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11. 发明授权

US07740944B2 Multilayer coating 有权
标题翻译：多层涂层
公开(公告)号：US07740944B2
公开(公告)日：2010-06-22
申请号：US10469132
申请日：2002-03-01
申请人： Zen Komiya , Masahito Mase , Junji Yoshizawa , Takashi Ukachi
发明人： Zen Komiya , Masahito Mase , Junji Yoshizawa , Takashi Ukachi
IPC分类号： B32B27/40 , C08F2/46
CPC分类号： C03C17/3405 , C03C25/1065 , C03C25/50 , Y10T428/31504 , Y10T428/31554
摘要： The present invention relates to a multilayer coating in which a plurality of photocurable resin cured films are layered on a substrate, wherein at least two adjacent layers comprise the same hindered phenol-type antioxidant.The multilayer coating can be applied onto a substrate, such as glass fibers, vinyl chloride sheets, polycarbonate sheets, glass plates, polyethylene films, wood, acrylic sheets, metal plates, and the like.
摘要翻译：本发明涉及一种多层涂层，其中多个光固化树脂固化膜层叠在基底上，其中至少两个相邻层包含相同的受阻酚型抗氧化剂。可以将多层涂层涂布在基材上，例如玻璃纤维，氯乙烯片，聚碳酸酯片，玻璃板，聚乙烯薄膜，木材，丙烯酸片，金属板等。

12. 发明申请

US20050272829A1 Curable liquid resin composition 审中-公开
标题翻译：可固化液体树脂组合物
公开(公告)号：US20050272829A1
公开(公告)日：2005-12-08
申请号：US10507016
申请日：2003-03-27
申请人： Masanobu Sugimoto , Hideki Sugimoto , Takeo Shigemoto , Zen Komiya , Takashi Ukachi
发明人： Masanobu Sugimoto , Hideki Sugimoto , Takeo Shigemoto , Zen Komiya , Takashi Ukachi
IPC分类号： G02B6/44 , C03C25/10 , C08F283/00 , C08F283/06 , C08F290/06 , C08G18/48 , C08G18/67 , C09D175/16 , C08G2/00
CPC分类号： C09D175/16 , C03C25/1065 , C08F283/006 , C08F283/06 , C08G18/4854 , C08G18/672 , C08G18/48
摘要： This invention relates to a curable liquid resin composition comprising: (a) 5-94 parts by weight of a urethane (meth)acrylate comprising a polyether backbone, at least one urethane group and at least one (meth)acrylate end group (b) 5-94 parts by weight of a polymerizable monomer, and; (c) 0.01-10 parts by weight of a photoinitiator, in 100 parts by weight of the curable liquid resin composition, wherein the cured product of the composition has a glass transition temperature between 30 and 85° C. or less and a stress relaxation time of 30 minutes or less.
摘要翻译：本发明涉及一种可固化液体树脂组合物，其包含：（a）5-94重量份的包含聚醚主链，至少一个氨基甲酸酯基和至少一个（甲基）丙烯酸酯端基（b）的氨基甲酸酯（甲基）丙烯酸酯， 5-94重量份的可聚合单体，和（c）0.01-10重量份的光引发剂，在100重量份的可固化液体树脂组合物中，其中组合物的固化产物的玻璃化转变温度为30-85℃或更低，应力松弛时间30分钟以内。

13. 发明申请

US20050228063A1 Radiation curable resin composition 审中-公开
公开(公告)号：US20050228063A1
公开(公告)日：2005-10-13
申请号：US11038572
申请日：2005-01-21
申请人： Zen Komiya , Adrianus Abel , Duurt Alkema , Masahito Mase , Takashi Ukachi
发明人： Zen Komiya , Adrianus Abel , Duurt Alkema , Masahito Mase , Takashi Ukachi
IPC分类号： C03C25/10 , C08F2/46 , C08F2/48 , C08F283/00 , C08F290/06 , C08F290/14 , C08G2/00 , C08G18/28 , C08G18/48 , C08G18/67 , C09D175/16
CPC分类号： C09D175/16 , C03C25/106 , C03C25/1065 , C08F283/006 , C08F290/06 , C08F290/067 , C08F290/14 , C08F290/147 , C08G18/289 , C08G18/4866 , C08G18/672 , Y10T428/19 , Y10T428/2938 , Y10T428/294 , Y10T428/2942 , Y10T428/2956 , Y10T428/31645 , C08G18/48 , C08G18/40
摘要： The present invention provides a curable composition, comprising: a (meth)acrylate urethane compound derived from a polypropylene glycol or a propyleneoxide ethyleneoxide copolymer glycol having a molecular weight between 1,000 and 13,000 and an amount of unsaturation less than 0.01 meq/g. The liquid curable resin composition of the present invention has improved liquid stability and can produce cured products having superior mechanical characteristics by polymerization. The composition further comprises preferably a primary or secondary amine. The liquid curable resin composition can be used as a coating material for optical fibers, adhesives, and the like. The composition is particularly suitable as a coating material for optical fibers for which long-term stability is required.

14. 发明授权

US5913004A Optical glass fiber coating composition 失效
标题翻译：光学玻璃纤维涂料组合物
公开(公告)号：US5913004A
公开(公告)日：1999-06-15
申请号：US840169
申请日：1997-04-14
申请人： Hideaki Takase , Mitsuhito Suwa , Zen Komiya , Takashi Ukachi
发明人： Hideaki Takase , Mitsuhito Suwa , Zen Komiya , Takashi Ukachi
IPC分类号： C03C25/10 , C08F290/06 , C08G18/10 , C08G18/67 , C09D175/16 , G02B6/02 , G02B6/16
CPC分类号： C09D175/16 , C03C25/106 , C08F290/067 , C08G18/10 , C08G18/672
摘要： Provided is an optical glass fiber coating composition which when coated on an optical glass fiber and suitably cured provides a coating having the combination of properties (i) through (iv):(i) a stable tensile modulus that is low at room temperature and over a broad range of temperatures below room temperature,(ii) an adhesion to the optical glass fiber sufficient to prevent structural defects and microbending in the optical glass fiber,(iii) the capability of being removed by stripping from the optical glass fiber substantially no residue left on the optical glass fiber, and(iv) which satisfies each of the following inequalities (I) and (II),X.ltoreq.0.2 kg/mm.sup.2 (I)X/Y.gtoreq.1/10 (II) wherein X is the tensile modulus (kg/mm.sup.2) measured at 23.degree. C. and Y is the tensile modulus (kg/mm.sup.2) measured at -40.degree. C.,This coating composition comprises:(A) a urethane (meth)acrylate formed from,(a) a diol compound containing at least one structure represented by one of the following formulas (1) and (2), ##STR1## (b) a compound containing two isocyanate groups, and (c) a compound containing a (meth)acrylate group and a hydroxy group;(B) a second (meth)acrylate-containing compound of which the homopolymer has a glass transition temperature of at most about 0.degree. C.; and(C) a polymerization initiator.
摘要翻译：提供了一种光学玻璃纤维涂料组合物，其在光学玻璃纤维上涂覆并适当固化时提供了具有性能（i）至（iv）的组合的涂层：（i）在室温和过高时稳定的拉伸模量低于室温的宽范围的温度，（ii）足以防止光学玻璃纤维中的结构缺陷和微弯曲的光学玻璃纤维的粘附，（iii）通过从光学玻璃纤维剥离而基本上没有残留物的去除能力留下在光学玻璃纤维上，和（iv）满足以下不等式（I）和（II）中的每一个，X <= 0.2kg / mm 2（I）X / Y> / = 1/10（II）其中 X为在23℃下测定的拉伸弹性模量（kg / mm2），Y为在-40℃下测定的拉伸弹性模量（kg / mm2）。该涂料组合物包含：（A）形成的氨基甲酸酯（甲基）由（a）含有由下述式（1）表示的至少一种结构的二醇化合物a nd（2），（b）含有2个异氰酸酯基的化合物，（c）含有（甲基）丙烯酸酯基和羟基的化合物; （B）第二（甲基）丙烯酸酯化合物，其均聚物的玻璃化转变温度为至多约0℃; 和（C）聚合引发剂。

15. 发明授权

US07214431B2 Two-layer film formed of radiation cured resin compositions and methods of making the same 有权
标题翻译：由辐射固化树脂组合物形成的两层膜及其制备方法
公开(公告)号：US07214431B2
公开(公告)日：2007-05-08
申请号：US10240559
申请日：2001-04-03
申请人： Zen Komiya , Takashi Ukachi
发明人： Zen Komiya , Takashi Ukachi
IPC分类号： B32B9/04 , B32B9/00 , B32B17/10 , B05D5/00 , G02B6/00
CPC分类号： C09D175/16 , C03C25/106 , C03C25/1065 , C08F290/147 , C08G18/3215 , C08G18/4854 , C08G18/672 , C09D4/00 , C09D4/06 , Y10T428/31504 , Y10T428/31507 , Y10T428/31551 , Y10T428/31554 , Y10T428/31645 , C08G18/6674 , C08F222/1006 , C08F290/067
摘要： The invention relates to a liquid curable resin composition capable of forming a ribbon matrix material which can be completely removed from a coloring layer when separating the optical fiber ribbon. A liquid curable resin composition comprising: (1) 30–80 wt. % of a urethane (meth)acrylate produced by reacting (A) a polyol compound, (B) a polyisocyanate compound, and (C) a (meth)acrylate compound containing a hydroxyl group, (2) 0.01–10 wt % of 2-methly-1-[4-(methylthio)phenyl]-2-morpholino-propan-1-one, and (3) 10–70 wt. % of a polymerizable diluent comprising a polymerizable monofunctional vinyl monomer which is copolymerizable with the component (1), wherein a two-layer film, which is obtained by applying the composition to a cured film of a UV-curable resin comprising the compound shown by the above formula (1) and curing the composition, has a T-peel strength of about 1.8 g/cm or less.
摘要翻译：本发明涉及一种能够形成在分离光纤带时可以从着色层完全除去的带状基体材料的液体可固化树脂组合物。一种液体可固化树脂组合物，其包含：（1）30-80重量％通过（A）多元醇化合物，（B）多异氰酸酯化合物和（C）含羟基的（甲基）丙烯酸酯化合物反应制得的氨基甲酸酯（甲基）丙烯酸酯，（2）0.01-10重量％ - 甲基-1- [4-（甲硫基）苯基] -2-吗啉代 - 丙-1-酮，和（3）10-70wt。％的可聚合稀释剂，其包含可与组分（1）共聚的可聚合单官能乙烯基单体，其中通过将组合物施加到包含以下化合物的UV固化树脂的固化膜上获得的双层膜：上述式（1）和固化组合物的T剥离强度为约1.8g / cm 3以下。

16. 发明授权

US06528553B1 Radiation curable resin composition 失效
标题翻译：辐射固化树脂组合物
公开(公告)号：US06528553B1
公开(公告)日：2003-03-04
申请号：US09620367
申请日：2000-07-20
申请人： Zen Komiya , Adrianus G. M. Abel , Duurt P. W. Alkema , Masahito Mase , Takashi Ukachi
发明人： Zen Komiya , Adrianus G. M. Abel , Duurt P. W. Alkema , Masahito Mase , Takashi Ukachi
IPC分类号： C08F248
CPC分类号： C09D175/16 , C03C25/106 , C03C25/1065 , C08F283/006 , C08F290/06 , C08F290/067 , C08F290/14 , C08F290/147 , C08G18/289 , C08G18/4866 , C08G18/672 , Y10T428/19 , Y10T428/2938 , Y10T428/294 , Y10T428/2942 , Y10T428/2956 , Y10T428/31645 , C08G18/48 , C08G18/40
摘要： The present invention provides a curable composition, comprising: a (meth)acrylate urethane compound derived from a polypropylene glycol or a propyleneoxide ethyleneoxide copolymer glycol having a molecular weight between 1,000 and 13,000 and an amount of unsaturation less than 0.01 meq/g. The liquid curable resin composition of the present invention has improved liquid stability and can produce cured products having superior mechanical characteristics by polymerization. The composition further comprises preferably a primary or secondary amine. The liquid curable resin composition can be used as a coating material for optical fibers, adhesives, and the like. The composition is particularly suitable as a coating material for optical fibers for which long-term stability is required.
摘要翻译：本发明提供一种可固化组合物，其包含：衍生自分子量为1,000至13,000的聚丙二醇或环氧丙烷环氧乙烷共聚物二醇的（甲基）丙烯酸酯氨基甲酸酯化合物，并且不饱和度的量小于0.01meq / g。本发明的液体固化型树脂组合物具有改善的液体稳定性，可以通过聚合制造具有优异的机械特性的固化物。组合物还优选包含伯胺或仲胺。液体固化性树脂组合物可以用作光纤，粘合剂等的涂料。该组合物特别适用于需要长期稳定性的光纤用涂料。

17. 发明授权

US06359025B1 Radiation-curable liquid resin composition for coating optical fibers 有权
标题翻译：用于涂覆光纤的可辐射固化液体树脂组合物
公开(公告)号：US06359025B1
公开(公告)日：2002-03-19
申请号：US09514309
申请日：2000-02-28
申请人： Paul Eugene Snowwhite , Timothy Edward Bishop , David Michael Szum , Zen Komiya , Miyuki Ishikawa , Takashi Ukachi
发明人： Paul Eugene Snowwhite , Timothy Edward Bishop , David Michael Szum , Zen Komiya , Miyuki Ishikawa , Takashi Ukachi
IPC分类号： C08F246
CPC分类号： C08G18/672 , C03C25/106 , C08G18/48 , C08G18/40
摘要： A radiation-curable composition for optical fiber coatings comprising about 10 wt. % to about 90 wt. % of at least one radiation-curable oligomer (A), about 10 wt. % to about 90 wt. % of at least one radiation-curable monomer diluent (B), and an effective amount of at least one photoinitiator (C) represented by formula (1): wherein Ar1 to Ar3 are aromatic groups which may have one or more substitution groups.
摘要翻译：一种用于光纤涂层的可辐射固化组合物，其包含约10wt。％至约90wt。％的至少一种可辐射固化的低聚物（A），约10wt。％至约90wt。至少一种可辐射固化的单体稀释剂（B）的％，和有效量的由式（1）表示的至少一种光引发剂（C）：其中Ar 1至Ar 3是可具有一个或多个取代基的芳族基团。

18. 发明授权

US5986018A Liquid curable resin compositions 失效
标题翻译：液体固化树脂组合物
公开(公告)号：US5986018A
公开(公告)日：1999-11-16
申请号：US26676
申请日：1998-02-20
申请人： Yoshikazu Yamaguchi , Zen Komiya , Takashi Ukachi
发明人： Yoshikazu Yamaguchi , Zen Komiya , Takashi Ukachi
IPC分类号： G02B6/44 , C03C25/24 , C08F299/06 , C08L75/16 , C08L83/04 , C09D4/06 , C09D133/14 , C09D175/16 , C08F283/04
CPC分类号： C09D133/14 , C09D175/16 , C09D4/06
摘要： A liquid curable resin composition comprising a dialkylpolysiloxane particles with at least two urethane bonds and/or urea bonds in the terminal groups. The resin composition exhibits superior shelf life in a liquid state and produces cured products having a slippery surface. It is suitable as a coating material for optical fibers, particularly as a ribbon matrix material and a bundling material.
摘要翻译：一种液体固化树脂组合物，其包含端基中具有至少两个氨基甲酸酯键和/或脲键的二烷基聚硅氧烷颗粒。树脂组合物在液态下表现出优异的保质期，并产生具有光滑表面的固化产物。它适合用作光纤的涂料，特别是作为带状基体材料和捆扎材料。

19. 发明授权

US5804311A Liquid curable resin composition for optical fibers 失效
标题翻译：光纤用液固树脂组合物
公开(公告)号：US5804311A
公开(公告)日：1998-09-08
申请号：US701428
申请日：1996-08-22
申请人： Mitsuhito Suwa , Zen Komiya , Yuji Takasugi , Takashi Ukachi
发明人： Mitsuhito Suwa , Zen Komiya , Yuji Takasugi , Takashi Ukachi
IPC分类号： C03C25/10 , C03C25/28 , C09D4/06 , G02B6/02 , C08F265/02 , C08F265/08
CPC分类号： C09D4/06 , C03C25/106 , C03C25/28 , Y10T428/2933 , Y10T428/2938
摘要： A liquid curable resin composition for optical fibers comprising a polymer (a) having a number average molecular weight of 5,000 or more and derived from at least two types of recurring ethylenic units, of which one type has a substituent group containing an ethylenically unsaturated group and the second type is substituted by a group --COOR.sup.3 (wherein R.sup.3 is a hydrogen atom or a hydrocarbon group having 1-30 carbon atoms), an aryl group, a cyano group, an alkyl group having 1-10 carbon atoms or by one or more halogen atoms.
摘要翻译：一种光纤用液态固化性树脂组合物，其含有数均分子量为5000以上且由至少两种重复烯属性单元衍生的聚合物（a），其中一种具有含有烯键式不饱和基团的取代基，第二种类型被-COOR 3（其中R3是氢原子或具有1-30个碳原子的烃基），芳基，氰基，具有1-10个碳原子的烷基或一个或多个更多的卤素原子。

20. 发明申请

US20070232713A1 Radiation Curable Liquid Resin Composition for Optical Three-Dimensional Molding and Optical Molded Article Obtained by Photocuring Same 审中-公开
标题翻译：用于光学三维成型的辐射可固化液体树脂组合物和通过光固化获得的光学成型品
公开(公告)号：US20070232713A1
公开(公告)日：2007-10-04
申请号：US11596744
申请日：2005-05-26
申请人： Katsuyuki Takase , Ryouji Tatara , Masanobu Sugimoto , Zen Komiya
发明人： Katsuyuki Takase , Ryouji Tatara , Masanobu Sugimoto , Zen Komiya
IPC分类号： C08G59/18 , B29C67/00 , C08K5/13 , C08K5/524 , C08L63/00
CPC分类号： G03F7/027 , B29C64/00 , G03F7/0037 , G03F7/038
摘要： Provided is a radiation curing liquid resin composition for optical three-dimensional modeling, which has a small step on the side face and excellent surface smoothness, and allows forming a high accuracy optically modeled article, is composed of the components (A) through (F). The content of (A) component in the total quantity of the composition is 0.1 to 10% by mass, and the content of (F) polyether polyol compound is 1 to 35% by mass. (A) A compound having phenolic hydroxyl group and/or phosphite group, (B) A cationic polymerizable compound, (C) A cationic polymerization initiator, (D) A radical polymerizable compound, (E) A radical polymerization initiator, and (F) A polyether polyol compound.
摘要翻译：提供一种用于光学三维建模的辐射固化液体树脂组合物，其在侧面具有小的台阶和优异的表面平滑度，并且允许形成高精度的光学建模的制品由组分（A）至（F ）。组合物中（A）成分的含量为0.1〜10质量％，（F）聚醚多元醇化合物的含量为1〜35质量％。（A）具有酚羟基和/或亚磷酸酯基的化合物，（B）阳离子聚合性化合物，（C）阳离子聚合引发剂，（D）自由基聚合性化合物，（E）自由基聚合引发剂，（F ）聚醚多元醇化合物。

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