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11. 发明专利

JPS6351420A PRODUCTION OF THERMOSETTING HYDROCARBON RESIN 失效
公开(公告)号：JPS6351420A
公开(公告)日：1988-03-04
申请号：JP19602886
申请日：1986-08-21
申请人： OTANI SUGIRO , FUJI SEKYU KK , FUJI STANDARD RES INC
发明人： OTANI SUGIRO , FUJII MASAMI , SASAKI TAKUMI , ARAI TOMIO
IPC分类号： C08G61/02 , C08G61/00
摘要： PURPOSE:To obtain in a short time the titled resin of good fluidity by reaction on heating in the presence of acid catalyst between a condensed polycyclic aromatic compound and crosslinking agent comprising a second aromatic compound having at least two hydroxymethyl groups under increased pressure sufficient for suppressing expansion of the reaction mixture. CONSTITUTION:A mixture F made up of (A) a raw material consisting mainly of condensed polycyclic aromatic compound (e.g., naphthalene), (B) a crosslinking agent consisting mainly of a second aromatic compound having at least two hydroxymethyl or halomethyl groups (e.g., p-xylylene glycol), and (C) an acid catalyst (e.g., p-toluenesulfonic acid) is fed to a reaction vessel 1 followed by reaction on heating with the inner space of the reaction vessel 1 pressurized by a circulating inert gas G of increased pressure through a line 22 to suppress expansion of the reaction mixture F, thus obtaining the objective thermosetting resin.

12. 发明专利

JPS6351417A PRODUCTION OF HYDROCARBON RESIN CURED PRODUCT 失效
公开(公告)号：JPS6351417A
公开(公告)日：1988-03-04
申请号：JP19602586
申请日：1986-08-21
申请人： OTANI SUGIRO , FUJI SEKYU KK , FUJI STANDARD RES INC
发明人： OTANI SUGIRO , FUJII MASAMI , SASAKI TAKUMI , ARAI TOMIO
IPC分类号： C08G61/02 , C08G61/00
摘要： PURPOSE:To obtain the titled cured product for e.g., metal composite materials free from metal corrosion, by heating in the presence of acid catalyst a condensed polycyclic aromatic compound and a second aromatic compound containing two or more hydroxymethyl groups followed by molding together with an organic carboxylic acid and postcuring at elevated temperatures. CONSTITUTION:(A) A raw material consisting mainly of condensed polycyclic aromatic compound (e.g., pyrene) and (B) a crosslinking agent consisting mainly of a second aromatic compound having at least two hydroxymethyl groups (e.g., p-xylylene glycol) are allowed to react in the presence of a small amount of an acid catalyst (e.g., p-toluenesulfonic acid) by heating to form a non-acidic thermosetting resin. Thence, the resultant resin is molded on heating together with an organic carboxylic acid (e.g., trichloroacetic acid) followed by postcuring the resulting cured product at a temperature higher than the above molding temperature to decompose or volatilize the organic carboxylic acid, thus obtaining the objective cured product.

13. 发明专利

JPS6348327A PRODUCTION OF THERMOSETTING HYDROCARBON RESIN 失效
公开(公告)号：JPS6348327A
公开(公告)日：1988-03-01
申请号：JP19110986
申请日：1986-08-14
申请人： OTANI SUGIRO , FUJI SEKYU KK , FUJI STANDARD RES INC
发明人： OTANI SUGIRO , OKADA SHINICHI , KAWASE JUNICHI , ARAI TOMIO
IPC分类号： C10C3/02 , C08G61/00 , C08G61/02 , C10C3/10
摘要： PURPOSE:To produce the titled resin of a high softening point and a high yield of carbonization, by reacting a starting material based on a benzene ring-bearing condensed polycyclic aromatic compound with a specified crosslinking agent in the presence of an acid catalyst in a halohydrocarbon solvent. CONSTITUTION:A starting material (A) (e.g., coal tar) obtained from petroleum or coal and based on a condensed polycyclic aromatic compound having 2-5 benzene nuclei, having an aromatic carbon fraction >=0.6, an aromatic ring hydrogen content >=30% and an MW >=200, is reacted with a crosslinking agent (B) [e.g., di(hydroxymethyl)benzene] based on an aromatic compound having at least two hydroxymethyl or halomethyl group in a molar ratio of 0.2-10 at 70-300 deg.C and a pressure of normal pressure to 20kg/cm G in the presence of 0.2-20wt%, based on (A+B), acid catalyst (C) (e.g., sulfuric acid) in 0.5-10 pts.wt., per pt.wt. components A and B, halohydrocarbon solvent (D) (e.g., trichloroethylene) until the torque of agitation increases to a value which is 1.2-5 times the initial torque.

14. 发明专利

JPS62283806A IMPERMEABLE CARBON MATERIAL AND ITS PRODUCTION 失效
公开(公告)号：JPS62283806A
公开(公告)日：1987-12-09
申请号：JP12450086
申请日：1986-05-29
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C10C3/02 , C01B31/02 , C01B31/04 , C04B35/52 , C08G61/00 , C08G61/02
摘要： PURPOSE:To develop an impermeable carbon material which is small in shrinkage at the time of carbonization by subjecting a thermosetting intermediate product which is obtd. by a thermal reaction of a mixture composed of a condensed polycyclic arom. compd., specific arom. crosslinking agent and acid catalyst to thermal curing and molding, then to a carbonization or graphitization at a high temp. CONSTITUTION:The mixture composed of the condensed polycyclic arom. compd. which is a mixture of >=1 kinds of derivs. consisting of naphthalene, anthracene, etc., as main skeleton, heavy gravity oils of coal and petroleum, tar, pitch, and the oxide, sulfide, halide, etc., of said materials, the arom. crosslinking agent consisting of 1 or >=2 arom. rings contg. 1 or >=2 kinds of a hydroxy methyl group and halomethyl group, and the acid catalyst such as aluminum chloride, boron fluoride or phosphoric acid or the thermosetting intermediate product obtd. by the thermal reaction of such mixture is heated to 100-400 deg.C in an oxidative or nonoxidative atmosphere and is plasticized, by which the mixture is thermally cured and molded to the prescribed shape; thereafter the molding is carbonized or graphitized. The impermeable carbon material which is small in shrinkage at the time of carbonization and has an intricate shape is thus produced.

15. 发明专利

JPS62191469A CARBON, GRAPHITE MATERIAL USING THERMOSETABLE RESIN AND MANUFACTURE 失效
公开(公告)号：JPS62191469A
公开(公告)日：1987-08-21
申请号：JP3476186
申请日：1986-02-19
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C04B35/52 , C01B31/04

16. 发明专利

JPS62135580A CONDUCTIVE BONDED STRUCTURE AND PRODUCTION THEREOF 失效
公开(公告)号：JPS62135580A
公开(公告)日：1987-06-18
申请号：JP27880085
申请日：1985-12-10
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： H01R43/00 , C08F32/00 , C08F32/08 , C08G61/00 , C08G61/02 , C09J9/02 , C09J11/04 , C09J159/00 , C09J201/00 , H01B1/12 , H01R4/04
摘要： PURPOSE:To obtain the titled bonded structure free from conductive aggregates and having excellent heat resistance and strength, by bonding an adherend with an adhesive comprised of a thermosetting compsn. comprising a condensed arom. polycyclic compd., an arom. crosslinking agent, and an acid catalyst. CONSTITUTION:A mixture of a condensed arom. polycyclic compd. (a) and an arom. crosslinking agent (b) in a molar ratio of (b) to (a) of 0.5-4.0 is reacted with an acid catalyst (c) in an amt. of 0.1-10wt% based on the mixture at 60-300 deg.C to obtain an adhesive (B) comprised of a thermosetting compsn. An adherend (A) which is electrically conductive and has H, halogen, OH group, epoxy or acid anhydride structure, etc., on its surface is bonded to the component B via an arom. crosslinking agent (C) which is a mono- or polycyclic arom. compd. having at least two groups of at least one member selected from hydroxymethyl groups and halomethyl group, a surface treating agent which is a mixture of components (b) and (c) or an additive, in the presence of a catalyst for promoting the conductivity impartment, thereby curing the component B at 100-400 deg.C for 10-30hr and imparting conductivity by virtue of the org. conjugation.

17. 发明专利

JPS62521A PRODUCTION OF FUSED POLYCYCLIC POLYNUCLEAR AROMATIC RESIN AND THERMOSETTING COMPOSITION USED THEREFOR 失效
公开(公告)号：JPS62521A
公开(公告)日：1987-01-06
申请号：JP3332686
申请日：1986-02-18
申请人： OTANI SUGIRO , NAGAI YOICHIRO
发明人： OTANI SUGIRO , NAGAI YOICHIRO
IPC分类号： C08G61/00 , C08G61/02
摘要： PURPOSE:To obtain an aromatic resin of excellent heat resistance industrially and inexpensively, by mixing and reacting a fused polycyclic aromatic compound with a crosslinking agent comprising an aromatic compound at a specified ratio and forming a thermosetting substance comprising an intermediate condensation product. CONSTITUTION:A starting material consisting mainly of a fused polycyclic aromatic compound having at least three fused benzene nuclei is mixed with a crosslinking agent consisting mainly of an aromatic compound having at least two hydroxymethyl or halomethyl groups at a ratio represented by the formula. This mixture is heated 70-300 deg.C in the presence of an acid catalyst to form a thermosetting substance comprising an intermediate condensation product. In the formula, W1 is the weight of the starting material, W2 is the weight of the crosslinking agent, (a) is the MW or average-MW of the starting material, (b) is the MW or average MW of the crosslinking agent and (n) is the number of the hydroxymethyl or halomethyl groups which are bonded with 1mol of the aromatic compound as the crosslinking agent.

18. 发明专利

JPH0366720A ORGANIC FERROMAGNETIC PRECURSOR, ORGANIC FERROMAGNETIC MATERIAL AND PREPARATION THEREOF 失效
公开(公告)号：JPH0366720A
公开(公告)日：1991-03-22
申请号：JP20369189
申请日：1989-08-04
申请人： OSAKA GAS CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OTANI SUGIRO
IPC分类号： H01F1/00 , C08G8/04 , C08G8/10 , H01F1/42
摘要： PURPOSE:To prepare an organic ferromagnetic precursor comprising oxo or thioxo group-containing aromatic compounds crosslinked with methine bonds by polycondensing a specific aromatic compound with a specified aromatic aldehyde compound in the presence of an acid catalyst and subsequently oxidizing the polycondensed product to form oxo or thioxo groups thereon. CONSTITUTION:An aromatic compound having one or more of hydroxyl, mercapto, dialkylamino and methoxy groups is polycondensed with an aromatic aldehyde having at least one formly group in the presence of an acid catalyst and the prepared triarylmethane type polymer is oxidized to form oxo or thioxo groups, thereby providing an organic ferromagnetic precursor comprising aromatic compounds having one or more oxo or thioxo groups and crosslinked with methine groups. The radicalization of the methine carbon portion of the precursor preferably by the irradiation of UV rays, etc., gives an organic ferromagnetic material having a radical concentration of >=10 /g, excellent moldability and a light weight.

19. 发明专利

JPH02255136A ARTIFICIAL TOOTH ROOT MATERIAL 失效
公开(公告)号：JPH02255136A
公开(公告)日：1990-10-15
申请号：JP7769689
申请日：1989-03-29
申请人： OTANI SUGIRO , YANAGISAWA SADAKATSU , NIIJIMA KUNIO , JAPAN RES DEV CORP , MITSUBISHI CHEM IND
发明人： OTANI SUGIRO , YANAGISAWA SADAKATSU , NIIJIMA KUNIO , MATSUURA KAZUSHI , FUSE TORU
IPC分类号： A61C8/00
摘要： PURPOSE:To maintain the fixed state stable over a long period of time after embedment and to prevent the generation of the dislodgment, rotation, etc., of a core material by constituting the above material of the core material and a porous layer and forming the core material to a noncircular sectional shape in a part of the sectional shape thereof. CONSTITUTION:The artificial tooth root material is formed with the porous layer on the surface of the core material. The core has a bar shape and is preferably formed by using bioinert carbon fiber reinforced carbon material having high strength, titanium, alumina, etc. The porous layer may be made of such a material which allows the biotissue to advance into the pores of the porous layer to form the secure connective tissue when embedded into a living body and allows the connective tissue to cause calcification and change to the osteostructure; for example, the porous layer consisting of alumina and the carbonaceous porous layer or the like formed by depositing pyrolysis carbon on a non-woven fabric of carbon fibers, etc., are exemplified. The sectional shape in at least a part of the core material has the noncircular sectional shape and is not made into a threaded structure. Since the porous layer is formed on such core material, the peeling, rotation, etc., at the boundary between the core material and the porous layer is prevented.

20. 发明专利

JPH02153851A CEMENT COMPOSITE MATERIAL HAVING ELECTROMAGNETIC WAVE SHIELDING PROPERTY 失效
公开(公告)号：JPH02153851A
公开(公告)日：1990-06-13
申请号：JP30712588
申请日：1988-12-05
申请人： INAX CORP , KOJIMA AKIRA , OTANI SUGIRO
发明人： KOJIMA AKIRA , OTANI SUGIRO , MIWA MASAKI
IPC分类号： E04B1/92 , C04B14/36 , C04B14/38 , C04B28/02 , H05K9/00
摘要： PURPOSE:To provide a composite material having high electromagnetic shielding properties and strength by mixing carbon fiber paper in a specific amount or more with cement. CONSTITUTION:The above-mentioned cement material is obtained by mixing >=0.7vol.% carbon fiber paper with cement. The aforementioned carbon fiber paper refers to carbon fiber having a two-dimensional extent and includes nonwoven fabric-like paper, paper produced by a sheet forming method, woven fabric-like paper, etc. The above-mentioned cement composite material has the following advantages. Lightweight and high electromagnetic wave shielding properties and strength relative to a low carbon fiber content, good dispersion of the carbon fiber and moldability, excellent in corrosion resistance and high deformability.

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