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1. 发明申请

WO2014139335A1 铁、铝、钛还原熔盐法无渣生产工艺审中-公开
公开(公告)号：WO2014139335A1
公开(公告)日：2014-09-18
申请号：PCT/CN2014/070655
申请日：2014-01-15
申请人：胡长春 , 胡晓雪
发明人：胡长春 , 胡晓雪
IPC分类号： C21B11/00 , F27D17/00
CPC分类号： C21C5/56 , C22B21/02 , C22B34/1263 , F27B19/04 , F27D17/004
摘要：铁、铝、钛还原熔盐法无渣生产工艺，包括以下步骤：1）在熔盐反应罐（3）中加入硫酸铵；2）加入高温熔融渣；3）氨气输入到低温余热发电（5）；4）将硫酸铝、硫酸氧钛、二氧化硅和硫酸钙通入到第一固液分离（11）内；5）将氨水精馏，泵入熔分炉裂解管（2b）；6）裂解气通入到回转窑内（1）；7）液氨输送到硫酸铝溶液罐（14）中；8）硫酸铝、硫酸氧钛水解；9）由第二固液分离（13）分离。它彻底解决高温熔融渣潜热能、有价元素无法提取利用的难题。

2. 发明申请

WO2003106081A1 METHOD FOR FABRICATING A METALLIC ARTICLE WITHOUT ANY MELTING 审中-公开
标题翻译：一种没有任何熔化的金属制品的制造方法
公开(公告)号：WO2003106081A1
公开(公告)日：2003-12-24
申请号：PCT/US2003/018700
申请日：2003-06-12
申请人： GENERAL ELECTRIC COMPANY
发明人： WOODFIELD, Andrew, Philip , OTT, Eric, Allen , SHAMBLEN, Clifford, Earl
IPC分类号： B22F3/00
CPC分类号： C22B34/1295 , B22F3/001 , B22F9/18 , B22F2998/00 , C22B4/06 , C22B34/1263 , B22F9/28 , B22F3/12 , B22F3/15 , B22F3/17 , B22F3/20
摘要： A metallic article (20) made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds is chemically reduced to produce an initial metallic material, without melting the initial metallic material. The initial metallic material is consolidated to produce a consolidated metallic article (20), without melting the initial metallic material and without melting the consolidated metallic article (20).
摘要翻译：由金属构成元件制成的金属制品（20）由金属构成元件的非金属前体化合物的混合物制成。化学还原非金属前体化合物的混合物以产生初始金属材料，而不熔化初始金属材料。初始金属材料被固结以产生固结的金属制品（20），而不熔化初始金属材料并且不熔化固结的金属制品（20）。

3. 发明申请

WO1998014622A1 PROCESS FOR OBTAINING TITANIUM OR OTHER METALS USING SHUTTLE ALLOYS 审中-公开
标题翻译：使用合金合金获得钛或其他金属的工艺
公开(公告)号：WO1998014622A1
公开(公告)日：1998-04-09
申请号：PCT/AU1997000624
申请日：1997-09-23
申请人： KLEEMAN, Ashley , FORTIN, Claude
发明人： KLEEMAN, Ashley
IPC分类号： C22B05/00
CPC分类号： C22B34/1277 , C22B5/04 , C22B34/1218 , C22B34/1263 , Y02P10/23
摘要： The present invention relates to a process for obtaining metals from oxides using shuttle alloys, particularly titanium metal from titanium dioxide in the form of illmenite, rutile. The process can be adapted to obtain elemental metal or alloys of metals such as zirconium, chromium, molybdenum, tungsten, tantalum, lithium, cobalt and zinc. The process of the present invention comprises two stages, a first stage in which a metal oxide is reduced in the presence of primary shuttle material, which forms a shuttle alloy with the reduced metal, and a second stage wherein the reduced metal is separated from the shuttle alloy as a metal or alloy. Typically the primary shuttle material comprises bismuth or antimony or a mixture of the two and optionally lead. The reduction reaction may be carried out by chemical means or electrochemical means or by a combination of the two. The process permits the two stages to be linked and the process run continuously such that energy recovered from the second stage may be transferred to the first stage and used to drive the reduction of the metal oxide or other reactions, such as the decarbonisation of calcium carbonate used as a melting agent. The addition of material such as silica to the process, may facilitate recovery of by-products such as aluminous cements.
摘要翻译：本发明涉及一种使用梭合金，特别是钛金属，由钛铁矿，金红石形式的二氧化钛从氧化物中获得金属的方法。该方法可适用于获得元素金属或诸如锆，铬，钼，钨，钽，锂，钴和锌的金属合金。本发明的方法包括两个阶段：第一阶段，其中金属氧化物在存在主要穿梭材料的情况下被还原，其与还原金属形成穿梭合金，以及第二阶段，其中还原金属与穿梭合金作为金属或合金。通常，主穿梭材料包括铋或锑或两者的混合物和任选的铅。还原反应可以通过化学方法或电化学手段或两者的组合进行。该方法允许两个阶段连接，并且该过程连续运行，使得从第二阶段回收的能量可以转移到第一阶段并用于驱动金属氧化物或其它反应的还原，例如碳酸钙的脱碳用作熔化剂。在该方法中添加诸如二氧化硅的材料可以促进副产物如铝土壤的回收。

4. 发明申请

WO1996020892A1 METHODS AND SYSTEMS FOR PRODUCING ULTRA HIGH PURITY TITANIUM TETRAIODIDE (TiI4) AND ULTRA HIGH PURITY TITANIUM METAL 审中-公开
标题翻译：用于生产超高钛酸四铁（TiI4）和超高纯度钛金属的方法和系统
公开(公告)号：WO1996020892A1
公开(公告)日：1996-07-11
申请号：PCT/US1995004870
申请日：1995-04-24
申请人： MATERIALS RESEARCH CORPORATION
发明人： MATERIALS RESEARCH CORPORATION , LAM, Raymond, K., F.
IPC分类号： C01G23/02
CPC分类号： C22B34/1263 , C01G23/02 , C22B34/1222 , C22B34/1277 , Y02P10/23
摘要： Systems and methods are provided for producing ultra high purity titanium tetraiodide, on the order of at least 99.998 % pure, and for producing ultra high purity titanium metal having a purity of greater than 99.998 % pure. The system includes a titanium tetraiodide generating subsystem; a titanium tetraiodide purification subsystem wherein titanium tetraiodide is refined to ultra high purity by a double distillation process at reduced pressure; and a titanium tetraiodide decomposition subsystem wherein titanium tetraiodide is decomposed and ultra high purity titanium metal is deposited on a deposition substrate. The ultra high purity titanium tetraiodide can be used as a precursor for the titanium metal production, or it may be utilized in other semiconductor applications. Also contemplated are methods of making ultra high purity metal halides wherein the halide is selected from the group consisting of bromides, chlorides, iodides and fluorides.
摘要翻译：提供了用于生产纯度高达99.998％的超高纯度四碘化钛的系统和方法，以及用于生产纯度高于99.998％纯度的超高纯钛金属。该系统包括四碘化钛生成子系统; 四碘化钛净化子系统，其中通过双蒸馏方法在减压下将四碘化钛精制成超高纯度; 和四碘化钛分解的四碘化钛分解子系统，并且在沉积基板上沉积超高纯度钛金属。超高纯钛四碘化钛可用作钛金属生产的前体，或者可用于其它半导体应用。还考虑制备超高纯度金属卤化物的方法，其中卤化物选自溴化物，氯化物，碘化物和氟化物。

5. 发明申请

WO2013096893A1 A SYSTEM AND METHOD FOR EXTRACTION AND REFINING OF TITANIUM 审中-公开
标题翻译：一种提取和精制钛的系统和方法
公开(公告)号：WO2013096893A1
公开(公告)日：2013-06-27
申请号：PCT/US2012/071467
申请日：2012-12-21
申请人： UNIVERSAL TECHNICAL RESOURCE SERVICES, INC.
发明人： COX, James, R. , DEALWIS, Chanaka, L. , KOHLER, Benjamin, A. , LEWIS, Michael, G.
IPC分类号： C22B34/12 , C22B3/02
CPC分类号： C25C3/28 , C22B34/1263 , C22B34/1277 , C22C14/00
摘要： A method to extract and refine metal products from metal-bearing ores, including a method to extract and refine titanium products. Titanium products can be extracted from titanium-bearing ores with TiO 2 and impurity levels unsuitable for conventional methods.
摘要翻译：一种从金属矿石中提取和精炼金属产品的方法，包括提取和精制钛产品的方法。可以从含钛的矿石中提取钛产品，而不适用于常规方法。

6. 发明申请

WO2006027612A2 IMPROVED ELECTROLYTIC METHOD APPARATUS AND PRODUCT 审中-公开
标题翻译：改进的电解方法设备和产品
公开(公告)号：WO2006027612A2
公开(公告)日：2006-03-16
申请号：PCT/GB2005003497
申请日：2005-09-09
申请人： UNIV CAMBRIDGE TECH , BRITISH TITANIUM PLC , FRAY DEREK JOHN , SCHWANDT CARSTEN , DOUGHTY GREG
发明人： FRAY DEREK JOHN , SCHWANDT CARSTEN , DOUGHTY GREG
CPC分类号： C25C3/00 , C22B34/1263 , C22B34/129 , C25C3/28 , C25C5/04
摘要： In an electro-decomposition process a cathode comprising a metal compound is contacted with a fused salt electrolyte in an electrochemical cell. The metal compound is a compound between a metal and another substance, and a voltage is applied between the cathode and an anode such that the substance is removed from the metal compound. In the improved method, the applied voltage increases with time, either continuously or stepwise, up to a predetermined maximum voltage. In addition, or in the alternative, the fused salt composition is selected so as to maintain a predetermined concentration of the substance in the fused salt during electro-decomposition.
摘要翻译：在电解分解过程中，包含金属化合物的阴极在电化学电池中与熔融盐电解质接触。金属化合物是金属与另一物质之间的化合物，并且在阴极和阳极之间施加电压，使得物质从金属化合物中除去。在改进的方法中，施加的电压随时间而连续地或逐步地增加直到预定的最大电压。此外，或者在替代方案中，选择熔融盐组合物以便在电分解期间将物质保持在熔融盐中的预定浓度。

7. 发明申请

WO02061168A2 METHODS OF FORMING TITANIUM-BASED AND ZIRCONIUM-BASED MIXED-METAL MATERIALS; AND SPUTTERING TARGETS 审中-公开
标题翻译：形成基于金属和基于锆的混合金属材料的方法; 和飞溅目标
公开(公告)号：WO02061168A2
公开(公告)日：2002-08-08
申请号：PCT/US0150645
申请日：2001-10-17
申请人： HONEYWELL INT INC
发明人： TURNER STEPHEN P , GREEN JOSEPH E , SCAGLINE RODNEY L , XU YUN
IPC分类号： C22B5/04 , C22B5/12 , C22B34/12 , C22B34/14 , C22C14/00 , C22C16/00 , C23C14/34 , C25C3/26 , C22B34/00 , C22C27/00 , C23C16/08
CPC分类号： C22B34/14 , C22B34/1263 , C23C14/3414
摘要： The invention encompasses methods of forming titanium-based mixed-metal materials and zirconium-based mixed-metal materials utilizing one or more of a reduction process, electrolysis process and iodide process. The invention also encompasses a sputtering target comprising zirconium and one or more elements selected from the group consisting of Al, B, Ba, Be, Ca, Ce, Co, Cs, Dy, Er, Fe, Gd, Hf, Ho, La, Mg, Mn, Mo, Nb, Ni, Pr, Sc, Sm, Sr, Ta, Ti, V, W, Y, and Yb. The invention also encompasses a sputtering target comprising titanium and boron.
摘要翻译：本发明包括利用还原法，电解法和碘化法中的一种或多种形成钛基混合金属材料和锆基混合金属材料的方法。本发明还包括包含锆和选自Al，B，Ba，Be，Ca，Ce，Co，Cs，Dy，Er，Fe，Gd，Hf，Ho，La中的一种或多种元素的溅射靶， Mg，Mn，Mo，Nb，Ni，Pr，Sc，Sm，Sr，Ta，Ti，V，W，Y和Yb。本发明还包括包含钛和硼的溅射靶。

8. 发明申请

WO0145906A3 PRODUCTION OF METALS AND THEIR ALLOYS 审中-公开
标题翻译：金属及其合金的生产
公开(公告)号：WO0145906A3
公开(公告)日：2002-01-24
申请号：PCT/US0042699
申请日：2000-12-08
申请人： MYRICK JAMES J
发明人： MYRICK JAMES J
IPC分类号： B22F9/00 , B22F9/28 , C22B34/12
CPC分类号： B22F9/28 , B22F9/002 , C22B34/1263
摘要： Methods for manufacturing titanium and zirconium alloys, particularly including such alloys in powder form by continuous vapor phase chloroaluminothermic reduction.
摘要翻译：用于制造钛和锆合金的方法，特别是包括通过连续气相氯铝热还原的粉末形式的这种合金。

9. 发明申请

WO99064638A1 REMOVAL OF OXYGEN FROM METAL OXIDES AND SOLID SOLUTIONS BY ELECTROLYSIS IN A FUSED SALT 审中-公开
标题翻译：从金属氧化物和固体溶液中通过电解在熔盐中去除氧
公开(公告)号：WO99064638A1
公开(公告)日：1999-12-16
申请号：PCT/GB1999/001781
申请日：1999-06-07
IPC分类号： C22B4/00 , C22B5/00 , C22B21/00 , C22B34/12 , C23C8/00 , C23C8/40 , C25C3/28 , C25F1/12 , C25F1/16
CPC分类号： C22B34/129 , C22B21/0038 , C22B34/1263 , C25C3/28 , C25F1/12 , C25F1/16
摘要： A method for removing a substance (X) from a solid metal or semi-metal compound (M X) by electrolysis in a melt of M Y, comprises conducting the electrolysis under conditions such that reaction of X rather than M deposition occurs at an electrode surface, and that X dissolves in the electrolyte M Y. The substance X is either removed from the surface (i.c. M X) or by means of diffusion extracted from the care material. The temperature of the fused salt is chosen below the melting temperature of the metal M . The potential is chosen below the decomposition potential of the electrolyte.
摘要翻译：通过在M 2 Y的熔体中电解从固体金属或半金属化合物（M 1 X）中除去物质（X）的方法包括在使X反应而不是 M 2沉积发生在电极表面，X溶解在电解液M 2 Y中。物质X或者通过从护理材料中提取的扩散物从表面（i.c.M 1 X）中去除。熔融盐的温度选择在金属M 1的熔融温度以下。电位低于电解液的分解电位。

10. 发明申请

WO2016142714A1 METHOD OF PRODUCING METAL 审中-公开
标题翻译：生产金属的方法
公开(公告)号：WO2016142714A1
公开(公告)日：2016-09-15
申请号：PCT/GB2016/050660
申请日：2016-03-10
申请人： METALYSIS LIMITED
发明人： DEANE, James
IPC分类号： C25C7/02 , C25C3/36 , C25C3/26 , B01J2/00 , C22B34/00
CPC分类号： C25C5/04 , B01J2/16 , B22F1/0048 , B22F9/20 , C22B34/1263 , C22C1/045 , C22C1/0458 , C22C14/00 , C25C3/26 , C25C3/36 , C25C7/025
摘要： A method of producing a non-metallic feedstock powder suitable for reduction to metal comprises the steps of combining a liquid with solid metal oxide particles to form a mixture, subjecting the mixture to high-shear mixing to form a liquid suspension of metal oxide and the liquid, and drying the liquid suspension using a fluidised-bed spray-granulation process to grow a plurality particles to form the non-metallic feedstock powder. The method allows feedstock powders to be grown to desired particle sizes. The method allows production of feedstock powders having controlled compositions.
摘要翻译：制备适合还原成金属的非金属原料粉末的方法包括以下步骤：将液体与固体金属氧化物颗粒混合以形成混合物，使混合物进行高剪切混合以形成金属氧化物的液体悬浮液和液体，并使用流化床喷雾造粒方法干燥液体悬浮液，以生长多个颗粒以形成非金属原料粉末。该方法允许原料粉末生长至所需的粒度。该方法允许生产具有受控组合物的原料粉末。

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