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1. 发明申请

WO2012003415A1 PROCESS FOR PREPARING MONOALKYLTIN TRIHALIDES AND DIALKYLTIN DIHALIDES 审中-公开
标题翻译：制备单羟基三乙内酰脲和二烷基二氢吲哚的方法
公开(公告)号：WO2012003415A1
公开(公告)日：2012-01-05
申请号：PCT/US2011/042730
申请日：2011-07-01
申请人： ARKEMA INC. , MERZ, George J., III , WALASAVAGE, Michelle, F. , DEELMAN, Berth, Jan , BOELE, Maarten, D., K. , GODDARD, Andrew, R. , HONNICK, William, D.
发明人： MERZ, George J., III , WALASAVAGE, Michelle, F. , DEELMAN, Berth, Jan , BOELE, Maarten, D., K. , GODDARD, Andrew, R. , HONNICK, William, D.
IPC分类号： C07F7/22
CPC分类号： C07F7/2216
摘要： The invention provides a process for producing monoalkyltin trihalide or a mixture of monoalkyltin trihalide and dialkyltin dihalide by: (a) contacting dialkyltin dihalide with an alkylation agent and, optionally, tin tetrahalide, to form a tetraalkyltin mixture comprising tetraalkyltin, trialkyltin halide, and dialkyltin dihalide; (b) reacting the tetraalkyltin mixture with tin tetrahalide to form a monoalkyltin trihalide mixture comprising monoalkyltin trihalide, dialkyltin dihalide and optionally triaklyltin halide; (c) processing the monoalkyltin trihalide mixture to separately recover the monoalkyltin trihalide and a dialkyltin dihalide stream optionally containing trialkyltin halide; and (d) recycling at least a portion of the dialkyltin dihalide stream recovered in step (c) to the contacting step (a).
摘要翻译：本发明提供了通过以下方法制备三卤化一烷基锡或三卤化二烷基锡的混合物的方法：（a）使二烷基锡二卤化物与烷基化剂和任选的四卤化锡接触，形成四烷基锡混合物，其包括四烷基锡，三烷基锡卤化物和二烷基锡卤化物; （b）使四烷基锡混合物与四卤化锡反应形成三烷基锡三卤化物混合物，其包括三烷基锡三卤化物，二烷基锡二卤化物和任选的三烷基锡卤化物; （c）处理单烷基锡三卤化物混合物以分别回收三烷基锡三卤化物和任选含有三烷基锡卤化物的二烷基锡二卤化物流; 和（d）将步骤（c）中回收的二烷基锡二卤化物物流的至少一部分再循环到接触步骤（a）。

2. 发明申请

WO00015644A1 PROCESS FOR THE SYNTHESIS OF TIN CARBAPENEM INTERMEDIATES 审中-公开
标题翻译：合成中草药中间体的方法
公开(公告)号：WO00015644A1
公开(公告)日：2000-03-23
申请号：PCT/US1999/021294
申请日：1999-09-10
IPC分类号： C07B61/00 , C07F7/22
CPC分类号： C07F7/2216
摘要： The present invention relates to a process for synthesizing novel intermediates of formula (III) wherein R is a halogen. The intermediate compounds described herein are useful for the preparation of carbapenem compounds.
摘要翻译：本发明涉及一种合成式（III）的新中间体的方法，其中R 1是卤素。本文所述的中间体化合物可用于制备碳青霉烯化合物。

3. 发明申请

WO2017109097A1 PROCESS FOR MAKING ALKYLTIN TRIHALIDES AND THEIR USE 审中-公开
标题翻译：制备烷基三癸酸酯及其用途的方法
公开(公告)号：WO2017109097A1
公开(公告)日：2017-06-29
申请号：PCT/EP2016/082425
申请日：2016-12-22
申请人： ARKEMA B.V.
发明人： DEELMAN, Berth Jan , DE PATER, Jeroen
IPC分类号： C07F15/00 , C07F7/22
CPC分类号： C07F7/2216 , C07F15/0093
摘要： The present invention relates to a process for the preparation of monoalkyltin trihalides. In particular the present invention relates to an improved process for the preparation of monoalkyltin trihalides involving a redistribution reaction. More particularly the present invention relates to an improved process for the preparation of monoalkyltin trihalides involving a redistribution reaction in presence of at least one transition metal complex, said complex containing only one monodentate phosphorus ligand per metal centre.
摘要翻译：本发明涉及制备三卤化单烷基锡的方法。特别地，本发明涉及用于制备涉及再分布反应的单烷基锡三卤化物的改进方法。更具体地说，本发明涉及一种改进的制备单烷基锡三卤化物的方法，涉及在至少一种过渡金属络合物存在下的再分配反应，所述络合物每个金属中心仅含有一个单齿磷配体。

4. 发明申请

WO2013167585A2 RECYCLING OF ORGANOTIN COMPOUNDS 审中-公开
标题翻译：有机化合物的回收
公开(公告)号：WO2013167585A2
公开(公告)日：2013-11-14
申请号：PCT/EP2013/059479
申请日：2013-05-07
申请人： UNIVERSITEIT ANTWERPEN
发明人： KUVSHINOV, Alexandr , FRANCK, Philippe , DEPRAETERE, Stefaan , MAES, Bert , DE HOUWER, Johan , WYBON, Clarence , STERCKX, Hans , SERGUEEV, Serguei
IPC分类号： C07F7/22
CPC分类号： C07F7/222 , C07F7/2212 , C07F7/2216 , C07F7/2296 , Y02P20/582
摘要： A method for the synthesis of a first organic molecule, said method comprising the steps of: a) Reacting a first reactant with an organotin reactant having at least one optionally substituted organic group having from 5 to 20 carbon atoms selected from alkyl, alkenyl, alkynyl, alkoxyalkyl, alkoxy, alkylthioalkyl, carboxylates and alkylaminoalkyl groups, thereby forming a mixture of a product and a tin-containing by-product, and b) Removing most of the tin-containing by-product from said mixture in such a way as to provide a purified product comprising less than 1000 ppm of remaining tin-containing by- product, wherein said step of removing most of said tin-containing by-product is either an extraction between a first liquid and a second liquid, said second liquid being more polar than said first liquid and at least partly immiscible therewith or is a reversed phase chromatography.
摘要翻译：一种合成第一有机分子的方法，所述方法包括以下步骤：a）用具有至少一个选自烷基，烯基，炔基的至少一个任选取代的具有5至20个碳原子的有机基团的有机锡反应物反应第一反应物，烷氧基烷基，烷氧基，烷硫基烷基，羧酸酯和烷基氨基烷基，从而形成产物和含锡副产物的混合物，和b）从所述混合物中除去大部分含锡副产物，提供包含小于1000ppm剩余的含锡副产物的纯化产物，其中所述除去大部分所述含锡副产物的步骤是在第一液体和第二液体之间的提取，所述第二液体更多极性比所述第一液体至少部分地与其不混溶，或者是反相色谱法。

5. 发明申请

WO2012001703A1 IONIC FLUIDS 审中-公开
标题翻译：离子液体
公开(公告)号：WO2012001703A1
公开(公告)日：2012-01-05
申请号：PCT/IN2011000422
申请日：2011-06-22
申请人： RELIANCE IND LTD , PAVAN KUMAR ADURI , PARASUVEERA UPPARA , UDAY RATNAPARKHI , NANGESH SAKHALKAR
发明人： PAVAN KUMAR ADURI , PARASUVEERA UPPARA , UDAY RATNAPARKHI , NANGESH SAKHALKAR
IPC分类号： B01F3/08
CPC分类号： B01J27/138 , C07D213/04 , C07F1/04 , C07F1/08 , C07F3/06 , C07F5/069 , C07F7/2216 , C07F13/005 , C07F15/025 , H01B1/122 , H01M10/0566 , H01M2300/0045
摘要： A method for preparing an ionic compound by mixing at least one compound of formula CxAy-zH20 (1) with at least one hydrogen donor and heating the mixture obtained is provided. The said ionic compound remains in a physical state selected from the group consisting of liquid and semisolid at a temperature below 150°C, preferably below 125 °C.
摘要翻译：提供了通过将至少一种式C x A y-z H 20（1）的化合物与至少一个氢供体并且加热获得的混合物来制备离子化合物的方法。所述离子化合物在低于150℃，优选低于125℃的温度下保持选自液体和半固体的物理状态。

6. 发明申请

WO02057277A8 PROCESS FOR THE PRODUCTION OF MONOALKYLTIN TRIHALIDES 审中-公开
标题翻译：生产单羟基胆碱酯的方法
公开(公告)号：WO02057277A8
公开(公告)日：2003-11-13
申请号：PCT/NL0200045
申请日：2002-01-21
申请人： ATOFINA VLISSINGEN B V , THOONEN SANDER , VAN KOTEN GERARD , DEELMAN BERTH JAN
发明人： THOONEN SANDER , VAN KOTEN GERARD , DEELMAN BERTH JAN
IPC分类号： C07B61/00 , C07F7/22
CPC分类号： C07F7/2216
摘要： The present invention is directed to a process for the production of monoalkyltin trihalides of the formula RSnX3 wherein R-alkyl or cycloalkyl and X-C1, Br or I, involving a redistribution reaction between tetraorganotins, triorganotin halides or diorganotin halides and tin tetrahalides, said process comprising contacting tetra-(R4Sn), tri-(R3SnX) or diorganotin halides (R2SnX2) with SnX4 to afford said monoorganotin trihalides in the presence of at least one transition metal complex, said complex comprising at least one transition metal, M, selected from Group VIII of the periodic Table of elements, at least one monodentate ligand or bidentate ligand, L, L' or L", and optionally one or more anions, X, of an organic or inorganic acid, as a catalyst or catalyst precursor.
摘要翻译：本发明涉及一种制备式RSnX 3的单烷基锡三卤化物的方法，其中R-烷基或环烷基和X-C1，Br或I涉及四有机锡，三有机锡卤化物或二有机锡卤化物和四卤化锡之间的再分布反应，所述方法包括使四 - （R4Sn），三 - （R3SnX）或二有机锡卤化物（R2SnX2）与SnX4接触以在至少一种过渡金属络合物存在下提供所述单有机锡三卤化物，所述络合物包含至少一种过渡金属M 元素周期表第VIII族，至少一种单齿配位体或二齿配体L，L'或L“，以及任选的一种或多种有机或无机酸的阴离子X作为催化剂或催化剂前体。

7. 发明申请

WO2007006783A1 PROCESS FOR THE PREPARATION OF MONOALKYLTIN TRIHALIDES AND DIALKYLTIN DIHALIDES 审中-公开
标题翻译：制备单羟基三聚物和二烷基二氢吲哚的方法
公开(公告)号：WO2007006783A1
公开(公告)日：2007-01-18
申请号：PCT/EP2006/064098
申请日：2006-07-11
申请人： ARKEMA VLISSINGEN BV , BOELE, Maarten , DEELMAN, Berth-Jan , VAN KOTEN, Gerard , WAGNER, Erika Monika
发明人： BOELE, Maarten , DEELMAN, Berth-Jan , VAN KOTEN, Gerard , WAGNER, Erika Monika
IPC分类号： C07F7/22
CPC分类号： C07F7/2216
摘要： The present invention relates to a process for the production of monoalkyltin trihalides of the formula RSnHal 3 , in which R = alkyl or cycloalkyl and Hal = Cl. Br or l. Said process comprises contacting the corresponding alkene or cycioalkene, stannous halide SnHal 2 , hydrogen halide HHal and optionally Sn metal, in the presence of at least one transition metal-based catalyst, thereafter isolating the monoalkyltin trihalides from the medium. The present invention also relates to a process for the production of dialkyltin dihalides of the formula R 2 SnHal 2 from monoalkyltin trihalides of the formula RsnHal 3 , . in which R = alkyl or cycloalkyl and Hal = Cl, Br or l. Said process comprises contacting monoalkyltin trihalides RsnHal 3 and Sn metal, optionally thereafter isolating the dialkyltin dihalides R 2 SnHal 2 from the medium.
摘要翻译：本发明涉及制备式RSnHal 3的单烷基锡三卤化物的方法，其中R =烷基或环烷基，Hal = Cl。 Br或l。所述方法包括在至少一种基于过渡金属的催化剂的存在下，使相应的烯烃或环烯烃，卤化亚锡SnH 2 O 2，卤化氢氦气和任选的Sn金属接触，然后将三烷基锡卤化物从中。本发明还涉及一种由式R 2 N 2 O 2的单烷基锡三卤化物制备式R 2 SnH 2/2的二烷基锡二卤化物的方法， ^，。

8. 发明申请

WO2006007407A1 AIR-ACTIVATED ORGANOTIN CATALYSTS FOR POLYURETHANE SYNTHESIS 审中-公开
标题翻译：用于聚氨酯合成的空气活化的有机锡催化剂
公开(公告)号：WO2006007407A1
公开(公告)日：2006-01-19
申请号：PCT/US2005/021346
申请日：2005-06-16
申请人： E.I. DUPONT DE NEMOURS AND COMPANY , FELDMAN, Jerald , MCLAIN, Stephan, J.
发明人： FELDMAN, Jerald , MCLAIN, Stephan, J.
IPC分类号： C08G18/24
CPC分类号： B01J31/122 , B01J31/0202 , B01J31/0207 , B01J31/0211 , B01J31/28 , B01J2231/14 , B01J2231/341 , B01J2531/42 , C07F7/2216 , C07F7/2292 , C08G18/242 , C08G18/346 , C08G18/792 , C09D175/04
摘要： This invention relates to an organotin-based catalyst system for polyurethane synthesis that is useful in coatings applications. The catalyst has low activity in the absence of oxygen. When a coating mixture comprising the catalyst is sprayed and/or applied to a substrate as a thin film in air, the catalyst is activated. For solvent-based refinish systems comprising hydroxyl and isocyanate species at high solids levels, the catalyst system therefore provides extended viscosity stability, i.e., pot life.
摘要翻译：本发明涉及在涂料应用中有用的用于聚氨酯合成的基于有机锡的催化剂体系。催化剂在没有氧的情况下具有低活性。当含有催化剂的涂料混合物在空气中作为薄膜喷涂和/或施加到基材上时，催化剂被活化。对于包含高固体含量的羟基和异氰酸酯物质的基于溶剂的修补体系，催化剂体系因此提供了延长的粘度稳定性，即适用期。

9. 发明申请

WO2005118600A2 PROCESS FOR THE PREPARATION OF HYDROCARBYL HALIDES 审中-公开
标题翻译：制备氢氯酸盐的方法
公开(公告)号：WO2005118600A2
公开(公告)日：2005-12-15
申请号：PCT/EP2005005496
申请日：2005-05-20
申请人： BAERLOCHER ITALIA S P A , COMINI ANDREA , MAYUKH GANESH WARAWDEKAR , ANAND PADMAKAR GOKHALE , RAJENDRA SHANTILAL KASLIWAL , GITA ANIL BENDALE
发明人： COMINI ANDREA , MAYUKH GANESH WARAWDEKAR , ANAND PADMAKAR GOKHALE , RAJENDRA SHANTILAL KASLIWAL , GITA ANIL BENDALE
IPC分类号： C07F7/22
CPC分类号： C07F7/2216
摘要： Described is a process for the preparation of hydrocarbyl metal halides, such as alkyl tin chlorides, in which a reaction between the metal in its metallic state and a hydrocarbyl halide is catalyzed by a dihydrocarbyl sulfoxide or a dihydrocarbyl formamide in the presence of a hydrocarbyl metal halide and wherein the pressure of the reaction vessel is varied during the reaction.
摘要翻译：描述了制备烃基金属卤化物的方法，例如烷基氯化锡，其中金属状态的金属与烃基卤化物之间的反应在二烃基亚砜或二烃基甲酰胺中在烃基金属的存在下催化卤化物，并且其中反应容器的压力在反应期间变化。

10. 发明申请

WO02057277A1 PROCESS FOR THE PRODUCTION OF MONOALKYLTIN TRIHALIDES 审中-公开
标题翻译：生产单羟基胆碱酯的方法
公开(公告)号：WO02057277A1
公开(公告)日：2002-07-25
申请号：PCT/NL2002/000045
申请日：2002-01-21
IPC分类号： C07B61/00 , C07F7/22
CPC分类号： C07F7/2216
摘要： The present invention is directed to a process for the production of monoalkyltin trihalides of the formula RSnX3 wherein R-alkyl or cycloalkyl and X-C1, Br or I, involving a redistribution reaction between tetraorganotins, triorganotin halides or diorganotin halides and tin tetrahalides, said process comprising contacting tetra-(R4Sn), tri-(R3SnX) or diorganotin halides (R2SnX2) with SnX4 to afford said monoorganotin trihalides in the presence of at least one transition metal complex, said complex comprising at least one transition metal, M, selected from Group VIII of the periodic Table of elements, at least one monodentate ligand or bidentate ligand, L, L' or L", and optionally one or more anions, X, of an organic or inorganic acid, as a catalyst or catalyst precursor.
摘要翻译：本发明涉及一种制备式RSnX 3的单烷基锡三卤化物的方法，其中R-烷基或环烷基和X-C1，Br或I涉及四有机锡，三有机锡卤化物或二有机锡卤化物和四卤化锡之间的再分布反应，所述方法包括使四 - （R4Sn），三 - （R3SnX）或二有机锡卤化物（R2SnX2）与SnX4接触以在至少一种过渡金属络合物存在下提供所述单有机锡三卤化物，所述络合物包含至少一种过渡金属M 元素周期表第VIII族，至少一种单齿配位体或二齿配体L，L'或L“，以及任选的一种或多种有机或无机酸的阴离子X作为催化剂或催化剂前体。

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