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1. 发明申请

WO2017137908A1 DISTILLATION OF NEUTRAL COMPOUNDS FROM TALL OIL SOAP 审中-公开
标题翻译：从高油脂肥皂中提取中性化合物
公开(公告)号：WO2017137908A1
公开(公告)日：2017-08-17
申请号：PCT/IB2017/050694
申请日：2017-02-09
申请人： STORA ENSO OYJ
发明人： KAVAKKA, Jari , LOTTI, Heikki
IPC分类号： B01D3/12 , B01D3/14 , B01D1/22 , C11B13/00
CPC分类号： B01D1/065 , B01D1/24 , B01D3/009 , B01D3/14 , B01D5/0027 , C11B13/005 , Y02W30/74
摘要： The present invention relates to isolation of phytosterols and other neutral compounds from alkaline tall oil soap (TOS) which is obtained from the Kraft process black liquor by skimming. The invention also enables the production of tall oil with high acid number.
摘要翻译：本发明涉及从由硫酸盐法黑液通过撇取获得的碱性妥尔油皂（TOS）中分离植物甾醇和其它中性化合物。本发明还能生产高酸值的妥尔油。

2. 发明申请

WO2013173029A1 PROCESS FOR SEPARATING CRUDE TALL OIL FOR PROCESSING INTO FUELS 审中-公开
标题翻译：将原油分离成燃料的方法
公开(公告)号：WO2013173029A1
公开(公告)日：2013-11-21
申请号：PCT/US2013/037681
申请日：2013-04-23
申请人： UOP LLC
发明人： PETRI, John A.
IPC分类号： C11C3/00 , C11B3/00 , C09F1/00 , C09F1/02 , C11C1/08 , C11C1/10
CPC分类号： C10G3/50 , C11B3/12 , C11B13/00 , C11B13/005 , Y02P30/20 , Y02W30/74
摘要： Crude tall oil is subjected to a distillation process that substantially removes impurities. The process produces a combined pitch and a distillate of free fatty acids and rosin acids from two vacuum columns. The distillate stream is amenable to further downstream hydroprocessing.
摘要翻译：将粗妥尔油进行基本上去除杂质的蒸馏过程。该方法从两个真空柱产生游离脂肪酸和松香酸的组合沥青和馏出物。馏出物流适合进一步的下游加氢处理。

3. 发明申请

WO2011117475A1 METHOD OF TREATING TALL OIL PITCH 审中-公开
标题翻译：石油沥青处理方法
公开(公告)号：WO2011117475A1
公开(公告)日：2011-09-29
申请号：PCT/FI2011/050257
申请日：2011-03-28
申请人： FORCHEM OY , KIVIRANTA, Esko , SAVIAINEN, Juhani , RINTOLA, Mikko
发明人： KIVIRANTA, Esko , SAVIAINEN, Juhani , RINTOLA, Mikko
IPC分类号： C11B13/00 , C07J9/00 , C11C1/02 , C07C51/09
CPC分类号： C11B13/005 , C07C51/09 , C07J9/00 , C11C1/04 , C11C3/003 , Y02W30/74
摘要： A method of treating tall oil pitch, which comprises sterol esters of fatty acids. According to the present invention, the esters of sterols and fatty acids are broken down, in which case especially formic acid esters or acetic acid esters of sterols are formed instead. The free fatty acids and sterol esters generated are distilled or separated in another way. Use of the present invention increases the yield of fatty acids and also facilitates the separation of sterols from tall oil pitch.
摘要翻译：一种处理妥尔油沥青的方法，其包括脂肪酸的甾醇酯。根据本发明，固醇和脂肪酸的酯被分解，在这种情况下，特别是形成甾醇酯或甾醇的乙酸酯。产生的游离脂肪酸和甾醇酯以另一种方式蒸馏或分离。本发明的使用增加了脂肪酸的产率，并且也促进了甾醇与妥尔油沥青的分离。

4. 发明申请

WO2008017730A1 WOOD PRESERVATIVE AND METHOD FOR MANUFACTURING WOOD PRESERVATIVE 审中-公开
标题翻译：木材防腐剂及其制造方法
公开(公告)号：WO2008017730A1
公开(公告)日：2008-02-14
申请号：PCT/FI2007/000198
申请日：2007-08-07
申请人： HÖLJÄKKÄ OY , BOREN, Hannu
发明人： BOREN, Hannu
IPC分类号： B27K3/50 , B27K3/52 , A01N61/00 , C11B13/00 , C09D15/00
CPC分类号： C09F1/02 , A01N65/06 , B27K3/34 , B27K3/36 , B27K3/50 , C09D15/00 , C11B13/005 , Y02W30/74 , A01N37/02 , A01N59/14 , A01N59/16 , A01N59/20
摘要： The invention relates to a wood preservative, which wood preservative contains vegetable oils processed from crude tall oil, such as resin acids and fatty acids. The wood preservative according to the invention is characterised by that the wood preservative is crude tall oil, from which have been removed neutral components contained by the crude tall oil, especially compounds acting as the breeding ground and nutriment of rot fungi and/or compounds causing esterification reactions, such as fatty alcohols and/or steroid groups, such as sitosterol and sitostanol. The invention also relates to a method for manufacturing wood preservative according to the invention.
摘要翻译：本发明涉及木材防腐剂，木材防腐剂含有由粗妥尔油加工的植物油，例如树脂酸和脂肪酸。根据本发明的木材防腐剂的特征在于木材防腐剂是粗的妥尔油，已经除去了粗妥尔油所含的中性成分，特别是作为滋生地的化合物和腐烂真菌和/或化合物的营养物酯化反应，如脂肪醇和/或类固醇基团，如谷甾醇和谷甾烷醇。本发明还涉及根据本发明的木材防腐剂的制造方法。

5. 发明申请

WO2007147837A1 PROCESS FOR PRODUCING TALL OIL AND USE OF HEATING IN THE PRODUCTION OF TALL OIL 审中-公开
标题翻译：生产石油和加热用于生产油的过程
公开(公告)号：WO2007147837A1
公开(公告)日：2007-12-27
申请号：PCT/EP2007/056116
申请日：2007-06-20
申请人： LINDE AKTIENGESELLSCHAFT , SELLERHOLM, Per , KJELLBERG, Nils , JÖNSSON, Jonas , NAYDENOV, Valeri , LINDSTRÖM, Curt
发明人： SELLERHOLM, Per , KJELLBERG, Nils , JÖNSSON, Jonas , NAYDENOV, Valeri , LINDSTRÖM, Curt
IPC分类号： C11B13/00
CPC分类号： C11B13/005 , Y02W30/74
摘要： The invention relates to a process for the production of tall oil from soap oil and to the use of heating in order to improve the production of tall oil. Soap oil, which has been produced by neutralization of tall oil soap, is acidulated by reacting the soap oil with an acid and freed tall oil is recovered. In the acidulation step, the temperature is raised above 100 °C, preferably over 105 °C, for improving the acidulation of soap oil. The acid is preferably concentrated sulfuric acid.
摘要翻译：本发明涉及一种从皂油生产妥尔油和加热使用以提高妥尔油的生产的方法。通过中和妥尔油皂生产的肥皂油通过使皂油与酸反应而酸化，并回收除去的妥尔油。在酸化步骤中，为了改善皂油的酸化，将温度升高到100℃以上，优选超过105℃。酸优选为浓硫酸。

6. 发明申请

WO0064921A3 PROCESS OF PURIFYING PHYTOSTEROLS FROM WOOD OR PLANT-DERIVED SOURCES BY MEANS OF METAL SALT COMPLEXES AND COMPOSITIONS RESULTING THEREFROM 审中-公开
标题翻译：通过金属盐复合物和由其衍生的组合物从木材或植物衍生来源净化植物甾醇的方法
公开(公告)号：WO0064921A3
公开(公告)日：2001-07-12
申请号：PCT/CA0000455
申请日：2000-04-27
申请人： FORBES MEDI TECH INC
发明人： COSS JAMES L , KUTNEY JAMES P , MILANOVA RADKA K , JOLLEZ PAUL
IPC分类号： A61K31/575 , A61P3/06 , A61P9/10 , C07J9/00 , C11B13/00 , C11B13/02
CPC分类号： C11B13/02 , A61K31/575 , C07J9/00 , C11B13/005 , Y02W30/74 , A61K31/57 , A61K2300/00
摘要： A universal process for purifying phytosterols from a wood or plant derived source comprises extracting from the source a concentrated extract comprising phytosterols and a hydrocarbon; complexing the extract so formed with a metal salt; separating the phytosterol/metal salt complex from the hydrocarbon; washing the complex with a solvent mixture comprising one or both of a hydrocarbon and a ketone; hydrolysing the washed complex so formed and finally separating the phytosterols therefrom. A novel composition comprises beta-sitosterol, campesterol, campestanol, sitostanol and optionally brassicasterol and brassicastanol.
摘要翻译：从木材或植物衍生来源纯化植物甾醇的通用方法包括从源中提取包含植物甾醇和烃的浓缩提取物; 使由金属盐形成的提取物络合; 将植物甾醇/金属盐络合物与烃分离; 用包含一种或两种烃和酮的溶剂混合物洗涤络合物; 水解所形成的洗涤过的配合物，最后从其中分离植物甾醇。一种新型组合物包括β-谷甾醇，菜油甾醇，菜油甾醇，谷甾烷醇和任选的菜子甾醇和黄豆酚醇。

7. 发明申请

WO00027867A1 ISOLATION AND PURIFICATION OF STEROLS FROM NEUTRALS FRACTION OF TALL OIL PITCH BY SINGLE DECANTATION CRYSTALLIZATION 审中-公开
标题翻译：通过单一代谢结晶分离和纯化来自中性点的石油沥青分离
公开(公告)号：WO00027867A1
公开(公告)日：2000-05-18
申请号：PCT/US1999/014136
申请日：1999-07-12
IPC分类号： C07J9/00 , C11B13/00
CPC分类号： C11B13/005 , C07J9/00 , Y02W30/74
摘要： Sterols from the solvent-extracted or distilled neutrals of saponified tall oil pitch are disclosed to be isolated and purified by a process of a liquid-liquid extraction where the hydrocarbon extraction stream is washed with an aqueous methanol solution to remove methanol-soluble impurities by adding the methanol and water, sequentially or as a blend. The resulting hydrocarbon/neutrals/methanol/water solution separates into an upper organic phase and a lower methanol/water phase, which lower phase is removed. The remaining organic phase is allowed to cool to from about 20-30 DEG C, with agitation, to facilitate crystallization of sterols, which crystals are recovered by filtering.
摘要翻译：公开了从溶剂提取或蒸馏的皂化的妥尔油沥青的中性粒子中的甾醇通过液 - 液萃取方法分离和纯化，其中烃萃取物流用甲醇水溶液洗涤以除去甲醇可溶性杂质，加入甲醇和水，依次或作为混合物。所得的烃/中性/甲醇/水溶液分离成上部有机相和较低的甲醇/水相，其中较低的相被除去。将剩余的有机相冷却至约20-30℃，同时搅拌，以促进固醇的结晶，通过过滤回收晶体。

8. 发明申请

WO00012533A1 ISOLATION AND PURIFICATION OF STEROLS FROM NEUTRALS FRACTION OF TALL OIL PITCH BY DIRECT CRYSTALLIZATION, DUAL PHASE 审中-公开
标题翻译：通过直接结晶，双相分离和纯化来自中性点的石油分离物
公开(公告)号：WO00012533A1
公开(公告)日：2000-03-09
申请号：PCT/US1999/014135
申请日：1999-07-12
IPC分类号： C07J9/00 , C11B13/00
CPC分类号： C11B13/005 , C07J9/00 , Y02W30/74
摘要： Isolation of the sterol component of the neutrals fraction of saponified tall oil pitch is disclosed. Sterol isolation is accomplished by a liquid-liquid extraction from the tall oil pitch-derived neutrals, resulting in a hydrocarbon (preferably heptane) phase at a relatively high temperature (preferably greater than 50 DEG C) to which small amounts of an alcohol solvent, preferably methanol, is added. To the hydrocarbon/alcohol/neutrals solution is then added water of a higher temperature, preferably 60-70 DEG C to result in the formation of two separate phases. The blended solution is allowed to cool slowly, with agitation, to facilitate crystallization of sterols. The sterols are isolated by filtration and then washed with hydrocarbon solvent to result in high yield and high purity.
摘要翻译：公开了皂化妥尔油沥青的中性部分的甾醇成分的分离。通过从妥尔油沥青衍生的中性粒子中提取液体 - 液体来实现甾烷醇分离，得到相对较高温度（优选大于50℃）的烃（优选庚烷）相，其中少量的醇溶剂，优选加入甲醇。然后向烃/醇/中性溶液中加入较高温度，优选60-70℃的水，导致形成两个分开的相。混合溶液在搅拌下缓慢冷却，以促进固醇的结晶。通过过滤分离固醇，然后用烃溶剂洗涤，得到高产率和高纯度。

9. 发明申请

WO2016189200A1 PRODUCTION OF STEROLS 审中-公开
标题翻译：生产甾体
公开(公告)号：WO2016189200A1
公开(公告)日：2016-12-01
申请号：PCT/FI2016/050353
申请日：2016-05-24
申请人： FORCHEM OY
发明人： ORTE, Juha , RINTOLA, Mikko
IPC分类号： C07J9/00 , C11B13/00 , C07C67/03 , C07J75/00
CPC分类号： C07J9/00 , C07C67/03 , C11B13/005 , C11C3/003 , Y02W30/74 , C07C69/52
摘要： Method of recovering sterols from tall oil pitch which contains steryl esters. In the method the tall oil pitch is subjected to a transefterification reaction with a lower alcohol in a reaction zone to provide a reaction product mixture containing lower alkyl fatty acid esters, free sterols, and at least some unreacted steryl esters. The invention comprises separating the transesterified esters from the reaction product mixture to form a sterol rich fraction which contains free sterols and unreacted steryl esters, liberating sterols from the unreacted steryl esters to form further free sterols, and recovering and optionally purifying the free sterols. The recovery of free sterols can be increased to up to 80 wt % or more while avoiding the formation of undesired side streams containing troublesome impurities.
摘要翻译：从含有甾醇酯的妥尔油沥青中回收固醇的方法。在该方法中，将妥尔油沥青与反应区中的低级醇进行转化反应以提供含有低级烷基脂肪酸酯，游离甾醇和至少一些未反应的甾酯的反应产物混合物。本发明包括从反应产物混合物中分离出酯交换酯形成富含固醇的级分，其含有游离甾醇和未反应的甾酯，从未反应的甾醇酯释放固醇以形成更多的游离甾醇，并回收和任选地纯化游离甾醇。游离甾醇的回收率可以提高至高达80重量％或更多，同时避免形成含有麻烦杂质的不期望的侧流。

10. 发明申请

WO2016040915A1 PROCESS FOR RECOVERING CRUDE TALL OIL 审中-公开
标题翻译：回收原油的方法
公开(公告)号：WO2016040915A1
公开(公告)日：2016-03-17
申请号：PCT/US2015/049860
申请日：2015-09-12
申请人： ARIZONA CHEMICAL COMPANY, LLC
发明人： FORAN, Charles, Douglas , SWANN, Francis, Edwin , BOWLES, Robert, Earl
IPC分类号： B03D1/14 , C11B13/00
CPC分类号： C11B13/005 , B03D1/1412 , B03D1/1431 , B03D2203/005 , C11B3/001 , C11B3/04 , C11B3/06 , C11B3/16 , Y02W30/74
摘要： A process and apparatus for recovering crude tall oil are disclosed. Acidulation of a crude tall oil soap stream generates a spent acid stream that comprises lignin and entrained crude tall oil. By subjecting the spent acid stream to dissolved gas flotation, a lignin phase comprising entrained crude tall oil can be recovered and causticized, resulting in recovery of most of the crude tall oil that was present in the spent acid stream. A clarified spent acid stream is also generated, which can be treated with caustic and utilized for a soap washing process that integrates easily into the overall CTO recovery process. The apparatus comprises a crude tall oil acidulation unit, a dissolved gas flotation unit, a causticizing unit, and a soap separation unit. The inventive process marries dissolved gas flotation, a well- known water treatment process, with causticization of a recovered lignin phase, a step known from batch acidulation, to improve overall tall oil recovery from a continuous process.
摘要翻译：公开了回收粗妥油的方法和装置。粗的妥尔油皂液流的酸化产生包含木质素和夹带的粗妥尔油的废酸流。通过使废酸流进行溶解气体浮选，可以回收包含夹带的粗妥尔油的木质素相并苛化，导致废酸流中存在的大多数粗妥尔油的回收。还产生澄清的废酸流，其可以用苛性碱处理并用于肥皂洗涤过程，其容易地整合到整个CTO回收过程中。该装置包括粗妥质油酸化单元，溶解气浮选单元，苛化单元和皂分离单元。本发明的方法将溶解气体浮选，已知的水处理过程与回收的木质素相的苛化相结合，这是从批次酸化中已知的步骤，以从连续方法提高整体妥尔油的回收率。

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