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21. 发明授权

US4349514A Process for recovery of reusable chromic acid from the waste chromic acid solution containing impurities 失效
标题翻译：从含有杂质的废铬酸溶液中回收可重复使用的铬酸的方法
公开(公告)号：US4349514A
公开(公告)日：1982-09-14
申请号：US66167
申请日：1979-08-13
申请人： Morio Watanabe , Sanji Nishimura
发明人： Morio Watanabe , Sanji Nishimura
IPC分类号： B01D11/04 , C01G37/00 , C01G37/033 , C01G37/14 , C02F1/469 , C23C22/86 , C25B1/00 , C25D21/16 , C25F7/02 , B01D11/00
CPC分类号： B01D61/44 , C01G37/003 , C25B1/00 , B01D2311/04 , C02F1/469 , C02F2101/22 , Y10S204/13 , Y10S210/913
摘要： A process for recovery of reusable chromic acid from waste chromic acid solution containing impurities, which process comprises a first step in which the solution containing chromic acid is introduced into the cathode compartment in an electro-dialysis process and free chromic acid or chromate ions in the above solution are transferred to the anode compartment, a second step in which H.sub.2 SO.sub.4 is added in at least equivalent amounts to the heavy metallic ion contained in the outlet solution, in which chromic acid ion concentration is reduced, in order to convert chemical species of the contained metallic ion and increase the H.sup.+ ion concentration and then chromate ions in the resultant solution are extracted into an organic phase with contact of an organic solvent (A), and a third step in which residual amounts of chromic acid ion remaining in the aqueous raffinate from the second step are extracted into an organic phase with contact of an organic solvent (B). Organic solvents A and B are regenerated by stripping the organic phase with a suitable strip reagent.
摘要翻译：从含有杂质的废铬酸溶液中回收可再利用的铬酸的方法，该方法包括第一步骤，其中将含有铬酸的溶液在电渗析过程中引入阴极室，并且将游离的铬酸或铬酸根离子将上述溶液转移到阳极室，第二步骤，其中以至少等量的量加入H 2 SO 4，其中所述重金属离子包含在出口溶液中，其中铬酸离子浓度降低，以便将化学物质转化为含有金属离子并增加H +离子浓度，然后将所得溶液中的铬酸根离子与有机溶剂（A）接触而萃取到有机相中，并且残留在残液中的残余量的铬酸离子的第三步骤从有机溶剂（B）与第二步骤萃取到有机相中。有机溶剂A和B通过用合适的剥离试剂汽提有机相来再生。

22. 发明授权

US5597398A Process for producing glass preform for optical fiber 失效
标题翻译：光纤用玻璃预制棒的制造方法
公开(公告)号：US5597398A
公开(公告)日：1997-01-28
申请号：US260747
申请日：1994-06-15
申请人： Shinji Ishikawa , Yoshiki Chigusa , Motonori Nakamura , Yoshinori Makio , Morio Watanabe
发明人： Shinji Ishikawa , Yoshiki Chigusa , Motonori Nakamura , Yoshinori Makio , Morio Watanabe
IPC分类号： C03B37/014 , C03B37/018
CPC分类号： C03B37/0148 , Y02P40/57
摘要： A process for producing a porous glass preform for optical fiber by depositing fine glass particles on an outer surface of a glass material while moving the glass material, including the steps of: preheating a portion of the glass material for not less than 5 minutes to clean the portion of the glass material in an apparatus for depositing fine glass particles; and depositing fine glass particles on the portion of the glass material cleaned by the preheating, in the apparatus for depositing fine glass particles.
摘要翻译：一种通过在移动玻璃材料的同时在玻璃材料的外表面上沉积微细玻璃颗粒而制造光纤用多孔玻璃预制件的方法，包括以下步骤：将玻璃材料的一部分预热至少5分钟以进行清洁用于沉积细微玻璃颗粒的装置中的玻璃材料部分; 以及在用于沉积微细玻璃颗粒的装置中，通过预热清洁的玻璃材料的部分上沉积微细玻璃颗粒。

23. 发明授权

US5277816A Process for producing titanium dioxide 失效
标题翻译：二氧化钛生产工艺
公开(公告)号：US5277816A
公开(公告)日：1994-01-11
申请号：US756481
申请日：1991-09-09
申请人： Morio Watanabe
发明人： Morio Watanabe
IPC分类号： C01G23/00 , C01G23/053 , B01D11/04
CPC分类号： C01G23/0532 , C01G23/001
摘要： A process for producing titanium dioxide which discharges no waste is disclosed. In a first step, a sulfuric acid solution containing titanium ion with one or more kinds of metal ions is contacted with a first organic solvent to extract the titanium ion as a sulfuric acid complex. The organic solvent containing the extracted titanium as a sulfuric acid complex (titanyl sulfate) is contacted with an aqueous liquid to strip the titanium into the aqueous liquid and regenerate the first organic solvent. In a second step, the aqueous liquid containing the titanium is subjected to hydrolysis to form insoluble titanium hydroxide, and the titanium hydroxide is washed with dilute sulfuric acid and/or clear water. In a third step, the raffinate of extraction in the first step is contacted with a second organic solvent to extract the titanium ion and the organic solvent containing extracted titanium is contacted with water, dilute sulfuric acid solution or a dilute titanyl sulfate solution to strip the titanium, and regenerate the organic solvent.
摘要翻译：公开了一种不排出废物的生产二氧化钛的方法。在第一步骤中，将含有一种或多种金属离子的钛离子的硫酸溶液与第一有机溶剂接触以提取作为硫酸络合物的钛离子。将含有作为硫酸络合物（硫酸氧钛）的提取的钛的有机溶剂与含水液体接触以将钛剥离到水性液体中并再生第一有机溶剂。在第二步骤中，将含有钛的含水液体进行水解以形成不溶性氢氧化钛，并用稀硫酸和/或清水洗涤氢氧化钛。在第三步骤中，将第一步骤中的萃取液与第二有机溶剂接触以提取钛离子，并将含有萃取的钛的有机溶剂与水，稀硫酸溶液或稀硫酸硫酸盐溶液接触以剥离钛，并再生有机溶剂。

24. 发明授权

US4952378A Method for neutralization treatment of sulfuric acid containing iron ions 失效
标题翻译：含铁离子中和处理方法
公开(公告)号：US4952378A
公开(公告)日：1990-08-28
申请号：US212439
申请日：1988-06-28
申请人： Morio Watanabe , Renpei Sei
发明人： Morio Watanabe , Renpei Sei
IPC分类号： C01G49/10 , B01D11/04 , C01B17/90 , C01B17/96 , C01D5/02 , C01G49/00 , C02F1/26 , C02F1/66
CPC分类号： C01G49/0009 , C01B17/903 , C02F1/26 , C02F1/66 , Y10S423/02 , Y10S423/14
摘要： A method for neutralization of sulfuric acid containing Fe ions, comprising adding ions selected from the group consisting of Na ions, K ions, Mg ions, Ca ions and NH.sub.4 ions in the form of a compound containing chlorine to a sulfuric acid solution to be treated in an amount corresponding at least to the chemical equivalent to SO.sub.4.sup.2-, and bringing the resultant solution into contact with an organic solvent containing oxygen or comprising alkylamine for extracting Fe ions from said aqueous solution into the organic phase as chloride complex. Iron chloride can be recovered from the organic phase by distilling or evaporating the organic solvent or by extracting back it into water.
摘要翻译：一种中和含有Fe离子的硫酸的方法，包括将含有氯化合物形式的Na离子，K离子，Mg离子，Ca离子和NH4离子的离子添加到待处理的硫酸溶液中其量至少相当于SO42-的化学当量，并使得到的溶液与含氧或包含烷基胺的有机溶剂接触，以将Fe离子从所述水溶液中提取到作为氯化物络合物的有机相中。通过蒸馏或蒸发有机溶剂或通过将其萃取回水中，可以从有机相中回收氯化铁。

25. 发明授权

US4434518A Sport shoes 失效
标题翻译：运动鞋
公开(公告)号：US4434518A
公开(公告)日：1984-03-06
申请号：US353799
申请日：1982-03-02
申请人： Morio Watanabe
发明人： Morio Watanabe
IPC分类号： A43B5/00 , A43B9/12 , A43B13/04 , A43B13/12 , A43B13/32 , B29D35/12 , A43C13/08
CPC分类号： B29D35/122 , A43B13/04 , A43B13/12 , A43B5/00 , A43B9/12
摘要： A sport shoe in which the shoe sole is bonded to an insert layer during the formation of the shoe sole by injection-molding and the assembly of the shoe sole and the insert layer is secured to the shoe upper by an adhesive applied between the insert layer and the shoe upper.
摘要翻译：一种运动鞋，其中鞋底通过注射成型在鞋底形成期间结合到插入层，并且鞋底和插入层的组装通过施加在插入层之间的粘合剂固定到鞋上和鞋面。

26. 发明授权

US4390508A Process for recovery of aluminum oxide from aluminum compounds containing fluorine 失效
标题翻译：从含氟化合物的铝化合物中回收氧化铝的方法
公开(公告)号：US4390508A
公开(公告)日：1983-06-28
申请号：US333294
申请日：1981-12-22
申请人： Morio Watanabe , Sanji Nishimura , Nobuatsu Watanabe
发明人： Morio Watanabe , Sanji Nishimura , Nobuatsu Watanabe
IPC分类号： C01F7/02 , C01F7/30 , C01F7/50 , C22B3/30 , C22B3/32 , C22B3/38 , C22B3/40
CPC分类号： C22B3/0068 , C01F7/30 , C01F7/50 , C22B3/0017 , C22B3/0024 , C22B3/0077 , C22B3/0087 , C22B3/0089 , C22B3/0093 , C22B3/0095 , Y02P10/234
摘要： A process for the production of aluminum oxide from aluminum compounds containing fluorine comprising:(1) extracting aluminum ions with an organic solvent containing one or more compounds selected from the groups of alkyl phosphoric acid, alkyl and aryl thio phosphoric acid, carboxylic acid and hydroxime together with a petroleum hydrocarbon as a diluent;(2) preparing aluminum compounds containing fluorine by stripping the aluminum ions in the resultant organic solvent from the step (1) in contact with an aqueous solution containing one or more compounds selected from the groups of HF, NH.sub.4 HF.sub.2, NH.sub.4 F or KHF.sub.2 and simultaneously regenerating the organic solvent; and(3) producing aluminum oxide by heating the resultant aluminum compounds containing fluorine from the step (2) in gas stream containing oxygen or H.sub.2 O.
摘要翻译：一种由含氟的铝化合物生产氧化铝的方法，包括：（1）用含有一种或多种选自烷基磷酸，烷基和芳基硫代磷酸，羧酸和氢氧基的化合物的有机溶剂萃取铝离子与石油烃一起作为稀释剂; （2）通过从所述步骤（1）中剥离所得有机溶剂中的铝离子与含有一种或多种选自HF，NH 4 HF 2，NH 4 F或KHF 2的化合物的水溶液接触来制备含氟化合物，同时再生有机溶剂; 和（3）通过在含有氧或H 2 O的气流中加热来自步骤（2）的所得的含氟铝化合物来生产氧化铝。

27. 发明授权

US4144145A Process for recovery of reusable chromic acid from the waste chromic acid solution containing impurities 失效
公开(公告)号：US4144145A
公开(公告)日：1979-03-13
申请号：US786770
申请日：1977-04-12
申请人： Morio Watanabe , Sanji Nishimura
发明人： Morio Watanabe , Sanji Nishimura
IPC分类号： B01D11/04 , C01G37/00 , C01G37/033 , C01G37/14 , C02F1/469 , C23C22/86 , C25B1/00 , C25D21/16 , C25F7/02 , B01D11/00 , C01G37/12
CPC分类号： B01D61/44 , C01G37/003 , C25B1/00 , B01D2311/04 , C02F1/469 , C02F2101/22 , Y10S204/13 , Y10S210/913
摘要： A process for recovery of reusable chromic acid from waste chromic acid solution containing impurities, which process comprises a first step in which the solution containing chromic acid is introduced into the cathode compartment in an electro-dialysis process and free chromic acid or chromate ions in the above solution are transferred to the anode compartment, a second step in which H.sub.2 SO.sub.4 is added in at least equivalent amounts to the heavy metallic ion contained in the outlet solution, in which chromic acid ion concentration is reduced, in order to convert chemical species of the contained metallic ion and increase the H.sup.+ ion concentration and then chromate ions in the resultant solution are extracted into an organic phase with contact of an organic solvent (A), and a third step in which residual amounts of chromic acid ion remaining in the aqueous raffinate from the second step are extracted into an organic phase with contact of an organic solvent (B). Organic solvents A and B are regenerated by stripping the organic phase with a suitable strip reagent.

28. 发明授权

US4113588A Process for recovery of waste H.sub.2 SO.sub.4 and HCl 失效
标题翻译：回收废水的方法H {HD 2 {B SO {HD 4 {B和HCl
公开(公告)号：US4113588A
公开(公告)日：1978-09-12
申请号：US773657
申请日：1977-03-02
申请人： Morio Watanabe , Sanji Nishimura
发明人： Morio Watanabe , Sanji Nishimura
IPC分类号： C01B7/00 , C01B7/01 , C01B17/90 , C01G49/00 , C01G49/06 , C23G1/36 , C25C1/06 , C25B1/22
CPC分类号： C25C1/06 , C01B17/902 , C01B17/903 , C01B7/01 , C01G49/0009 , C01G49/06 , C23G1/36 , Y10S423/14
摘要： This invention relates to a process for recovery of waste H.sub.2 SO.sub.4 and HCl which are used for pickling metallic materials and articles and contain a large quantities of Fe ions. Furthermore, it offers a process for the recovery of H.sub.2 SO.sub.4 and HCl from waste H.sub.2 SO.sub.4 which contains large amounts of Fe ions after removal of Ti ions by a hydrolysis process in the production of TiO.sub.2 and also for the recovery of high-purity electrolytic iron or iron hydroxide.
摘要翻译：本发明涉及回收用于酸洗金属材料和制品并含有大量Fe离子的废H2SO4和HCl的方法。此外，它提供了一种从废物H2SO4中回收H2SO4和HCl的方法，其中通过在制备TiO 2中的水解过程除去Ti离子之后含有大量的Fe离子，并且还用于回收高纯度电解铁或铁氢氧化物。

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