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1. 发明申请

US20050230019A1 Reduced sensitivity melt-cast explosives 审中-公开
标题翻译：灵敏度降低的熔铸炸药
公开(公告)号：US20050230019A1
公开(公告)日：2005-10-20
申请号：US10995883
申请日：2004-11-23
申请人： Daniel Doll , Jami Hanks , Thomas Highsmith , Gary Lund , John Niles
发明人： Daniel Doll , Jami Hanks , Thomas Highsmith , Gary Lund , John Niles
IPC分类号： F42B5/16 , C06B21/00 , C06B25/06 , C06B25/34 , C06B29/16
CPC分类号： C06B21/005 , C06B25/06
摘要： A melt-cast explosive which shares comparable explosive properties to those of COMP B explosives and is melt-pourable and castable under conditions comparable to those of COMP B explosives, but experiences less impact, shock, and thermal sensitivity and avoids the issues of toxicity associated with COMP B. A fundamental and well-accepted component of COMP B, i.e., trinitrotoluene (TNT), is replaced with one or more mononitro-substituted or dinitro-substituted melt-cast binders, such as dinitroanisole, which can be melt-cast without presenting the toxicity drawbacks experienced with the use of TNT. The melt-cast binder can also be combined with a processing aid selected from the group consisting of alkylnitroanilines and arylnitroanilines. Preferably, the composition also includes coarse oxidizer particles and an energetic filler in fine particulate form.
摘要翻译：与COMP B爆炸物具有相当的爆炸特性的熔铸炸药，在与COMP B爆炸物相当的条件下可熔融浇注和浇注，但具有较小的冲击，冲击和热敏感性，并避免了毒性相关的问题使用COMP B。COMP B的一个基本和被广泛接受的组分即三硝基甲苯（TNT）被一个或多个单硝基取代或二硝基取代的熔融流延粘合剂替代，例如二硝基苯甲醚，其可以熔融浇铸而没有呈现使用TNT所经历的毒性缺点。熔融粘合剂也可以与选自烷基硝基苯胺和芳基硝基苯胺的加工助剂组合。优选地，组合物还包括粗氧化剂颗粒和精细颗粒形式的能量填料。

2. 发明申请

US20070066839A1 Method for the production of alpha-alane 有权
标题翻译：生产α-烯烃的方法
公开(公告)号：US20070066839A1
公开(公告)日：2007-03-22
申请号：US11329201
申请日：2006-01-09
申请人： Gary Lund , Jami Hanks , Harold Johnston
发明人： Gary Lund , Jami Hanks , Harold Johnston
IPC分类号： C07F5/06
CPC分类号： C01B6/06
摘要： A method of forming α-alane. The method includes reacting aluminum trichloride and an alkali metal hydride to form an alane-ether complex solution. An aqueous diethyl ether solution is optionally added to the alane-ether complex solution to form a partially hydrolyzed ether/alane-ether complex solution. A solution of a first crystallization additive is added to the alane-ether complex solution or to the aqueous ether/alane-ether complex solution to form a crystallization solution. The first crystallization additive is selected from the group consisting of polystyrene, polybutadiene, polystyrene-co-polybutadiene, polyisoprene, poly-alpha-methylstyrene, polystyrene-co-polyindene, poly-alpha-pinene, and mixtures thereof. Optionally, a second crystallization additive is added to the crystallization solution. The second crystallization additive is selected from the group consisting of squalene, cyclododecatriene, norbornylene, norbornadiene, a phenyl terminated polybutadiene, 2,4-dimethyl anisole, 3,5-dimethyl anisole, 2,6-dimethyl anisole, polydimethyl siloxane, and mixtures thereof Solvents are removed from the crystallization solution to crystallize the α-alane.
摘要翻译：形成α-烯烃的方法。该方法包括使三氯化铝与碱金属氢化物反应以形成丙烯 - 醚络合物溶液。任选将乙醚水溶液加入到丙烷 - 醚络合物溶液中以形成部分水解的醚/丙烷 - 醚络合物溶液。将第一结晶添加剂的溶液加入到丙烷 - 醚络合物溶液或乙醚/丙烷 - 醚络合物水溶液中以形成结晶溶液。第一结晶添加剂选自聚苯乙烯，聚丁二烯，聚苯乙烯 - 共聚丁二烯，聚异戊二烯，聚-α-甲基苯乙烯，聚苯乙烯 - 共 - 多烯，聚-α-蒎烯及其混合物。任选地，向结晶溶液中加入第二结晶添加剂。第二结晶添加剂选自角鲨烯，环十二碳三烯，降冰片烯，降冰片二烯，苯基封端的聚丁二烯，2,4-二甲基苯甲醚，3,5-二甲基苯甲醚，2,6-二甲基苯甲醚，聚二甲基硅氧烷和混合物其溶剂从结晶溶液中除去以使α-烷烃结晶。

3. 发明申请

US20050222445A1 METHOD FOR THE PRODUCTION OF ALPHA-ALANE 有权
标题翻译： ALPHA-ALANE生产方法
公开(公告)号：US20050222445A1
公开(公告)日：2005-10-06
申请号：US10947078
申请日：2004-09-22
申请人： Gary Lund , Jami Hanks , Harold Johnston
发明人： Gary Lund , Jami Hanks , Harold Johnston
IPC分类号： C01B3/00 , C01B6/06 , C07F5/06
CPC分类号： C01B6/06 , C01B3/00 , Y02E60/324
摘要： A method of forming alpha-alane. The method includes reacting aluminum trichloride and an alkali metal hydride to form an alane-ether complex solution. An aqueous ether solution is optionally added to the alane-ether complex solution to form a partially hydrolyzed ether/alane-ether complex solution. A solution of a crystallization additive is added to the alane-ether complex solution or to the aqueous ether/alane-ether complex solution to form a crystallization solution. The crystallization additive is selected from the group consisting of squalene, cyclododecatriene, norbomylene, norbomadiene, a phenyl terminated polybutadiene, 2,4-dimethyl anisole, 3,5-dimethyl anisole, 2,6-dimethyl anisole, polydimethyl siloxane, and mixtures thereof. Ether is removed from the crystallization solution to crystallize the alpha-alane.
摘要翻译：形成α-烯烃的方法。该方法包括使三氯化铝与碱金属氢化物反应以形成丙烯 - 醚络合物溶液。任选将乙醚水溶液加入到丙烷 - 醚络合物溶液中以形成部分水解的醚/丙烷 - 醚络合物溶液。将结晶添加剂的溶液加入到丙烷 - 醚络合物溶液或醚/丙醚 - 醚络合物水溶液中以形成结晶溶液。结晶添加剂选自角鲨烯，环十二碳三烯，降冰片烯，降冰片二烯，苯基封端的聚丁二烯，2,4-二甲基苯甲醚，3,5-二甲基苯甲醚，2,6-二甲基苯甲醚，聚二甲基硅氧烷及其混合物。从结晶溶液中除去乙醚以结晶α-丙烯。

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