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11. 发明授权

US06906110B1 Method for the production of polyurethanes 有权
标题翻译：生产聚氨酯的方法
公开(公告)号：US06906110B1
公开(公告)日：2005-06-14
申请号：US10019998
申请日：2000-11-04
申请人： Reinhard Lorenz , Stephan Bauer , Dieter Junge , Eva Baum , Kathrin Harre , Jörg Erbes , Thomas Ostrowski , Georg Heinrich Grosch
发明人： Reinhard Lorenz , Stephan Bauer , Dieter Junge , Eva Baum , Kathrin Harre , Jörg Erbes , Thomas Ostrowski , Georg Heinrich Grosch
IPC分类号： C08G18/22 , C08G18/48 , C08G65/26 , C08K3/10 , C08K3/16 , C08K3/24 , C08K3/26 , C08K5/09
CPC分类号： C08G18/4866 , C08G18/225 , C08G65/2663 , C08G2101/0008 , C08G2101/0083
摘要： In a process for producing polyurethanes by reacting at least one polyisocyanate with at least one compound containing at least two hydrogen atoms which are reactive toward isocyanate groups, the compound having at least two active hydrogen atoms which is used is at least one polyether alcohol prepared by addition of alkylene oxides onto H-functional initiator substances by means of multimetal cyanide catalysis and the reaction is carried out in the presence of at least one metal salt.
摘要翻译：在通过使至少一种多异氰酸酯与至少一种含有至少两个对异氰酸酯基团具有反应性的氢原子的化合物反应来生产聚氨酯的方法中，使用至少两个活性氢原子的化合物是至少一种由通过多金属氰化物催化将氧化烯加成到H-官能引发剂物质上，并且反应在至少一种金属盐的存在下进行。

12. 发明申请

US20050004343A1 Suspensions of multimetal cyanide compounds, their preparation and their use 审中-公开
标题翻译：多金属氰化物化合物的悬浮液，其制备及其用途
公开(公告)号：US20050004343A1
公开(公告)日：2005-01-06
申请号：US10897872
申请日：2004-07-23
申请人： Georg Grosch , Kathrin Harre , Jorg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge , Edward Dexheimer
发明人： Georg Grosch , Kathrin Harre , Jorg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge , Edward Dexheimer
IPC分类号： B01J27/26 , C08G65/26 , B01J31/00 , C07C41/03 , C08G59/68 , C08G65/04
CPC分类号： B01J27/26 , C08G65/2663
摘要： Catalyst suspensions for the ring-opening polymerization of alkylene oxides comprise a) at least one multimetal cyanide compound having a crystalline structure and a content of platelet-shaped particles of at least 30% by weight, based on the multimetal cyanide compound, and b) at least one organic complexing agent c) water and/or d) at least one polyether and/or e) at least one surface-active substance, with the proviso that at least component a) and at least two of the components b) to e) have to be present.
摘要翻译：用于环氧烷烃开环聚合的催化剂悬浮液包括a）至少一种多金属氰化物化合物，其基于多金属氰化合物具有至少30重量％的晶体结构和片状颗粒的含量，以及b）至少一种有机络合剂c）水和/或d）至少一种聚醚和/或e）至少一种表面活性物质，条件是至少组分a）和至少两种组分b）至 e）必须存在。

13. 发明授权

US06613714B2 Multimetal cyanide compounds, their preparation and their use 失效
标题翻译：多金属氰化合物，其制备及其用途
公开(公告)号：US06613714B2
公开(公告)日：2003-09-02
申请号：US09324145
申请日：1999-06-02
申请人： Georg Heinrich Grosch , Kathrin Harre , Jörg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge
发明人： Georg Heinrich Grosch , Kathrin Harre , Jörg Erbes , Reinhard Lorenz , Stephan Bauer , Thomas Ostrowski , Eva Baum , Dieter Junge
IPC分类号： B01J2726
CPC分类号： C08G65/2663 , B01J27/26 , B01J35/023
摘要： In multimetal cyanide complexes, more than 30% by weight of the primary particles have a platelet-like habit, i.e. the length and width of the primary particles is at least three times the thickness of the particles.
摘要翻译：在多金属氰化物络合物中，超过30重量％的初级颗粒具有血小板样习惯，即一次颗粒的长度和宽度至少为颗粒厚度的三倍。

14. 发明授权

US06548714B1 Method for producing polyetherols by ring-opening polymerisation of alkylene oxides 失效
标题翻译：通过环氧烷开环聚合生产聚醚的方法
公开(公告)号：US06548714B1
公开(公告)日：2003-04-15
申请号：US09744512
申请日：2001-01-24
申请人： Georg Heinrich Grosch , Harald Larbig , Reinhard Lorenz , Dieter Junge , Kathrin Harre
发明人： Georg Heinrich Grosch , Harald Larbig , Reinhard Lorenz , Dieter Junge , Kathrin Harre
IPC分类号： C07C4100
CPC分类号： B01J23/007 , B01J27/232 , B01J27/236 , B01J27/26 , C08G65/2642 , C08G65/2657 , C08G65/2663 , C08G65/269
摘要： A process for preparing polyetherols by ring-opening polymerization of alkylene oxides onto H-functional initiator molecules comprises at least one process step a) in which a compound of the formula (I) M′aM″b(OH)cOd* Ae*Lf (I), is applied to a solid inert support or incorporated in the latter or molded to form a shaped body is used as catalyst, and at least one process step b) in which a multimetal cyanide compound of the formula (II) M1a[M2(CN)b(A)c]d·fM1gXn·h(H20) eL (II) is applied to a solid, inert support or incorporated in the latter or molded to form a shaped body or in powder or paste form is used as catalyst.
摘要翻译：通过环氧烷烃在H-官能引发剂分子上的开环聚合制备聚醚的方法包括至少一种方法步骤a），其中将式（I）化合物施用于固体惰性载体或并入其中用于形成成形体的成型体用作催化剂，以及至少一种方法步骤b），其中将式（II）的多金属氰化物化合物施加到固体惰性载体上或并入其中，或者模制成形成身体或以粉末或糊状形式用作催化剂。

15. 发明授权

US06303833B1 Multi-metal cyanide complexes as catalysts and their use in preparing polyetherpolyols 有权
标题翻译：多金属氰化物络合物作为催化剂及其在制备聚醚多元醇中的应用
公开(公告)号：US06303833B1
公开(公告)日：2001-10-16
申请号：US09509515
申请日：2000-03-29
申请人： Georg Heinrich Grosch , Harald Larbig , Reinhard Lorenz , Dieter Junge , Eugen Gehrer , Ulrich Treuling
发明人： Georg Heinrich Grosch , Harald Larbig , Reinhard Lorenz , Dieter Junge , Eugen Gehrer , Ulrich Treuling
IPC分类号： C07C4311
CPC分类号： B01J27/26 , C08G65/2663
摘要： A crystalline multimetal cyanide complex of the formula (I) M1a[M2(CN)bL1c]d*e(M1fXg)*hL2′iH2O (I) where M1 is at least one element from the group consisting of Zn(II), Fe(II), Co(III), Ni(II), Mn(II), Co(II), Sn(II). Pb(II), Fe(III), Mo(IV), Mo(VI), Al(III), V(IV), V(V), Sr(II, W(IV), W(VI), Cu(II), and Cr(III), M2 is at least one element from the group consisting of Fe(II), Fe(III), Co(III), Cr(III), Mn(II), Mn(III), Ir(III), Rh(III), Ru(II), V(IV), V(V), Co(II) and Cr(II), L1 is at least one ligand from the group consisting of cyanide, carbonyl, cyanate, isocyanate, nitrile, thiocyanate and nitrosyl, X is a formate anion, an acetate anion or propionate anion, L2 is at least one water-miscible ligand from the group consisting of alcohols, aldehydes, ketones, ethers, polyethers, esters, urea derivatives, amides, nitriles and sulfides, a, b, c, d, e, f, g, h, i are integers, with a, b, c and d being chosen so that the electrical neutrality condition is satisfied, and f and g being chosen so that the electrical neutrality condition is satisfied, the X-ray diffiactogram of which shows reflections at particular d values, can be employed as catalyst.
摘要翻译：式（I）的结晶多金属氰化物络合物，其中M 1是由Zn（II），Fe（II），Co（III），Ni（II），Mn（II），Co（II）组成的组中的至少一种元素），Sn（II）。 Pb（II），Fe（III），Mo（IV），Mo（VI），Al（III），V（IV），V（V）（II），Fe（Ⅲ），Co（Ⅲ），Cr（Ⅲ），Mn（Ⅱ），Mn（Ⅲ）等元素中的至少一种元素，，Ir（III），Rh（III），Ru（II），V（IV），V（V），Co（II）和Cr（II），L1是至少一种由氰化物，羰基，氰酸酯，异氰酸酯，腈，硫氰酸酯和亚硝酰基，X是甲酸根阴离子，乙酸根阴离子或丙酸根阴离子，L2是至少一种与醇，醛，酮，醚，聚醚，酯，尿素衍生物，酰胺，腈和硫化物，a，b，c，d，e，f，g，h，i是整数，其中选择a，b，c和d，使得满足电中性条件，被选择为使得电中性条件满足，其X射线衍射图示出特定d值的反射可用作催化剂。

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