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1. 发明专利

JPH0366720A ORGANIC FERROMAGNETIC PRECURSOR, ORGANIC FERROMAGNETIC MATERIAL AND PREPARATION THEREOF 失效
公开(公告)号：JPH0366720A
公开(公告)日：1991-03-22
申请号：JP20369189
申请日：1989-08-04
申请人： OSAKA GAS CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OTANI SUGIRO
IPC分类号： H01F1/00 , C08G8/04 , C08G8/10 , H01F1/42
摘要： PURPOSE:To prepare an organic ferromagnetic precursor comprising oxo or thioxo group-containing aromatic compounds crosslinked with methine bonds by polycondensing a specific aromatic compound with a specified aromatic aldehyde compound in the presence of an acid catalyst and subsequently oxidizing the polycondensed product to form oxo or thioxo groups thereon. CONSTITUTION:An aromatic compound having one or more of hydroxyl, mercapto, dialkylamino and methoxy groups is polycondensed with an aromatic aldehyde having at least one formly group in the presence of an acid catalyst and the prepared triarylmethane type polymer is oxidized to form oxo or thioxo groups, thereby providing an organic ferromagnetic precursor comprising aromatic compounds having one or more oxo or thioxo groups and crosslinked with methine groups. The radicalization of the methine carbon portion of the precursor preferably by the irradiation of UV rays, etc., gives an organic ferromagnetic material having a radical concentration of >=10 /g, excellent moldability and a light weight.

2. 发明专利

JPH0642371B2 失效
公开(公告)号：JPH0642371B2
公开(公告)日：1994-06-01
申请号：JP11858686
申请日：1986-05-22
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OTANI SUGIRO
IPC分类号： C08L95/00 , H01M4/86 , H01M4/96 , H01M8/02

3. 发明专利

JPS6310664A PRODUCTION OF CARBON PRECURSOR COMPOSED OF THERMOSETTING RESIN PREPARED FROM HYDROGENATED PITCH 失效
公开(公告)号：JPS6310664A
公开(公告)日：1988-01-18
申请号：JP15290086
申请日：1986-06-30
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OTANI SUGIRO
IPC分类号： C10C3/02 , C08L95/00 , C10C3/04 , C10C3/10 , D01F9/14 , D01F9/145
摘要： PURPOSE:To obtain the title precursor which has a high carbonization yield and a low shrinkage factor during carbonization and allows graphatization to be freely controlled, by hydrogenating pitch to lower its softening point, adding a specified crosslinking agent thereto and heating the mixture in the presence of an acid catalyst. CONSTITUTION:At least one pitch having a solftening point of not lower than 120 deg.C selected from the group consisting of petroleum and coal pitches is hydrogenated to lower the softening point. A crosslinking agent mainly composed of an arom. compd. having at least two hydroxymethyl and/or halomethyl groups is added thereto. The mixture is heated in the presence of an acid catalyst at 60-300 deg.C to obtain the desired carbon precursor. The pitch used has a carbonization yield of not lower than 50wt%. It is desirable that the pitch having a low softening point and a high carbonization yield is used as a starting material. It is preferred that the hydrogenation is carried out by a direct hydrogenation method wherein the hydrogenation is carried out in the presence of a catalyst in a hydrogen stream at a high temp. under a high pressure.

4. 发明专利

JPS62274559A MANUFACTURE OF COMPOSITE ELECTRODE FOR FUEL CELL 失效
公开(公告)号：JPS62274559A
公开(公告)日：1987-11-28
申请号：JP11858686
申请日：1986-05-22
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OTANI SUGIRO
IPC分类号： C08L95/00 , H01M4/86 , H01M4/96 , H01M8/02
摘要： PURPOSE:To make a size large by bonding porous electrodes on both side surfaces of a separator comprising a cured body of conductive thermosetting resin by using thermosetting resin as a binder, and unifying them by thermosetting. CONSTITUTION:A cured body of thermosetting resin having high chemical resistance, impermeability, and conductivity after setting is used as a separator. The separator is bonded to porous carbon or graphite electrode by using which is a binder the same thermosetting resin as the cured body and they are cured. Thereby, a composite electrode for fuel cell having many excellent performances in heat resistance, dimensional stability, strength, elastic modulus, toughness, water resistance, chemical resistance, and conductivity in the cured state without carbinization can be obtained, In addition, its size and shape can freely be controlled.

5. 发明专利

JPH0575023B2 失效
公开(公告)号：JPH0575023B2
公开(公告)日：1993-10-19
申请号：JP15290086
申请日：1986-06-30
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： KAKEGAWA HIROYA , OOTANI SUGIRO
IPC分类号： C10C3/02 , C08L95/00 , C10C3/04 , C10C3/10 , D01F9/14 , D01F9/145

6. 发明专利

JPS62275009A IMPERMEABLE CARBON MATERIAL AND ITS PRODUCTION 失效
公开(公告)号：JPS62275009A
公开(公告)日：1987-11-30
申请号：JP11303486
申请日：1986-05-17
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C01B31/02 , C01B31/04 , C04B14/36 , C04B26/04 , C04B35/52 , C08K3/04 , C08L65/00 , C09K3/10
摘要： PURPOSE:To produce an impermeable carbon material having dimensional stability, strength, toughness and wear resistance by treating a skeleton material having functional groups on the surface with an aromatic cross-linking agent, combining the treated skeleton material with a specified thermosetting composition and carbonizing or graphitizing the resulting composite body. CONSTITUTION:The surface of a skeleton material having hydrogen, halogen, hydroxyl or other functional groups on the surface is treated with an aromatic cross-linking agent having one or more aromatic rings each having hydroxymethyl or halomethyl groups. A mixture of a condensed polycyclic aromatic compound having oxygen, sulfur, halogen or the like in the molecule having two or more rings with said aromatic cross-linking agent and an acid catalyst is prepd. or the mixture is brought into a reaction by heating to prepare a thermosetting intermediate reaction product. The treated skeleton material is combined with the thermosetting composition and the resulting composite body is plasticized by heating to 100-400 deg.C in an oxidizing or nonoxidizing atmosphere and molded into a prescribed shape by heat curing. The molded body is carbonized or further graphitized to obtain an impermeable carbon material.

7. 发明专利

JPS62138577A BONDED CONSTRUCTION AND ITS MANUFACTURE 失效
公开(公告)号：JPS62138577A
公开(公告)日：1987-06-22
申请号：JP27968385
申请日：1985-12-11
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C08J5/12 , B29C65/52 , C08G61/00 , C08G61/02 , C09J4/00 , C09J4/06 , C09J5/02 , C09J159/00
摘要： PURPOSE:To obtain the titled construction of both high bond strength and heat and water resistances by coating an adherend having functional group on its surface with a halomethyl group-contg. aromatic crosslinking agent followed by heat treatment and then bonding using an adhesive comprising condensed polycyclic aromatic compound and aromatic crosslinking agent followed by heat curing. CONSTITUTION:The surface of an adherend having thereon such functional group(s) as hydrogen, halogen, hydroxyl group, carbonyl group, carboxyl group, aldehyde group, epoxy structure, lactone structure, ether structure or acid anhydride structure is coated with a surface-treatment agent consisting mainly of aromatic crosslinking agent made up of mono- or polycyclic aromatic ring carrying at lest two hydroxymethyl-halomethyl groups, etc., followed by heat treatment. An adhesive consisting of a thermosetting composition comprising condensed polycyclic aromatic compound, aromatic crosslinking agent and acid catalyst is either plasticized or liquefied followed by bonding to the adhered coated with said surface-treating agent and then heating at 100-400 deg.C in a (non)oxidative atmosphere to effect curing of the adhesive, thus obtaining the objective construction.

8. 发明专利

JPS62283806A IMPERMEABLE CARBON MATERIAL AND ITS PRODUCTION 失效
公开(公告)号：JPS62283806A
公开(公告)日：1987-12-09
申请号：JP12450086
申请日：1986-05-29
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C10C3/02 , C01B31/02 , C01B31/04 , C04B35/52 , C08G61/00 , C08G61/02
摘要： PURPOSE:To develop an impermeable carbon material which is small in shrinkage at the time of carbonization by subjecting a thermosetting intermediate product which is obtd. by a thermal reaction of a mixture composed of a condensed polycyclic arom. compd., specific arom. crosslinking agent and acid catalyst to thermal curing and molding, then to a carbonization or graphitization at a high temp. CONSTITUTION:The mixture composed of the condensed polycyclic arom. compd. which is a mixture of >=1 kinds of derivs. consisting of naphthalene, anthracene, etc., as main skeleton, heavy gravity oils of coal and petroleum, tar, pitch, and the oxide, sulfide, halide, etc., of said materials, the arom. crosslinking agent consisting of 1 or >=2 arom. rings contg. 1 or >=2 kinds of a hydroxy methyl group and halomethyl group, and the acid catalyst such as aluminum chloride, boron fluoride or phosphoric acid or the thermosetting intermediate product obtd. by the thermal reaction of such mixture is heated to 100-400 deg.C in an oxidative or nonoxidative atmosphere and is plasticized, by which the mixture is thermally cured and molded to the prescribed shape; thereafter the molding is carbonized or graphitized. The impermeable carbon material which is small in shrinkage at the time of carbonization and has an intricate shape is thus produced.

9. 发明专利

JPS62191469A CARBON, GRAPHITE MATERIAL USING THERMOSETABLE RESIN AND MANUFACTURE 失效
公开(公告)号：JPS62191469A
公开(公告)日：1987-08-21
申请号：JP3476186
申请日：1986-02-19
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C04B35/52 , C01B31/04

10. 发明专利

JPS62135580A CONDUCTIVE BONDED STRUCTURE AND PRODUCTION THEREOF 失效
公开(公告)号：JPS62135580A
公开(公告)日：1987-06-18
申请号：JP27880085
申请日：1985-12-10
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： H01R43/00 , C08F32/00 , C08F32/08 , C08G61/00 , C08G61/02 , C09J9/02 , C09J11/04 , C09J159/00 , C09J201/00 , H01B1/12 , H01R4/04
摘要： PURPOSE:To obtain the titled bonded structure free from conductive aggregates and having excellent heat resistance and strength, by bonding an adherend with an adhesive comprised of a thermosetting compsn. comprising a condensed arom. polycyclic compd., an arom. crosslinking agent, and an acid catalyst. CONSTITUTION:A mixture of a condensed arom. polycyclic compd. (a) and an arom. crosslinking agent (b) in a molar ratio of (b) to (a) of 0.5-4.0 is reacted with an acid catalyst (c) in an amt. of 0.1-10wt% based on the mixture at 60-300 deg.C to obtain an adhesive (B) comprised of a thermosetting compsn. An adherend (A) which is electrically conductive and has H, halogen, OH group, epoxy or acid anhydride structure, etc., on its surface is bonded to the component B via an arom. crosslinking agent (C) which is a mono- or polycyclic arom. compd. having at least two groups of at least one member selected from hydroxymethyl groups and halomethyl group, a surface treating agent which is a mixture of components (b) and (c) or an additive, in the presence of a catalyst for promoting the conductivity impartment, thereby curing the component B at 100-400 deg.C for 10-30hr and imparting conductivity by virtue of the org. conjugation.

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