ⅰ）其中Rf是一价含氟有机基团，Q是单键或不含氟原子的二价有机基团，和彼此独立的R 1至R 5中的每一个为氢原子或一价有机基团。

2. 发明授权

US5663399A Method for producing fluorine-containing silicone compound 失效
标题翻译：含氟硅氧烷化合物的制造方法
公开(公告)号：US5663399A
公开(公告)日：1997-09-02
申请号：US547923
申请日：1995-10-25
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
IPC分类号： C08G77/385 , C07F7/08
CPC分类号： C08G77/385
摘要： A method for producing a fluorine-containing silicone compound, which comprises subjecting a compound of the following formula (I) and a hydrosilicone compound having at least one hydrogen atom bonded to a silicon atom to hydrosilylation to obtain a fluorine-containing silicone compound having a R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 HCR.sup.4 R.sup.5 -- group bonded to the silicon atom:R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 =CR.sup.4 R.sup.5 (I)wherein R.sup.f is a monovalent fluorine-containing organic group, Q is a single bond or a bivalent organic group containing no fluorine atom, and each of R.sup.1 to R.sup.5 which are independent of one another, is a hydrogen atom or a monovalent organic group.
摘要翻译：一种含氟硅氧烷化合物的制造方法，其特征在于，使下述式（I）的化合物与具有至少一个与硅原子键合的氢原子的氢硅氧烷化合物进行氢化硅烷化，得到具有 Rf-Q-CR1R2CR3HCR4R5-键合到硅原子上：Rf-Q-CR1R2CR3 = CR4R5（Ⅰ）其中Rf是一价含氟有机基团，Q是单键或不含氟原子的二价有机基团，和彼此独立的R 1至R 5中的每一个为氢原子或一价有机基团。

3. 发明授权

US5728903A Method for producing flourine-containing silicone compound 失效
标题翻译：生产含氟化硅化合物的方法
公开(公告)号：US5728903A
公开(公告)日：1998-03-17
申请号：US779370
申请日：1997-01-06
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Kazuya Oharu , Toshihiko Toma
IPC分类号： C08G77/385 , C07C17/15
CPC分类号： C08G77/385
摘要： A method for producing a fluorine-containing silicone compound, which comprises subjecting a compound of the following formula (I) and a hydrosilicone compound having at least one hydrogen atom bonded to a silicon atom to hydrosilylation to obtain a fluorine-containing silicone compound having a R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 HCR.sup.4 R.sup.5 -- group bonded to the silicon atom: R.sup.f --Q--CR.sup.1 R.sup.2 CR.sup.3 .dbd.CR.sup.4 R.sup.5(I) wherein R.sup.f is a monovalent fluorine-containing organic group, Q is a single bond or a bivalent organic group containing no fluorine atom, and each of R.sup.1 to R.sup.5 which are independent of one another, is a hydrogen atom or a monovalent organic group.
摘要翻译：一种含氟硅氧烷化合物的制造方法，其特征在于，使下述式（I）的化合物与具有至少一个与硅原子键合的氢原子的氢硅氧烷化合物进行氢化硅烷化，得到具有 Rf-Q-CR1R2CR3HCR4R5-键合到硅原子上：Rf-Q-CR1R2CR3 = CR4R5（Ⅰ）其中Rf是一价含氟有机基团，Q是单键或不含氟原子的二价有机基团，和彼此独立的R 1至R 5中的每一个为氢原子或一价有机基团。

4. 发明授权

US06197989B1 Fluorinated organosilicon compounds and process for the preparation thereof 有权
标题翻译：氟化有机硅化合物及其制备方法
公开(公告)号：US06197989B1
公开(公告)日：2001-03-06
申请号：US09147542
申请日：1999-03-17
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Robert E. Ruckle, Jr. , Gerald J. Murphy
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Robert E. Ruckle, Jr. , Gerald J. Murphy
IPC分类号： C07F702
CPC分类号： C08G77/385 , C08G77/24 , C08G77/46
摘要： A fluorine-containing organic silicon compound represented by the following formula 1, which is useful as various industrial base materials required to have performances such as water and oil repellency, anti-fouling properties or release properties and as raw materials therefor. Here, Af represents a specific polyfluorohydrocarbon group-containing organic group; R1 and R2 which are independent of each other, represent bivalent organic groups; R3 to R9 which are independent of one another, represent monovalent organic groups; a is an integer of at least 1, and b is an integer of at least 0:
摘要翻译：由下式1表示的含氟有机硅化合物，其可用作要具有防斥油性，防污性或脱模性等性能的各种工业基材，作为其原料。这里，Af表示具体的含多氟烃基的有机基团，彼此独立的R 1和R 2表示二价有机基团; 彼此独立的R3至R9表示一价有机基团; a是至少为1的整数，b是至少为0的整数：

5. 发明授权

US5834614A Method for producing a fluorine-containing silicone compound 失效
标题翻译：含氟硅氧烷化合物的制造方法
公开(公告)号：US5834614A
公开(公告)日：1998-11-10
申请号：US847454
申请日：1997-04-23
申请人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Gerald J. Murphy
发明人： Yutaka Furukawa , Mami Kotera , Seisaku Kumai , Gerald J. Murphy
IPC分类号： C08G77/22 , C08G77/385 , C07F7/08
CPC分类号： C08G77/385
摘要： A method for producing a fluorine-containing silicone compound, which comprises subjecting a fluorine-containing unsaturated compound of the following formula (1) and a hydrosilicone compound having at least one hydrogen atom bonded to a silicon atom to hydrosilylation in the presence of a catalyst to obtain a fluorine-containing silicone compound having a R.sup.f --Q--CR.sup.1 R.sup.2 --CHR.sup.3 --CR.sup.4 R.sup.5 -- group bonded to the silicon atom: R.sup.f --Q--CR.sup.1 R.sup.2 --CR.sup.3 .dbd.CR.sup.4 R.sup.5( 1) wherein R.sup.f is a monovalent fluorine-containing organic group, Q is a single bond or a bivalent organic group, and each of R.sup.1 to R.sup.5 which are independent of one another, is a hydrogen atom or a monovalent organic group, wherein the hydrosilylation is carried out substantially in the absence of a solvent.
摘要翻译：一种含氟硅氧烷化合物的制造方法，其特征在于，将下述式（1）所示的含氟不饱和化合物与至少一个与硅原子键合的氢原子的氢硅氧烷化合物在催化剂存在下进行氢化硅烷化得到具有与硅原子键合的Rf-Q-CR1R2-CHR3-CR4R5-基团的含氟硅氧烷化合物：Rf-Q-CR1R2-CR3 = CR4R5（1）其中Rf是一价含氟有机基团， Q是单键或二价有机基团，R 1〜R 5彼此独立的是氢原子或一价有机基团，其中氢化硅烷化基本上在没有溶剂的情况下进行。

6. 发明授权

US5568239A Stainproofing oil for a heat fixing roller 失效
标题翻译：用于热定影辊的防油
公开(公告)号：US5568239A
公开(公告)日：1996-10-22
申请号：US412221
申请日：1995-03-27
申请人： Yutaka Furukawa , Seisaku Kumai , Mami Yoshino
发明人： Yutaka Furukawa , Seisaku Kumai , Mami Yoshino
IPC分类号： C09K3/00 , C08G77/24 , C10M107/50 , G03G15/20
CPC分类号： C08G77/24 , G03G15/2025 , G03G2215/2093 , Y10S118/01
摘要： A stainproofing oil for a heat fixing roller, which consists essentially of a fluorosilicone compound having a silicon atom to which a monovalent fluorine-containing group selected from the formulae (1) to (3) is bonded:R.sub.f.sup.1 --X.sup.1 -- (1)R.sub.f.sup.2 --X.sup.2 --O--X.sup.3 -- (2)R.sub.f.sup.3 --X.sup.4 --O--X.sup.5 -- (3)wherein R.sub.f.sup.1 is a monovalent polyfluorohydrocarbon group, R.sub.f.sup.2 is a monovalent polyfluoroalkyl group containing an ether oxygen atom, R.sub.f.sup.3 is a monovalent polyfluorohydrocarbon group, and each of X.sup.1 to X.sup.5 independently is a bivalent hydrocarbon group.
摘要翻译：用于热定影辊的防污油，其基本上由具有选自式（1）至（3）的一价含氟基团的具有硅原子的氟硅氧烷化合物组成：Rf1-X1-（1）Rf2 -X2-O-X3-（2）Rf3-X4-O-X5-（3）其中Rf1是一价多氟烃基，Rf2是含有醚氧原子的一价多氟烷基，Rf3是一价多氟烃基， X1〜X5独立地为二价烃基。

7. 发明授权

US5834612A Fluorine-containing organic compound 失效
标题翻译：含氟有机化合物
公开(公告)号：US5834612A
公开(公告)日：1998-11-10
申请号：US855947
申请日：1997-05-14
申请人： Yutaka Furukawa , Seisaku Kumai , Jeffery A. Cooke , Gerald J. Murphy , George A. Policello
发明人： Yutaka Furukawa , Seisaku Kumai , Jeffery A. Cooke , Gerald J. Murphy , George A. Policello
IPC分类号： C07C43/17 , C08G77/385 , C07F7/08
CPC分类号： C07C43/17 , C08G77/385
摘要： A fluorine-containing organic compound of the following formula (1): R.sup.f CH.sub.2 CH.sub.2 CH.sub.2 OCH.sub.2 CH.dbd.CH.sub.2 ( 1) wherein R.sup.f is a C.sub.1-20 fluoroalkyl group.
摘要翻译：下式（1）的含氟有机化合物：RfCH2CH2CH2OCH2CH = CH2（1）其中Rf是C1-20氟代烷基。

8. 发明授权

US5908950A Polyether modified fluoroalkylsiloxanes 失效
标题翻译：聚醚改性氟烷基硅氧烷
公开(公告)号：US5908950A
公开(公告)日：1999-06-01
申请号：US862939
申请日：1997-05-29
申请人： Jeffrey A. Cooke , Gerald J. Murphy , Yutaka Furukawa , Seisaku Kumai
发明人： Jeffrey A. Cooke , Gerald J. Murphy , Yutaka Furukawa , Seisaku Kumai
IPC分类号： C08L83/05 , C08G77/385 , C08G77/46 , C08G81/00 , C07F7/08
CPC分类号： C08G77/385 , C08G77/46
摘要： Polyether modified fluoroalkylsiloxanes having the general structure of Formula (I), Formula (II) or Formula (III): ##STR1## wherein x is about 0 to 500, y is about 1 to 50, z is about 1 to 50, R=C.sub.p H.sub.2p --(OC.sub.2 H.sub.4).sub.n --(OC.sub.3 H.sub.6).sub.n).sub.m --OR' in which p is about 2 to 5, n is about 0 to 50, N is about 0 to 50, and one of n or m must be >0, and R'=H, an alkyl group with 1-4 carbons, or an acetyl group and R.sub.f =C.sub.a H.sub.2a --O.sub.b --C.sub.c H.sub.2c --C.sub.d F.sub.2d+1 in which a is 3 or 4, b is 0 or 1, c is 0 or 2-4 and d is 4-12 with the provisos that if b=0, then c=0, and that if b=1, then c=2-4; z.sub.1 is about 0 to 50 and y.sub.1 is about 0 to 50, are useful to reduce the coefficient of friction and to increase mar resistance of coatings, to increase spreadability and wettability of coating formulations, and as foam control agents.
摘要翻译：具有式（I），式（II）或式（III）的通式结构的聚醚改性氟代烷基硅氧烷：其中x为约0至500，y为约1至50，z为约1至50，R = CpH 2 p-（ OC2H4）n - （OC3H6）n）m-OR'，其中p为约2至5，n为约0至50，N为约0至50，n或m中的一个必须> 0，R' = H，具有1-4个碳原子的烷基或乙酰基，R f = CaH 2 a -Ob-CcH2c-CdF2d + 1，其中a为3或4，b为0或1，c为0或2-4， d为4-12，条件是如果b = 0，则c = 0，如果b = 1，则c = 2-4; z1为约0〜50，y1约为0〜50，可用于降低摩擦系数，提高涂层的耐磨性，增加涂料配方的铺展性和润湿性，以及泡沫控制剂。

9. 发明授权

US5861524A Oligomeric fluoroalkylsiloxanes as oil spreading agents 失效
标题翻译：低聚氟代烷基硅氧烷作为油扩散剂
公开(公告)号：US5861524A
公开(公告)日：1999-01-19
申请号：US844810
申请日：1997-04-22
申请人： Gerald J. Murphy , Seisaku Kumai , Jeffrey A. Cooke , Yutaka Furukawa , George A. Policello
发明人： Gerald J. Murphy , Seisaku Kumai , Jeffrey A. Cooke , Yutaka Furukawa , George A. Policello
IPC分类号： B01F17/54 , A01N25/02 , A01N25/30 , C07F7/08 , C07F7/12
CPC分类号： C07F7/085 , C07F7/0852 , Y10S424/08
摘要： Oligomeric fluoroalkylsiloxanes corresponding to the formula: ##STR1## wherein x is 0 to 3, y is 0, 1, or 2; z is 0 or 1; x+y>0, and R has the formula --C.sub.a H.sub.2a --O.sub.b --C.sub.d H.sub.2c --C.sub.d F.sub.2d+1 in which a is 2-4, b is 0 or 1, c is 0-8 and d is 4-12, and compositions thereof with an oil, are useful as spreading agents and in agricultural applications.
摘要翻译：对应于下式的低聚氟代烷基硅氧烷：其中x为0至3，y为0,1或2; z为0或1; x + y> 0，R具有式-CaH2a-Ob-CdH2c-CdF2d + 1，其中a为2-4，b为0或1，c为0-8且d为4-12，其组成为有油，可用作扩散剂和农业应用。

10. 发明授权

US06410808B1 Method for producing a fluoroalcohol 有权
标题翻译：氟代醇的制造方法
公开(公告)号：US06410808B1
公开(公告)日：2002-06-25
申请号：US09840072
申请日：2001-04-24
申请人： Yutaka Furukawa , Nobuyuki Kasahara , Kazuya Oharu , Shin Tatematsu
发明人： Yutaka Furukawa , Nobuyuki Kasahara , Kazuya Oharu , Shin Tatematsu
IPC分类号： C07C3134
CPC分类号： C07C41/26 , C07C29/124 , C07C43/137 , C07C31/38
摘要： A method for producing a fluoroalcohol of the following formula 1a, which comprises reacting a compound of the following formula 1 with water in a liquid phase at a temperature of 150° C. or higher under a gauge pressure of 0.4 MPa or higher: wherein n is an integer of from 1 to 5, X is a chlorine atom, a bromine atom or an iodine atom, p is an integer of at least 1, and R is a p-valent organic group, provided that when p is 1, R may be a hydrogen atom or a halogen atom.
摘要翻译：一种下式1a的氟代醇的制造方法，其特征在于，在表压为0.4MPa以上的条件下，使下式1的化合物与液相中的水在150℃以上的温度下反应：其中n 为1〜5的整数，X为氯原子，溴原子或碘原子，p为1以上的整数，R为p价有机基团，条件是当p为1时，R 可以是氢原子或卤素原子。

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