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1. 发明授权

US06774088B2 Rare earth-Ba-Cu complex composition and method of producing superconductor using same 失效
标题翻译：稀土 - Ba-Cu络合物的组成及使用其制造超导体的方法
公开(公告)号：US06774088B2
公开(公告)日：2004-08-10
申请号：US10086377
申请日：2002-03-04
申请人： Takaaki Manabe , Iwao Yamaguchi , Tetsuo Tsuchiya , Toshiya Kumagai , Susumu Mizuta , Susumu Nakamura
发明人： Takaaki Manabe , Iwao Yamaguchi , Tetsuo Tsuchiya , Toshiya Kumagai , Susumu Mizuta , Susumu Nakamura
IPC分类号： H01B100
CPC分类号： H01L39/2425 , C23C18/1216 , C23C18/1295 , Y10S505/70 , Y10S505/734 , Y10S505/741
摘要： A metal complex composition containing complexes having metal species of a rare earth element, barium and copper and ligands of a trifluoroacetic acid or pentafluoropropionic acid ligand, a pyridine ligand and an acetylacetone ligand. A superconductive film may be obtained by applying an organic solvent solution of the above metal complex composition to a substrate and by heat treating the coating.
摘要翻译：含有具有稀土元素金属物质，钡和铜以及三氟乙酸或五氟丙酸配体配体，吡啶配体和乙酰丙酮配体的配合物的金属络合物组合物。可以通过将上述金属络合物组合物的有机溶剂溶液涂布到基材上并通过热处理涂层来获得超导膜。

2. 发明授权

US06576302B1 Method for producing a metal oxide and method for forming a minute pattern 失效
标题翻译：金属氧化物的制造方法及形成微小图案的方法
公开(公告)号：US06576302B1
公开(公告)日：2003-06-10
申请号：US09513814
申请日：2000-02-25
申请人： Susumu Mizuta , Tetsuo Tsuchiya , Akio Watanabe , Yoji Imai , Iwao Yamaguchi , Toshiya Kumagai , Takaaki Manabe , Hiroyuki Niino , Akira Yabe
发明人： Susumu Mizuta , Tetsuo Tsuchiya , Akio Watanabe , Yoji Imai , Iwao Yamaguchi , Toshiya Kumagai , Takaaki Manabe , Hiroyuki Niino , Akira Yabe
IPC分类号： C08J718
CPC分类号： C23C18/14 , C23C18/06 , C23C18/1216
摘要： There is disclosed a method for producing a metal oxide, which comprises the steps of: dissolving a metal organic compound (e.g. a metal organic acid salt, a metal acetylacetonato complex, and a metal alkoxide having an organic group with 6 or more carbon atoms) in a solvent to provide a state of solution, applying the solution onto a substrate, drying the solution, and subjecting the resultant substrate to irradiation with a laser light of a 400 nm or less wavelength, to form a metal oxide on the substrate. According to that method, a metal oxide can be produced without applying a heat treatment at a high temperature of the degree adopted in the conventionally known application thermal decomposition method.
摘要翻译：公开了一种金属氧化物的制造方法，该方法包括以下步骤：将金属有机化合物（例如金属有机酸盐，金属乙酰丙酮络合物和具有6个或更多个碳原子的有机基团的金属醇盐）在溶剂中以提供溶液状态，将溶液施加到基材上，干燥溶液，并使所得基板对波长为400nm以下的激光进行照射，以在基板上形成金属氧化物。根据该方法，可以在常规已知的应用热分解方法中采用的高温下进行金属氧化物而不进行热处理。

3. 发明授权

US06183554B2 Method for preparing dense, epitaxial metal oxide film 失效
标题翻译：制备密集的外延金属氧化物膜的方法
公开(公告)号：US06183554B2
公开(公告)日：2001-02-06
申请号：US09272564
申请日：1999-03-19
申请人： Susumu Mizuta , Iwao Yamaguchi , Toshiya Kumagai , Takaaki Manabe , Wakichi Kondo , Tadao Shimizu , Tsuyoshi Terayama
发明人： Susumu Mizuta , Iwao Yamaguchi , Toshiya Kumagai , Takaaki Manabe , Wakichi Kondo , Tadao Shimizu , Tsuyoshi Terayama
IPC分类号： C30B702
CPC分类号： C23C18/1216 , C23C18/04
摘要： A process for forming a dense, epitaxial metal oxide film on a single crystal substrate, including cleaning the surface of the single crystal substrate, contacting the cleaned surface with a polar organic compound such as a small molecular weight alcohol, so that the cleaned surface adsorbs the polar organic compound, then applying a hydrocarbon solvent solution containing at least one organic group-containing metal compound on the polar organic compound-adsorbed surface, and then heating the substrate to decompose the organic group-containing metal compound and to form a dense epitaxial metal oxide film on the substrate.
摘要翻译：一种用于在单晶衬底上形成致密的外延金属氧化物膜的方法，包括清洗单晶衬底的表面，使清洁的表面与极小的有机化合物如小分子量醇接触，使得清洁的表面吸附极性有机化合物，然后在极性有机化合物吸附表面上施加含有至少一种含有机基团的金属化合物的烃溶剂溶液，然后加热底物以分解含有机基团的金属化合物并形成致密的外延金属氧化物膜在基板上。

4. 发明申请

US20120270738A1 SOLUTION FOR FORMING RARE-EARTH SUPERCONDUCTIVE FILM AND PRODUCTION METHOD THEREOF 有权
标题翻译：形成稀土超导薄膜的方法及其制备方法
公开(公告)号：US20120270738A1
公开(公告)日：2012-10-25
申请号：US13514139
申请日：2010-12-09
申请人： Takaaki Manabe , Iwao Yamaguchi , Toshiya Kumagai , Mitsugu Sohma , Wakichi Kondou , Kenichi Tsukada
发明人： Takaaki Manabe , Iwao Yamaguchi , Toshiya Kumagai , Mitsugu Sohma , Wakichi Kondou , Kenichi Tsukada
IPC分类号： H01L39/12
CPC分类号： C01G3/006 , H01L39/2425
摘要： Provided is a coating solution where, upon producing a rare-earth superconductive composite metal oxide film by means of a coating-pyrolysis method, cracks are not generated in the heat treatment process for eliminating organic components, even when the thickness of the rare-earth superconductive film produced in a single coating is 500 nm or more, and without having to repeat the coating and annealing process. A solution for producing a rare-earth superconductive film which is made into a homogeneous solution by dissolving, in a solvent formed by adding a polyhydric alcohol to a univalent linear alcohol having a carbon number of 1 to 8 and/or water, a metal complex coordinated, relative to metal ions of a metallic species containing rare-earth elements, barium and copper, with pyridine and/or at least one type of tertiary amine, at least one type of carboxylic acid having a carbon number of 1 to 8, and, as needed, an acetylacetonato group.
摘要翻译：提供一种涂布溶液，其中通过涂布 - 热解法在制备稀土超导复合金属氧化物膜时，即使在稀土元素的厚度方面，在用于消除有机组分的热处理过程中也不会产生裂纹在单个涂层中制造的超导膜为500nm以上，不必重复涂布和退火处理。一种制备稀土超导膜的方法，该稀土超导膜通过将溶解在通过将多元醇加入到碳原子数1至8的一价直链醇和/或水形成的溶剂中，形成均匀溶液，金属络合物相对于含有稀土元素的金属物质，钡和铜与吡啶和/或至少一种叔胺，至少一种碳原子数为1至8的羧酸的金属离子相互配位，以及根据需要，可以使用乙酰丙酮化合物。

5. 发明授权

US08865628B2 Solution for forming rare-earth superconductive film and production method thereof 有权
标题翻译：稀土超导薄膜的制造方法及其制造方法
公开(公告)号：US08865628B2
公开(公告)日：2014-10-21
申请号：US13514139
申请日：2010-12-09
申请人： Takaaki Manabe , Iwao Yamaguchi , Toshiya Kumagai , Mitsugu Sohma , Wakichi Kondou , Kenichi Tsukada
发明人： Takaaki Manabe , Iwao Yamaguchi , Toshiya Kumagai , Mitsugu Sohma , Wakichi Kondou , Kenichi Tsukada
IPC分类号： H01L39/12 , H01L39/24 , C01G3/00
CPC分类号： C01G3/006 , H01L39/2425
摘要： Provided is a coating solution where, upon producing a rare-earth superconductive composite metal oxide film by means of a coating-pyrolysis method, cracks are not generated in the heat treatment process for eliminating organic components, even when the thickness of the rare-earth superconductive film produced in a single coating is 500 nm or more, and without having to repeat the coating and annealing process. A solution for producing a rare-earth superconductive film which is made into a homogeneous solution by dissolving, in a solvent formed by adding a polyhydric alcohol to a univalent linear alcohol having a carbon number of 1 to 8 and/or water, a metal complex coordinated, relative to metal ions of a metallic species containing rare-earth elements, barium and copper, with pyridine and/or at least one type of tertiary amine, at least one type of carboxylic acid having a carbon number of 1 to 8, and, as needed, an acetylacetonato group.
摘要翻译：提供一种涂布溶液，其中通过涂布 - 热解法在制备稀土超导复合金属氧化物膜时，即使在稀土元素的厚度方面，在用于消除有机组分的热处理过程中也不会产生裂纹在单个涂层中制造的超导膜为500nm以上，不必重复涂布和退火处理。一种制备稀土超导膜的方法，该稀土超导膜通过将溶解在通过将多元醇加入到碳原子数1至8的一价直链醇和/或水形成的溶剂中，形成均匀溶液，金属络合物相对于含有稀土元素的金属物质，钡和铜与吡啶和/或至少一种叔胺，至少一种碳原子数为1至8的羧酸的金属离子相互配位，以及根据需要，可以使用乙酰丙酮化合物。

6. 发明申请

US20150105261A1 OXIDE SUPERCONDUCTING THIN FILM AND METHOD OF MANUFACTURING THE SAME 审中-公开
标题翻译：氧化物超导薄膜及其制造方法
公开(公告)号：US20150105261A1
公开(公告)日：2015-04-16
申请号：US14403706
申请日：2012-05-31
申请人： Tatsuoki Nagaishi , Genki Honda , Iwao Yamaguchi , Takaaki Manabe , Takeshi Hikata , Hiroaki Matsui , Wakichi Kondo , Hirofumi Yamasaki , Toshiya Kumagai
发明人： Tatsuoki Nagaishi , Genki Honda , Iwao Yamaguchi , Takaaki Manabe , Takeshi Hikata , Hiroaki Matsui , Wakichi Kondo , Hirofumi Yamasaki , Toshiya Kumagai
IPC分类号： H01B12/06 , H01B13/30
CPC分类号： H01B12/06 , H01B13/30 , H01L39/2425 , H01L39/2483
摘要： An oxide superconducting thin film wherein nanoparticles functioning as flux pins are dispersed in the film is provided. The oxide superconducting thin film wherein the nanoparticles in the oxide superconducting thin film have a dispersing density of 1020 particles/m3 to 1024 particles/m3 is provided. The oxide superconducting thin film wherein the nanoparticles have a particle diameter of 5 nm to 100 nm is provided. A method of manufacturing an oxide superconducting thin film wherein a predetermined amount of a solution obtained by dissolving nanoparticles functioning as flux pins in a solvent is added to a solution obtained by dissolving an organometallic compound in a solvent to prepare a source material solution for an oxide superconducting thin film, and the source material solution is used to manufacture the oxide superconducting thin film through a coating-pyrolysis process is provided.
摘要翻译：提供了其中作为磁通引脚的纳米颗粒分散在膜中的氧化物超导薄膜。提供氧化物超导薄膜中的氧化物超导薄膜的分散密度为1020粒子/ m 3至1024个/ m3的氧化物超导薄膜。提供其中纳米颗粒具有5nm至100nm的粒径的氧化物超导薄膜。一种制造氧化物超导薄膜的方法，其中将通过将用作助熔剂针的纳米颗粒溶解在溶剂中而获得的预定量的溶液加入到通过将有机金属化合物溶解在溶剂中而获得的溶液中，以制备用于氧化物的源材料溶液超导薄膜和源材料溶液用于通过涂层热解制备氧化物超导薄膜。

7. 发明申请

US20150162518A1 SOURCE MATERIAL SOLUTION FOR FORMING OXIDE SUPERCONDUCTOR 审中-公开
标题翻译：用于形成氧化物超导体的材料解决方案
公开(公告)号：US20150162518A1
公开(公告)日：2015-06-11
申请号：US14405287
申请日：2012-06-08
申请人： Genki Honda , Tatsuoki Nagaishi , Kei Hanafusa , Iwao Yamaguchi , Hiroaki Matsui , Wakichi Kondo , Toshiya Kumagai
发明人： Genki Honda , Tatsuoki Nagaishi , Kei Hanafusa , Iwao Yamaguchi , Hiroaki Matsui , Wakichi Kondo , Toshiya Kumagai
IPC分类号： H01L39/12
CPC分类号： H01L39/126 , H01L39/2425 , H01L39/2483
摘要： A source material solution for forming an oxide superconductor is provided, the source material solution being used for forming on a substrate an RE 123 oxide superconductor into which flux pinning points are introduced, using a coating-pyrolysis process. Nanoparticles of a predetermined amount for forming pinning points are dispersed in the solution in which an organometallic compound is dissolved for forming the oxide superconductor. The nanoparticles have a particle size of 5 to 100 nm. The organometallic compound is an organometallic compound containing no fluorine. Accordingly, even in an FF-MOD process, the material for pins can easily be added, a treatment for thermally decomposing a metal complex and a heat treatment for generating a pin compound are unnecessary, and the particle size of the pins can suitably be controlled.
摘要翻译：提供了一种用于形成氧化物超导体的源材料溶液，所述源材料溶液用于在衬底上形成引入了焊剂夹点的RE 123氧化物超导体，使用涂层热解法。用于形成钉扎点的预定量的纳米颗粒分散在其中溶解有机金属化合物的溶液中以形成氧化物超导体。纳米粒子的粒径为5〜100nm。有机金属化合物是不含氟的有机金属化合物。因此，即使在FF-MOD工序中，也可以容易地添加销的材料，不需要用于热分解金属络合物的处理和用于产生针化合物的热处理，并且可以适当地控制销的粒度。

8. 发明授权

US06750249B1 Controlled release oral preparations of esculetin and its derivatives 失效
标题翻译：七叶亭及其衍生物的控释口服制剂
公开(公告)号：US06750249B1
公开(公告)日：2004-06-15
申请号：US09806636
申请日：2001-05-23
申请人： Iwao Yamaguchi , Saichi Ono , Tadahiko Chiba
发明人： Iwao Yamaguchi , Saichi Ono , Tadahiko Chiba
IPC分类号： A61K3135
CPC分类号： A61K9/5042 , A61K9/2054 , A61K9/2866 , A61K9/4866 , A61K31/37
摘要： The present invention relates to an oral preparation of esculetin with controlled release. The oral preparation of esculetin with controlled release of the present invention comprises a gel-forming polymer base, preferably hydroxypropylmethylcellulose. The preparation may be coated with an enteric polymer base such as hydroxypropylmethylcellulose acetate succinate to thereby enhance solubility in the intestines. When orally administered, the preparation can continuously release esculetin. Thus, the administration frequency and dose can be reduced and a therapeutic effect on arthropathy can be established.
摘要翻译：本发明涉及具有控制释放的七叶亭的口服制剂。具有本发明的控制释放的七叶亭的口服制剂包含凝胶形成聚合物基质，优选羟丙基甲基纤维素。该制剂可以用肠溶性聚合物基质如乙酸琥珀酸羟丙基甲基纤维素包衣，从而增强肠内的溶解度。口服给药时，可以连续释放七叶亭。因此，可以降低给药频率和剂量，并且可以建立对关节病的治疗效果。

9. 发明申请

US20090110715A1 Edible film Package Having Product for Oral Intake Enclosed Therein 审中-公开
标题翻译：食用胶囊包装口腔内容产品
公开(公告)号：US20090110715A1
公开(公告)日：2009-04-30
申请号：US12227174
申请日：2007-05-08
申请人： Kazumi Ishii , Saichi Ono , Iwao Yamaguchi
发明人： Kazumi Ishii , Saichi Ono , Iwao Yamaguchi
IPC分类号： A61K9/00 , A23L1/48
CPC分类号： A61K9/286 , A23L29/284 , A23P20/10 , A61K9/0056 , A61K9/006 , A61K9/009 , A61K9/0095 , A61K9/70 , A61K9/7007
摘要： This invention aims to provide a novel taking or having-or-swallowing form for an oral material, such as drugs or foodstuffs.This invention provides an edible film packaging 1 containing an edible film material 10 which has adhesion properties and is softened upon contact with moisture. The edible film packaging 1 is taken or had-or-swallowed while an oral material being encapsulated. Moreover, this invention provides an oral-material taking method, including taking or having-or-swallowing the edible film packaging 1 in which the oral material 2 has been encapsulated as it is without opening or as it is without opening after being immersed in water for a given period of time.
摘要翻译：本发明的目的在于提供一种新颖的口服或吞咽形式的口服材料，例如药物或食品。本发明提供一种含有可食用膜材料10的可食性膜包装1，其具有粘合性并且在与水分接触时软化。食用薄膜包装1被采食或吞咽，而口服材料被包封。此外，本发明提供一种口服材料取出方法，其包括取食或者吞食可口膜材料2，其中口腔材料2已被包封而不开封或浸没在水中后不开口在一段给定的时间内

10. 发明申请

US20060223026A1 Liquid injection needle element capable of jetting a liquid in a predetermined angle range and method of producing the same 审中-公开
标题翻译：能够以预定角度范围喷射液体的液体注射针元件及其制造方法
公开(公告)号：US20060223026A1
公开(公告)日：2006-10-05
申请号：US11391239
申请日：2006-03-29
申请人： Akihiro Kuroiwa , Akio Yamamoto , Junichi Otogoto , Takaaki Murakoso , Hiroshi Hasegawa , Iwao Yamaguchi
发明人： Akihiro Kuroiwa , Akio Yamamoto , Junichi Otogoto , Takaaki Murakoso , Hiroshi Hasegawa , Iwao Yamaguchi
IPC分类号： A61C17/02 , A61C5/02
CPC分类号： B21C37/157 , A61C5/40 , A61C5/62 , A61M5/3291 , B05C17/00516
摘要： A cannula has a front part in a direction of a center axis X with its forward end portion closed. The front part has a plurality of nozzle orifices each of which has an orifice axis Y intersecting the center axis X. Each of the nozzle orifices has a first diameter in a first direction parallel to the center axis X and a second diameter in a second direction perpendicular to the first direction. The first diameter ranges between 0.1 mm and 0.5 mm while the second diameter ranges between 0.1 mm and 0.3 mm so that a liquid in the cannula is jetted from the nozzle orifices in an angle range of 45 degrees towards the forward end portion with respect to the orifice axis.
摘要翻译：插管具有在其前端部分封闭的中心轴线X的方向上的前部。前部具有多个喷嘴孔，每个喷嘴孔具有与中心轴线X相交的孔口轴线Y.每个喷嘴孔口在平行于中心轴线X的第一方向上具有第一直径，在第二方向上具有第二直径垂直于第一方向。第一直径在0.1mm和0.5mm之间，而第二直径在0.1mm和0.3mm之间，使得套管中的液体相对于第一直径从前端部分以45度的角度范围从喷嘴孔喷射孔轴。

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