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31. 发明授权

US4618714A Process for preparation of 3,3'- or 3,4'-diaminobenzophenones 失效
标题翻译：制备3,3'-或3,4'-二氨基二苯甲酮的方法
公开(公告)号：US4618714A
公开(公告)日：1986-10-21
申请号：US490546
申请日：1983-05-02
申请人： Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Saburo Kawashima , Akihiro Yamaguchi
发明人： Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Saburo Kawashima , Akihiro Yamaguchi
IPC分类号： C07B61/00 , B01J23/00 , B01J23/40 , B01J23/70 , B01J25/02 , B01J27/00 , B01J27/02 , B01J27/08 , C07C20060101 , C07C67/00 , C07C201/00 , C07C205/45 , C07C221/00 , C07C225/22 , C07C97/10
CPC分类号： C07C201/14 , C07C221/00
摘要： Preparation of 3,3'- or 3,4'-diaminobenzophenone by nitrating a chloronitrobenzophenone mixture obtained by the Friedel-Crafts reaction between 3- or 4-nitrobenzoyl chloride and chlorobenzene, and catalytically reducing and dechlorinating the resulting chlorodinitrobenzophenone mixture in the presence of a reduction catalyst and a dehydrochlorinating agent.
摘要翻译：通过硝化由3-或4-硝基苯甲酰氯与氯苯之间的Friedel-Crafts反应获得的氯硝基二苯甲酮混合物，并在所述氯代二硝基二苯甲酮混合物存在下催化还原和脱氯，从而制备3,3'-或3,4'-二氨基二苯甲酮还原催化剂和脱氯化氢剂。

32. 发明授权

US4380671A Process for the preparation of 2,2'-bis(4-substituted phenol)sulfides 失效
标题翻译：制备2,2'-双（4-取代苯酚）硫化物的方法
公开(公告)号：US4380671A
公开(公告)日：1983-04-19
申请号：US288428
申请日：1981-07-30
申请人： Akihiro Yamaguchi , Tadashi Kobayashi , Keizaburo Yamaguchi , Hisamichi Murakami
发明人： Akihiro Yamaguchi , Tadashi Kobayashi , Keizaburo Yamaguchi , Hisamichi Murakami
IPC分类号： C07C20060101 , C07C319/14 , C07C321/30 , C08K5/13 , C08K5/36 , C10M169/00 , C07C149/36
CPC分类号： C07C323/00
摘要： Disclosed is a process for the preparation of 2,2'-bis(4-substituted phenol)sulfides which comprises reacting a 4-substituted phenol with sulfur dichloride in a hydrocarbon solvent at a temperature of from -10.degree. to 40.degree. C. in the presence of a Lewis acid catalyst. For example, 2,2'-bis(4-cumylphenol)-sulfide, i.e. 2,2'-bis(4-.alpha.,.alpha.-dimethyl benzyl-phenol)monosulfide, which is a novel compound can be prepared by reacting 4-cumylphenol with sulfur dichloride in benzene at a temperature of from 0.degree.to 10.degree. C. in the presence of zinc chloride.
摘要翻译：公开了一种制备2,2'-双（4-取代苯酚）硫化物的方法，其包括使4-取代的苯酚与二氯化硫在烃溶剂中在-10℃至40℃的温度下反应存在路易斯酸催化剂。例如，作为新化合物的2,2'-双（4-枯基苯酚）硫化物，即2,2'-双（4-甲基-α，α-二甲基苄基 - 苯酚）单硫化物可以通过使4- 异丙苯酚与二氯化硫在苯中，在氯化锌存在下，在0〜10℃的温度下进行。

33. 发明授权

US06291600B1 Method of preventing scale adhesion to the surfaces of a polymerization tank 失效
标题翻译：防止水垢附着在聚合槽表面的方法
公开(公告)号：US06291600B1
公开(公告)日：2001-09-18
申请号：US08053974
申请日：1993-04-09
申请人： Seiichi Masuko , Ichisaburo Nakamura , Yoshimatsu Naka , Keiichi Fukuda , Akira Yamamoto , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
发明人： Seiichi Masuko , Ichisaburo Nakamura , Yoshimatsu Naka , Keiichi Fukuda , Akira Yamamoto , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
IPC分类号： C08F200
CPC分类号： C08F14/06 , C08F2/004
摘要： In a novel method of homo- or copolymerization of vinyl chloride, a specified coating agent is applied on the surfaces of the portions which will become into contact with the vinyl chloride monomer during the polymerization process. The coating agent is in a form of an aqueous solution of a modified condensation product of phenol and aldehyde, the pH of the solution being adjusted in a range that the product is dissolved at an ambient temperature upon coating of the solution and separates out of the solution upon being heated on the surfaces. The wall surface of the polymerization tank and the like is then coated with a thin film of the coating agent having a uniform thickness and being strongly adhered to the wall surface, thereby providing an excellent effect of preventing adhesion of the product polymer to the wall surface.
摘要翻译：在氯乙烯均聚或共聚的新方法中，在聚合过程中将在与氯乙烯单体接触的部分的表面上施加特定的涂布剂。涂层剂是苯酚和醛的改性缩合产物的水溶液形式，溶液的pH值在产物在环境温度下溶解的范围内被调节，并在分离出在表面上加热时的溶液。然后将聚合槽等的壁面用均匀厚度的涂布剂的薄膜涂布并牢固地附着在壁面上，从而提供优异的防止产品聚合物粘合到壁面上的效果。

34. 发明授权

US5470943A Polyimide 失效
标题翻译：聚酰亚胺
公开(公告)号：US5470943A
公开(公告)日：1995-11-28
申请号：US360584
申请日：1994-12-21
申请人： Yoshihiro Sakata , Wataru Yamashita , Yuichi Okawa , Shoji Tamai , Tsutomu Ishida , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Yoshihiro Sakata , Wataru Yamashita , Yuichi Okawa , Shoji Tamai , Tsutomu Ishida , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C08G73/10 , C08G77/10 , C07D213/69 , C08G69/26
CPC分类号： C08G73/1039 , C08G73/1085
摘要： This invention relates to a novel fluorine-containing polyimide or polyimide copolymer being colorless and having transparency and very low dielectric characteristics, and has a novel aromatic diamino compound used for the polyimide, a preparation process thereof, a polyimide-based resin composition comprising the polyimide or polyimide copolymer and a fibrous reinforcement, a process for preparing the resin composition, an injection molded article of the resin composition.The polyimide comprise a requisite structural unit having one or more recurring structural units of the formula: ##STR1## wherein Ar is a tetravalent radical having 6 to 27 carbon atoms and being selected from the group consisting of a monoaromatic radical, condensed polyaromatic radical and noncondensed polyaromatic radical having aromatic radicals connected to each other with a direct bond or a bridge member, a trifluoromethyl radical is situated at the 3- or the 4-position on a pyridine nucleus, and an imide nitrogen atom is connected at the 3- or the 4-position to an ether bond.The polyimide or polyimide copolymer has excellent heat resistance, outstanding melt-flow stability and greatly improved processability, and also is colorless and has high transparency and very low dielectric coefficient, and can be expected to be used as raw materials for electric.cndot.electronic appliances and optical instruments due to the above characteristics.
摘要翻译：本发明涉及一种新颖的含氟聚酰亚胺或聚酰亚胺共聚物，其具有透明性和非常低的介电特性，并且具有用于聚酰亚胺的新型芳族二氨基化合物及其制备方法，该聚酰亚胺系树脂组合物含有聚酰亚胺或聚酰亚胺共聚物和纤维增强剂，树脂组合物的制备方法，树脂组合物的注塑制品。聚酰亚胺包含具有一个或多个下式的重复结构单元的必需结构单元：其中Ar是具有6至27个碳原子的四价基团，并且选自单芳族基团，缩合多芳族基团具有芳族基团的自由基和非缩合多芳族基团彼此直接键合或桥接成员，三氟甲基位于吡啶核上的3-或4-位，酰亚胺氮原子连接在3 - 或4-位到醚键。聚酰亚胺或聚酰亚胺共聚物具有优异的耐热性，优异的熔体流动稳定性和极好的加工性，并且是无色的，具有高透明度和非常低的介电系数，并且可以预期用作电气电子设备的原料光学仪器由于上述特点。

35. 发明授权

US5147948A Method for polymerizing vinyl chloride while inhibiting adhesion to the polymerization reactor with coating from poly(hydricphenol sulfide) 失效
标题翻译：在聚合物（硫化氢）下，将聚氯乙烯聚合成聚合反应剂的方法，
公开(公告)号：US5147948A
公开(公告)日：1992-09-15
申请号：US631932
申请日：1990-12-21
申请人： Seiichi Masuko , Ichisaburo Nakamura , Keiichi Fukuda , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
发明人： Seiichi Masuko , Ichisaburo Nakamura , Keiichi Fukuda , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
IPC分类号： C08F14/06 , C08F2/00 , C08F2/20 , C08F14/00 , C09D181/02
CPC分类号： C08F2/004
摘要： A method for polymerizing vinyl chloride comprises polymerizing vinyl chloride in an aqueous medium or bulk-polymerizing vinyl chloride, wherein the inner wall of a polymerizer and parts of devices which come in contact with the monomer during the polymerization are coated, prior to the polymerization, with a reaction product having a molecular weight ranging from 500 to 100,000, obtained by condensing a polyhydric phenol and sulfur dichloride in the presence of a Lewis acid as a catalyst. The amount of the polymer adhered to the polymerizer during polymerization of vinyl chloride is substantially lowered and the adhered polymer can be easily washed away through simple water washing according to the foregoing method. Moreover, the method does not adversely affect the reaction time and the quality of the resulting product at all.

36. 发明授权

US5077436A Bis(3-aminophenoxy) aromatics and method of preparing the same 失效
标题翻译：双（3-氨基苯氧基）芳烃及其制备方法
公开(公告)号：US5077436A
公开(公告)日：1991-12-31
申请号：US831547
申请日：1986-02-21
申请人： Yukihiro Yoshikawa , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Akihiro Yamaguchi
发明人： Yukihiro Yoshikawa , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Akihiro Yamaguchi
IPC分类号： C04B7/32 , C04B7/345 , C04B28/02 , C07C205/38 , C07C217/90
CPC分类号： C07C213/02 , C07C201/12 , C07C319/20 , C07C2103/94
摘要： Bis(3-nitrophenoxy) derivatives of aromatic or bridged aromatic hydrocarbons are derived from m-dinitrobenzene and dihydroxy derivatives of said hydrocarbons and certain substituted derivatives thereof by a condensation reaction in dipolar aprotic solvents in the presence of bases. The bis(3-nitrophenoxy) derivatives and derivatives obtained are successively reduced to afford bis-(3-aminophenoxy)derivatives. This is a new method for reacting the dihydroxy-derivatives with m-dinitrobenzene, and hence can prepare novel bis(3-aminophenoxy) derivatives such as 4,4'-bis(3-amino-phenoxy)biphenyl, 1-[4-(3-aminophenoxy)phenyl]-1,3,3-trimethyl-6-(3-aminophenoxy)indan, 6,6'-bis(3-aminophenoxy)3,3,3',3'-tetramethyl-1,1'spirobiindan, and methyl substituted 2,2'-bis[4-(3-aminophenoxy)phenyl]propane.
摘要翻译：芳基或桥连芳烃的双（3-硝基苯氧基）衍生物衍生自所述烃的间二硝基苯和二羟基衍生物及其取代的衍生物，其在碱存在的情况下通过偶极非质子溶剂中的缩合反应。将所得的双（3-硝基苯氧基）衍生物和衍生物连续地还原得到双 - （3-氨基苯氧基）衍生物。这是使二羟基衍生物与间二硝基苯反应的新方法，因此可以制备新的双（3-氨基苯氧基）衍生物，如4,4'-双（3-氨基 - 苯氧基）联苯，1- [4- （3-氨基苯氧基）苯基] -1,3,3-三甲基-6-（3-氨基苯氧基）茚满，6,6'-双（3-氨基苯氧基）3,3,3'，3'-四甲基-1， 1'-螺二茚并和甲基取代的2,2'-双[4-（3-氨基苯氧基）苯基]丙烷。

37. 发明授权

US5051494A Thermosetting resin composition comprising an aromatic amine 失效
标题翻译：包含芳族胺的热固性树脂组合物
公开(公告)号：US5051494A
公开(公告)日：1991-09-24
申请号：US511235
申请日：1990-04-19
申请人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatshuiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
发明人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatshuiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
IPC分类号： C07C211/50 , C08G73/12
CPC分类号： C08G73/121 , C07C211/50
摘要： The invention relates to an aromatic amine resin comprising a mixture of aromatic amine compounds represented by the following general formula (a): ##STR1## wherein A represents a phenylene, alkyl-substituted phenylene, diphenylene, diphenyl ether or naphthylenyl group, R.sup.1 represents a halogen atom or a hydroxyl C.sub.1-4 alkoxy or C.sub.1-5 alkyl group, l is 1 or 2, m is 0, 1, 2 or 3, n is an integer from 0 to 300 and when m is 2 or 3, the R.sup.1 group may be the same or different and may join to form a 5- or 6-membered alicyclic moiety which may optionally contain one or more side chains, and also relates to processes for producing the same and a thermosetting composition containing the same.

38. 发明授权

US5013848A Aromatic bismaleimide derivatives and process for preparing same 失效
标题翻译：芳香双马来酰亚胺衍生物及其制备方法
公开(公告)号：US5013848A
公开(公告)日：1991-05-07
申请号：US87255
申请日：1987-07-22
申请人： Yukihiro Yoshikawa , Midori Yamazaki , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Akihiro Yamaguchi
发明人： Yukihiro Yoshikawa , Midori Yamazaki , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe , Akihiro Yamaguchi
IPC分类号： C07D207/44 , C07D207/452
CPC分类号： C07D207/452
摘要： A novel aromatic bismaleimide of the formula (I): ##STR1## wherein X is ##STR2## where R.sub.1 R.sub.2, R.sub.3 and R.sub.4 are a hydrogen atom or a methyl group. The bismaleimide is prepared by reacting an aromatic diamine having the formula (II): ##STR3## wherein X is the same as in the formula (I), with maleic anhydride and then conducting the ring-closing reaction of the resultant aromatic bismaleamic acid.

39. 发明授权

US4966961A Polymaleimide from polyarylene polyamine and process for the preparation thereof 失效
标题翻译：聚亚芳基多胺的聚马来酰亚胺及其制备方法
公开(公告)号：US4966961A
公开(公告)日：1990-10-30
申请号：US351705
申请日：1989-05-15
申请人： Yoshimitsu Tanabe , Keizaburo Yamaguchi , Tatsuhiro Urakami , Akihiro Yamaguchi
发明人： Yoshimitsu Tanabe , Keizaburo Yamaguchi , Tatsuhiro Urakami , Akihiro Yamaguchi
IPC分类号： C07D207/448 , C07D207/44 , C07D207/452 , C08G73/10 , C08G73/12
CPC分类号： C07D207/452 , C08G73/121
摘要： The present invention relates to polymaleimide compounds having the following chemical structure: ##STR1## wherein n represents an integer of from 0 to about 50 and to a process for preparing the same.

40. 发明授权

US4937318A Aromatic amine resins 失效
标题翻译：芳香族胺树脂
公开(公告)号：US4937318A
公开(公告)日：1990-06-26
申请号：US254701
申请日：1988-10-07
申请人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatsuhiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
发明人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatsuhiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
IPC分类号： C07C211/50 , C08G73/12
CPC分类号： C08G73/121 , C07C211/50
摘要： The invention relates to an aromatic amine resin comprising a mixture of aromatic amine compounds represented by the following general formula (a): ##STR1## wherein A represents a phenylene, alkyl-substituted phenylene, diphenylene, diphenyl ether or napthylenyl group, R.sup.1 represents a halogen atom or a hydroxyl C.sub.1-4 alkoxy or C.sub.1 -5 alkyl group, l is 1 or 2, m is 0, 1, 2 or 3, n is an integer from 0 to 300 and when m is 2 or 3, the R.sup.1 group may be same or different and may join to form a 5- to 6-membered alicyclic moiety which may optionally contain one or more side chains, and also relates to processes for producing the same and a thermosetting composition containing the same.

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