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1. 发明申请

WO2013032976A1 HIGH FLOW LIQUID CRYSTALLINE POLYMER COMPOSITION 审中-公开
标题翻译：高流动性液晶聚合物组合物
公开(公告)号：WO2013032976A1
公开(公告)日：2013-03-07
申请号：PCT/US2012/052439
申请日：2012-08-27
申请人： TICONA LLC , NAIR, Kamlesh P. , GRENCI, Joseph J. , GRAY, Steven D.
发明人： NAIR, Kamlesh P. , GRENCI, Joseph J. , GRAY, Steven D.
IPC分类号： C09K19/22 , C09K19/30 , C09K19/32 , C09K19/34 , C09K19/38 , C09K19/48
CPC分类号： C09K19/22 , C08L77/12 , C09K19/3086 , C09K19/322 , C09K19/3444 , C09K19/3809 , C09K19/48 , C09K2019/0481
摘要： A liquid crystalline polymer composition that contains a liquid crystalline polymer and an aromatic amide oligomer is provided. The oligomer can serve as a flow aid by altering intermolecular polymer chain interactions, thereby lowering the overall viscosity of the polymer matrix under shear. The oligomer is also not easily volatized or decomposed during compounding, molding, and/or use, which minimizes off-gassing and the formation of blisters that would otherwise impact the final mechanical properties of a part made from the polymer composition. While providing the benefits noted, the aromatic amide oligomer does not generally react with the polymer backbone of the liquid crystalline polymer to any appreciable extent so that the mechanical properties of the polymer are not adversely impacted.
摘要翻译：提供了包含液晶聚合物和芳族酰胺低聚物的液晶聚合物组合物。该低聚物可以通过改变分子间聚合物链相互作用而起流动助剂的作用，从而降低剪切下聚合物基质的总体粘度。低聚物在配混，成型和/或使用过程中也不容易挥发或分解，这最大限度地减少了废气和泡罩的形成，否则这些泡罩会影响由聚合物组合物制成的部件的最终机械性能。虽然提供了所提到的益处，但芳族酰胺低聚物通常不会与液晶聚合物的聚合物骨架发生任何明显程度的反应，从而不会不利地影响聚合物的机械性能。

2. 发明申请

WO2013032974A1 SOLID-STATE POLYMERIZATION OF A LIQUID CRYSTALLINE POLYMER 审中-公开
标题翻译：液晶聚合物的固态聚合
公开(公告)号：WO2013032974A1
公开(公告)日：2013-03-07
申请号：PCT/US2012/052437
申请日：2012-08-27
申请人： TICONA LLC , NAIR, Kamlesh P. , GRAY, Steven D.
发明人： NAIR, Kamlesh P. , GRAY, Steven D.
IPC分类号： C08K5/20 , C09K19/22 , C09K19/30 , C09K19/32 , C09K19/34 , C09K19/48
CPC分类号： C09K19/22 , C08K5/20 , C09K19/3086 , C09K19/322 , C09K19/3444 , C09K19/48 , C09K2019/0481
摘要： A method for forming a high molecular weight thermotropic liquid crystalline polymer is provided. The method includes melt polymerizing two or more monomers in the presence of a unique aromatic amide oligomer to form a prepolymer, and then solid-state polymerizing the prepolymer to achieve a target molecular weight. The present inventors have discovered that a unique aromatic amide oligomer can be employed to help increase the "low shear" complex viscosity of the resulting solid-state polymerized composition. This allows for the attainment of higher than conventional "low shear" complex viscosity values and/or a substantial reduction in the solid-state polymerization time needed to achieve a target complex viscosity. In addition, the oligomeric flow aid can also accelerate the extent to which the "high shear" melt viscosity is increased during solid-state polymerization, which may also contribute to a substantial reduction in the solid-state polymerization time needed to achieve a certain molecular weight.
摘要翻译：提供了形成高分子量热致液晶聚合物的方法。该方法包括在独特的芳族酰胺低聚物存在下熔融聚合两种或更多种单体以形成预聚物，然后使预聚物固相聚合以达到目标分子量。本发明人已经发现，可以使用独特的芳族酰胺低聚物来帮助提高所得固态聚合组合物的“低剪切”复数粘度。这允许达到高于常规“低剪切”复数粘度值和/或实现目标复合物粘度所需的固态聚合时间的显着降低。此外，低聚流动助剂还可以加速在固态聚合期间“高剪切”熔体粘度增加的程度，这也可能导致实现某种分子所需的固态聚合时间的显着降低重量。

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