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1. 发明申请

WO2019220707A1 テトラヒドロほう酸塩の製造方法审中-公开
公开(公告)号：WO2019220707A1
公开(公告)日：2019-11-21
申请号：PCT/JP2019/004873
申请日：2019-02-12
申请人：新東工業株式会社
发明人：長坂　政彦 , 石田　外茂二
IPC分类号： C01B6/17 , C01B35/02
摘要：本開示は、ほう酸塩及び炭素系還元剤を含む被処理物に対し、水素を構成元素として含有するガス雰囲気中で、粉砕メディアを用いてメカノケミカル処理を施すメカノケミカル処理工程を備える、テトラヒドロほう酸塩の製造方法に関する。

2. 发明申请

WO2019220708A1 テトラヒドロほう酸塩の製造方法审中-公开
公开(公告)号：WO2019220708A1
公开(公告)日：2019-11-21
申请号：PCT/JP2019/004901
申请日：2019-02-12
申请人：新東工業株式会社
发明人：長坂　政彦 , 石田　外茂二
IPC分类号： C01B6/17 , C01B35/02
摘要：本開示は、ほう酸塩及び鉄系還元剤を含む被処理物に対し、水素を構成元素として含有するガス雰囲気中で、粉砕メディアを用いてメカノケミカル処理を施すメカノケミカル処理工程を備える、テトラヒドロほう酸塩の製造方法に関する。

3. 发明申请

WO2018170304A1 METHODS OF PRODUCING COBALT NANOPARTICLES AND HOLLOW METAL NANOSPHERES 审中-公开
公开(公告)号：WO2018170304A1
公开(公告)日：2018-09-20
申请号：PCT/US2018/022713
申请日：2018-03-15
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
发明人： LINDLEY, Sarah , ZHANG, Jin
IPC分类号： B01J31/02 , B01J31/12 , B01J31/14 , C01B6/15 , C01B6/17 , C01G51/00
摘要： Provided are methods of producing cobalt-based nanoparticles (Co x B y NPs) of a pre-selected diameter. The methods include reducing Co 2+ ions with a sodium borohydride (NaBH 4 ) solution having a selected ratio of tetrahydroxyborate (B(OH) 4 - ) to tetrahydroborate (BH 4 - ) based on the pre-selected diameter, where the ratio of B(OH) 4 - to BH 4 - is positively correlated with the pre-selected diameter. Also provided are methods of using the Co x B y NPs to produce hollow metal nanospheres (HMNs). Methods of producing Co x B y NP core / metal shell structures are also provided, such methods including combining in an anaerobic galvanic exchange reaction a deaerated solution including Co x B y NP scaffolds and a deaerated solution including a metal. Also provided are methods of producing HMNs from the Co x B y NP core / metal shell structures. Compositions and kits that find use in practicing the methods of the present disclosure and using HMNs produced in accordance with the methods of the present disclosure, are also provided.

4. 发明申请

WO2017078534A3 METHOD FOR PRODUCING METAL BOROHYDRIDE AND MOLECULAR HYDROGEN 审中-公开
标题翻译：生产金属硼氢化物和分子氢的方法
公开(公告)号：WO2017078534A3
公开(公告)日：2017-05-11
申请号：PCT/NL2016/050776
申请日：2016-11-07
申请人： H2FUEL CASCADE B.V.
发明人： LUGTIGHEID, Gerardus Wilhelmus
IPC分类号： C01B3/06 , C01B6/17
摘要： Method for producing a metal borohydride and/or H 2 . The method comprises the following steps: A. producing a metal borohydride in a synthesis process, in which H 2 is a reactant and the reaction further takes metal hydroxide and boron oxide or further takes metal boron oxide; B. producing H 2 in a chemical reaction process, in which metal borohydride produced in step A and H 2 O are reactants, the amount of H 2 produced in step B being larger than the amount of H 2 required as a reactant in step A for the same amounts of metal borohydride as a reactant and a reaction product in steps B and A, respectively; and C. providing H 2 produced in step C to step A, and repeating steps A, B and C. Part of the metal borohydride and/or H 2 produced in steps A and B, respectively, is withdrawn while leaving an amount of metal borohydride and H 2 , respectively, so as to allow repeating steps A, B and C.
摘要翻译：用于生产金属硼氢化物和/或H 2的方法。该方法包括以下步骤：A.在合成过程中制备金属硼氢化物，其中H 2 O为反应物，反应进一步为金属氢氧化物和氧化硼或进一步为金属硼氧化物; B.在化学反应过程中产生H 2 O，其中步骤A中产生的金属硼氢化物和H 2 O为反应物，H 2 O的量为在步骤B中产生的反应物的量大于在步骤A中反应物所需的量H 2分别大于在步骤B和A中作为反应物和反应产物的相同量的金属硼氢化物; 和C.将步骤C中产生的H 2 O提供至步骤A，并重复步骤A，B和C.部分步骤B中产生的金属硼氢化物和/或H 2 分别取出A和B，同时分别留下一定量的金属硼氢化物和H 2，以便允许重复步骤A，B和C.

5. 发明申请

WO2017078534A2 METHOD FOR PRODUCING METAL BOROHYDRIDE AND MOLECULAR HYDROGEN 审中-公开
标题翻译：生产金属硼氢化物和分子氢的方法
公开(公告)号：WO2017078534A2
公开(公告)日：2017-05-11
申请号：PCT/NL2016/050776
申请日：2016-11-07
申请人： H2FUEL CASCADE B.V.
发明人： LUGTIGHEID, Gerardus Wilhelmus
IPC分类号： C01B3/06 , C01B6/17
CPC分类号： C01B3/065 , C01B6/17 , Y02E60/362
摘要： Method for producing a metal borohydride and/or H 2 . The method comprises the following steps: A. producing a metal borohydride in a synthesis process, in which H 2 is a reactant and the reaction further takes metal hydroxide and boron oxide or further takes metal boron oxide; B. producing H 2 in a chemical reaction process, in which metal borohydride produced in step A and H 2 O are reactants, the amount of H 2 produced in step B being larger than the amount of H 2 required as a reactant in step A for the same amounts of metal borohydride as a reactant and a reaction product in steps B and A, respectively; and C. providing H2 produced in step C to step A, and repeating steps A, B and C. Part of the metal borohydride and/or H 2 produced in steps A and B, respectively, is withdrawn while leaving an amount of metal borohydride and H 2 , respectively, so as to allow repeating steps A, B and C.
摘要翻译：用于生产金属硼氢化物和/或H 2的方法。该方法包括以下步骤：A.在合成过程中制备金属硼氢化物，其中H 2 O为反应物，反应进一步为金属氢氧化物和氧化硼或进一步为金属硼氧化物; B.在化学反应过程中产生H 2 O，其中步骤A中产生的金属硼氢化物和H 2 O为反应物，H 2 O的量为在步骤B中产生的反应物的量大于在步骤A中反应物所需的量H 2分别大于在步骤B和A中作为反应物和反应产物的相同量的金属硼氢化物; 和C.将步骤C中产生的H 2提供至步骤A，并且重复步骤A，B和C.分别在步骤A和B中产生的部分金属硼氢化物和/或H 2 O 同时分别留下一定量的硼氢化金属和H 2，以允许重复步骤A，B和C.

6. 发明申请

WO2021112670A1 METHOD FOR PRODUCING METAL BOROHYDRIDE FROM METAL BORON OXIDE 审中-公开
公开(公告)号：WO2021112670A1
公开(公告)日：2021-06-10
申请号：PCT/NL2020/050750
申请日：2020-12-02
申请人： H2FUEL-SYSTEMS B.V.
发明人： LUGTIGHEID, Gerardus Wilhelmus
IPC分类号： C01B6/17 , C01B6/11
摘要： A method for producing metal borohydride, Me(BH4)n, from metal boron oxide, Me(BO2)n, in which Me is a metal or a molecule that shows metal-like behaviour and can act as a metal, and n is an integer number that can be associated with the valence of the metal, wherein in a first fluidized bed step the metal boron oxide is provided in a first fluidized bed. The first fluidized bed is fluidized using a gas selected from at least one of nitrogen, N2, gas and a noble gas, optionally the noble gas being selected from at least one of helium, He; neon, Ne; argon, Ar; and xenon, Xe, under such circumstances, especially pressure and temperature, that oxygen atoms are removed from the metal boron oxide to provide metal boron, MeBn, particles, possibly ions. In a subsequent second fluidized bed step the metal boron particles are provided in a second fluidized bed that is fluidized using hydrogen, H2, gas under such circumstances that hydrogen chemically reacts with the metal boron particles to provide metal borohydride.

7. 发明申请

WO2005074531A3 METHODS OF SYNTHESIS OF ISOTOPICALLY ENRICHED BOROHYDRIDE AND METHODS OF SYNTHESIS OF ISOTOPICALLY ENRICHED BORANES 审中-公开
标题翻译：同位素丰富的硼氢化合物的合成方法和同位素丰富的硼烷的合成方法
公开(公告)号：WO2005074531A3
公开(公告)日：2007-01-18
申请号：PCT/US2005002629
申请日：2005-01-28
申请人： SEMEQUIP INC , SPIELVOGEL BERNARD , COOK KEVIN
发明人： SPIELVOGEL BERNARD , COOK KEVIN
IPC分类号： C07C69/76 , C01B6/17 , C01B6/21 , C01B15/037 , C07F5/04 , H01L21/336
CPC分类号： C01B6/17 , C01B6/21 , C07F5/04
摘要： The invention provides new methods for the synthesis of isotopically enriched metal borohydrides, metal tetrahydroundecaborate salts, and decaborane from isotopically enriched 10 B-boric acid or 11 B-boric acid. The invention is particularly useful for synthesis of isotopically enriched sodium or lithium borohydride, MB 11 H 14 (where M is Li, Na, K, or alkylammonium), and decaborane.
摘要翻译：本发明提供了从同位素富集的B-boric acid或11-B-boric acid合成同位素富集的金属硼氢化物，四氢十八硼酸盐金属和十硼烷的新方法。本发明特别可用于合成同位素富集的硼氢化钠或硼氢化钠，其中M为Li，Na，K或烷基铵）和十硼烷。

8. 发明申请

WO2005074531A2 METHODS OF SYNTHESIS OF ISOTOPICALLY ENRICHED BOROHYDRIDE AND METHODS OF SYNTHESIS OF ISOTOPICALLY ENRICHED BORANES 审中-公开
标题翻译：同位素丰富的硼氢化合物的合成方法和同位素丰富的硼烷的合成方法
公开(公告)号：WO2005074531A2
公开(公告)日：2005-08-18
申请号：PCT/US2005/002629
申请日：2005-01-28
申请人： SEMEQUIP INC. , SPIELVOGEL, Bernard , COOK, Kevin
发明人： SPIELVOGEL, Bernard , COOK, Kevin
IPC分类号： C01B6/17 , C01B6/21 , C01B15/037 , C07F5/04 , H01L21/336
CPC分类号： C01B6/17 , C01B6/21 , C07F5/04
摘要： The invention provides new methods for the synthesis of isotopically enriched metal borohydrides, metal tetrahydroundecaborate salts, and decaborane from isotopically enriched 10 B-boric acid or 11 B-boric acid. The invention is particularly useful for synthesis of isotopically enriched sodium or lithium borohydride, MB 11 H 14 (where M is Li, Na, K, or alkylammonium), and decaborane.
摘要翻译：本发明提供了同位素富集的金属硼氢化物，四氢十八硼酸盐金属盐和来自同位素富含的B-boric acid或11硼酸的十硼烷的新方法。本发明特别可用于合成同位素富集的硼氢化钠或硼氢化钠MB11H14（其中M为Li，Na，K或烷基铵）和十硼烷。

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