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1. 发明申请

WO2007081243A2 METHOD FOR EXTRACTING PRECIOUS METALS 审中-公开
标题翻译：提取精细金属的方法
公开(公告)号：WO2007081243A2
公开(公告)日：2007-07-19
申请号：PCT/RU2007000004
申请日：2007-01-09
申请人： ZAKRYTOE AKCIONERNOE OBSHESTVO , SINEGRIBOV VIKTOR ANDREEVICH , SMETANNIKOV ANDREI FILIPPOVICH , UDINA TATYANA BORISOVNA , NOVIKOV PAVEL URIEVICH , LOGVINENKO IZABELLA ALEKSEEVNA , KRASNOSHTEIN ARKADIY EVGENIEVI
发明人： SINEGRIBOV VIKTOR ANDREEVICH , SMETANNIKOV ANDREI FILIPPOVICH , UDINA TATYANA BORISOVNA , NOVIKOV PAVEL URIEVICH , LOGVINENKO IZABELLA ALEKSEEVNA , KRASNOSHTEIN ARKADIY EVGENIEVI
IPC分类号： C22B11/00
CPC分类号： C22B11/04 , C22B1/08 , C22B3/065 , C22B3/24 , C22B11/042 , C22B11/06 , Y02P10/214 , Y02P10/234
摘要： The invention relates to methods for extracting precious metals and can be used for extracting precious metals (platinum, palladium, gold, etc) from different mineral raw materials containing alkali and alkali-earth metal chlorides, for example a bulk concentrate obtainable from clay-salt wastes (slims) of potassium production, marking clays, etc. The inventive method consists in carrying out the chloridising roasting of the bulk concentrate which is obtainable during the initial material (clay-salt slims) dressing and contains residual chlorides in a quantity raging from 7 to 13 % or a natural concentrate (marking clays) wherein the chloride content is equal to or less than 15 %, in leaching a roasted product by a nitromuriatic acid solution, in sorbing precious metals from a pulp, in carrying out the chloridising roasting of a mineral raw material with a temperature of 600-700 °C, in leaching said precious metals from the sintered product by the diluted nitromuriatic acid solution and in sorbing the precious metals from the thus obtained pulp. The inventive method makes it possible to carry out a combined extraction of platinum group metals, gold ad silver from the mineral raw material containing alkali and alkali-earth metal chlorides and to increase the cost effectiveness of the process by using a chlorinating agent contained therein, reducing the number of operations (eliminating a pulp filtration), reducing a roasting temperature in comparison with the prior art and by leaching precious metals from the sintered product by the diluted acid solution.
摘要翻译：本发明涉及用于提取贵金属的方法，可用于从含有碱金属和碱土金属氯化物的不同矿物原料中提取贵金属（铂，钯，金等），例如可从粘土盐钾生产的废物（薄片），标记粘土等。本发明的方法在于进行在初始材料（粘土盐薄片）敷料期间可获得的散装浓缩物的氯化焙烧，并且含有来自 7〜13％的天然浓缩物（标记粘土），其中氯化物含量等于或小于15％，在硝化酸溶液浸取焙烤产品时，从纸浆中吸附贵金属，进行氯化焙烧的温度为600-700℃的矿物原料，通过稀释的硝酸酸溶液a从烧结产物中浸出所述贵金属从这样获得的纸浆中吸收贵金属。本发明的方法使得可以从含有碱金属和碱土金属氯化物的矿物原料中进行铂族金属，金银的组合提取，并且通过使用其中所含的氯化剂来提高该方法的成本效益，减少操作次数（消除纸浆过滤），与现有技术相比降低焙烧温度，并通过稀释的酸溶液从烧结产品中浸出贵金属。

2. 发明申请

WO2005007898A3 METHOD FOR PROCESSING OXIDISES NICKEL-COBALT ORE (VARIANTS) 审中-公开
标题翻译：加工氧化物镍 - 钴矿的方法（变体）
公开(公告)号：WO2005007898A3
公开(公告)日：2005-05-19
申请号：PCT/RU2004000283
申请日：2004-07-22
申请人： OBSCHESTVO S OGRANICHENNOY OTV , BATSHEV VASILIY IVANOVICH , KALASHNIKOV ALEXEY VLADIMIROVI , KOLTSOV VASILIY YURIEVICH , MELNIK DMITRIY VIKTOROVICH , SINEGRIBOV VIKTOR ANDREEVICH , SHCHUKIN MIKHAIL IGOREVICH
发明人： BATSHEV VASILIY IVANOVICH , KALASHNIKOV ALEXEY VLADIMIROVI , KOLTSOV VASILIY YURIEVICH , MELNIK DMITRIY VIKTOROVICH , SINEGRIBOV VIKTOR ANDREEVICH , SHCHUKIN MIKHAIL IGOREVICH
IPC分类号： C22B1/02 , C22B1/06 , C22B23/00
CPC分类号： C22B1/02 , C22B1/06 , C22B23/043
摘要： The group of invention relates to methods for extracting nickel and cobalt from oxidises nickel-cobalt ores and makes it possible to increase a nickel extraction ratio. In the first variant, the inventive method for processing an oxidised nickel-cobalt ore consists in treating said ore with sulphuric acid associated with the transfer thereof to a soluble sulphate solution. The ore is granulated with sulphuric acid, the thus obtained granules are sulphated at a temperature of 250-450 DEG C during 1-2 hours in one or two operations. Afterwards, the water leaching of nickel sulphates and other metals is carried out, the metals being extracted from the solution by means of known methods. The first operation is carried out at a temperature of 250-300 DEG C, the second operation at a temperature of 350-450 DEG C, and the granules are sulphated with a stechiometric sulphuric acid consumption. In the second variant, the inventive method for processing the oxidised nickel-cobalt ore also consists in treating said ore with sulphuric acid associated with the transfer thereof to soluble sulphate solution. The ore is granulated with sulphuric acid in a required stechiometric quantity, the granules are calcined at a temperature ranging from 650 to 700 DEG C during 2.5-3.0 hours, afterwards the water leaching being carried out. The granule calcination is carried out until the content of soluble iron therein is attained a range of 1.0-3.9 %, said granules being sulphated at a temperature of 200-250 DEG C during 1 hour prior to the calcination thereof. In the third variant, the inventive method for processing the oxidised nickel-cobalt ore consists in treating said ore with sulphuric acid associated with the transfer thereof to a soluble sulphate solution. The ore is granulated with sulphuric acid, the granules are calcined in the atmosphere of gases produced during the oxidation of elementary sulphur or sulphides by air oxygen. Afterwards, said gases together with sulphur oxides released during the granule calcination are sent for sulphuric acid production and the granules for water leaching.
摘要翻译：本发明组涉及从氧化镍钴矿石中提取镍和钴的方法，并且可以提高镍提取率。在第一变体中，本发明的用于处理氧化的镍 - 钴矿石的方法包括用硫酸处理所述矿石并将其转移到可溶性硫酸盐溶液中。矿石用硫酸造粒，这样得到的颗粒在250-450℃的温度下硫酸化1-2小时，一次或两次操作。之后，进行硫酸镍和其它金属的水浸，通过已知方法从溶液中提取金属。第一种操作是在250-300℃的温度下进行的，第二种操作是在350-450℃的温度下进行的，并且使用硫酸化学计量法将颗粒硫酸化。在第二变体中，本发明的用于处理氧化镍钴矿的方法还包括用硫酸处理所述矿石，所述硫酸与其转移至可溶性硫酸盐溶液有关。用硫酸按要求的化学计量量将矿石制粒，在2.5-3.0小时期间将颗粒在650-700℃的温度下煅烧，然后进行水浸。进行颗粒煅烧直至其中可溶性铁的含量达到1.0-3.9％的范围，所述颗粒在煅烧前1小时在200-250℃的温度下硫酸化。在第三变体中，本发明的用于处理氧化镍钴矿石的方法包括用硫酸处理所述矿石，所述硫酸与将其转移到可溶性硫酸盐溶液中有关。将矿石用硫酸造粒，将颗粒在通过空气氧氧化元素硫或硫化物期间产生的气体的气氛中煅烧。之后，将所述气体与在颗粒煅烧过程中释放的硫氧化物一起送入硫酸生产，并将颗粒送入水浸出。

3. 发明申请

WO2005007898A8 METHOD FOR PROCESSING OXIDIZED NICKEL-COBALT ORE (VARIANTS) 审中-公开
标题翻译：氧化镍钴矿（VARIANTS）的处理方法
公开(公告)号：WO2005007898A8
公开(公告)日：2007-06-28
申请号：PCT/RU2004000283
申请日：2004-07-22
申请人： OBSCHESTVO S OGRANICHENNOY OTV , BATSHEV VASILIY IVANOVICH , KALASHNIKOV ALEXEY VLADIMIROVI , KOLTSOV VASILIY YURIEVICH , MELNIK DMITRIY VIKTOROVICH , SINEGRIBOV VIKTOR ANDREEVICH , SHCHUKIN MIKHAIL IGOREVICH
发明人： BATSHEV VASILIY IVANOVICH , KALASHNIKOV ALEXEY VLADIMIROVI , KOLTSOV VASILIY YURIEVICH , MELNIK DMITRIY VIKTOROVICH , SINEGRIBOV VIKTOR ANDREEVICH , SHCHUKIN MIKHAIL IGOREVICH
IPC分类号： C22B23/00 , C22B1/02 , C22B1/06
CPC分类号： C22B1/02 , C22B1/06 , C22B23/043
摘要： The group of invention relates to methods for extracting nickel and cobalt from oxidizes nickel-cobalt ores and makes it possible to increase a nickel extraction ratio. In the first variant, the inventive method for processing an oxidized nickel-cobalt ore consists in treating said ore with sulphuric acid associated with the transfer thereof to a soluble sulphate solution. The ore is granulated with sulphuric acid, the thus obtained granules are sulphated at a temperature of 250-450°C during 1-2 hours in one or two operations. Afterwards, the water leaching of nickel sulphates and other metals is carried out, the metals being extracted from the solution by means of known methods. The first operation is carried out at a temperature of 250-300°C, the second operation at a temperature of 350-450°C, and the granules are sulphated with a stechiometric sulphuric acid consumption. In the second variant, the inventive method for processing the oxidised nickel-cobalt ore also consists in treating said ore with sulphuric acid associated with the transfer thereof to soluble sulphate solution. The ore is granulated with sulphuric acid in a required stechiometric quantity, the granules are calcined at a temperature ranging from 650 to 700°C during 2.5-3.0 hours, afterwards the water leaching being carried out. The granule calcination is carried out until the content of soluble iron therein is attained a range of 1.0-3.9 %, said granules being sulphated at a temperature of 200-250°C during 1 hour prior to the calcination thereof. In the third variant, the inventive method for processing the oxidised nickel-cobalt ore consists in treating said ore with sulphuric acid associated with the transfer thereof to a soluble sulphate solution. The ore is granulated with sulphuric acid, the granules are calcined in the atmosphere of gases produced during the oxidation of elementary sulphur or sulphides by air oxygen. Afterwards, said gases together with sulphur oxides released during the granule calcination are sent for sulphuric acid production and the granules for water leaching.
摘要翻译：本发明涉及从镍 - 钴矿石氧化提取镍和钴的方法，并且可以提高镍提取率。在第一种变型中，用于处理氧化的镍钴矿石的本发明方法在于将硫酸转移至可溶性硫酸盐溶液来处理所述矿石。矿石用硫酸造粒，所得颗粒在一个或两个操作中在1-24小时内在250-450℃的温度下硫酸化。之后，进行硫酸镍等金属的浸出，通过已知的方法从溶液中提取金属。第一次操作在250-300℃的温度下进行，第二次操作在350-450℃的温度下进行，颗粒用硫酸消耗硫酸化。在第二种变型中，用于处理氧化的镍钴矿石的本发明方法还包括用与其转移到可溶性硫酸盐溶液相关的硫酸处理所述矿石。矿石用硫酸以所需的刻度量造粒，颗粒在650-300℃的温度下在2.5-3.0小时内煅烧，然后进行水浸。进行颗粒煅烧直到其中可溶性铁的含量达到1.0-3.9％的范围，所述颗粒在其煅烧之前1小时内在200-250℃的温度下硫酸化。在第三变型中，用于处理氧化的镍钴矿石的本发明方法在于将硫酸转移到可溶性硫酸盐溶液中来处理所述矿石。矿石用硫酸造粒，颗粒在通过空气氧氧化元素硫或硫化物时产生的气体气氛中煅烧。之后，将所述气体与在颗粒煅烧期间释放的硫氧化物一起送入硫酸生产，并将颗粒用于水浸。

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