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1. 发明申请

WO2007024227A1 INORGANIC POLYMERS AND USE OF INORGANIC POLYMERS FOR DETECTING NITROAROMATIC COMPOUNDS 审中-公开
标题翻译：无机聚合物和无机聚合物用于检测硝基化合物的用途
公开(公告)号：WO2007024227A1
公开(公告)日：2007-03-01
申请号：PCT/US2005/030381
申请日：2005-08-25
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , URBAS, Sarah , TOAL, Sarah, J. , SANCHEZ, Jason
发明人： TROGLER, William, C. , URBAS, Sarah , TOAL, Sarah, J. , SANCHEZ, Jason
IPC分类号： G01N21/76 , B32B5/02 , C07F5/00
CPC分类号： C07F7/30 , G01N21/77 , G01N2021/6432 , G01N2021/7786
摘要： A method for detecting an analyze that may be present in ambient air, bound to a surface or as part of complex aqueous media that includes providing a metallole-containing polymer or copolymer, exposing the polymer or copolymer to a suspected analyze or a system suspected of including the analyze, and measuring a quenching of photoluminescence of the metallole-containing polymer or copolymer exposed to the system. Also included is a solid state inorganic-organic polymer sensor for detecting nitroaromatic compounds that includes a substrate and a thin film of a metallole-containing polymer or copolymer deposited on said substrate.
摘要翻译：用于检测可能存在于环境空气中，结合到表面或作为复合水性介质的一部分的分析的方法，所述复合水性介质包括提供含金属的聚合物或共聚物，将所述聚合物或共聚物暴露于怀疑分析物或涉嫌包括分析和测量暴露于该体系的含金属醇的聚合物或共聚物的光致发光的淬灭。还包括用于检测硝基芳族化合物的固态无机 - 有机聚合物传感器，其包括基材和沉积在所述基材上的含金属的聚合物或共聚物的薄膜。

2. 发明申请

WO2004058841A2 SYNTHESIS AND USE OF INORGANIC POLYMER SENSOR FOR DETECTING NITROAROMATIC COMPOUNDS 审中-公开
标题翻译：无机聚合物传感器用于检测硝基化合物的合成和使用
公开(公告)号：WO2004058841A2
公开(公告)日：2004-07-15
申请号：PCT/US2003/031600
申请日：2003-10-06
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , SAILOR, Michael, J. , TROGLER, William, C. , SOHN, Honglae , TOAL, Sarah, J.
发明人： SAILOR, Michael, J. , TROGLER, William, C. , SOHN, Honglae , TOAL, Sarah, J.
IPC分类号： C08G
CPC分类号： C08G79/00 , C07F7/0896 , C07F7/30 , C08G77/60 , G01N21/643 , G01N33/0049 , G01N2021/6432 , G01N2021/7786
摘要： A dehydrocoupling polycondensation method for synthesizing polymetalloles including obtaining a dihydrometallole that includes silicon or germanium atoms, designating a reducing agent for preparation of dihydrometallole monomer, measuring a predetermined molar percentage of the reducing agent corresponding to a molar amount of the dihydrometallole, selecting a catalyst, and reacting the catalyst with the dihydrometallole to obtain a polymetallole. A method for detecting an analyte that may be present in ambient air or complex aqueous media including providing a polymer or copolymer containing a metalloid-metalloid backbone, exposing the polymer or copolymer to a suspected analyte or a system suspected of including the analyte, and measuring a quenching of photoluminescence of the metallole polymer or copolymer exposed to the system.
摘要翻译：一种用于合成多元醇的脱氢缩合缩聚方法，包括获得包含硅或锗原子的二羟基醇，指定用于制备二羟基醇单体的还原剂，测量对应于二羟基醇的摩尔量的预定摩尔百分数的还原剂，选择催化剂，并使催化剂与二水合醇反应以获得多元醇。用于检测可能存在于环境空气或复合水性介质中的分析物的方法，包括提供含有准金属 - 准金属主链的聚合物或共聚物，将聚合物或共聚物暴露于可疑分析物或怀疑包含分析物的体系，并测量暴露于体系的金属聚合物或共聚物的光致发光的淬灭。

3. 发明申请

WO2009011806A2 FLUORESCENCE DETECTION OF NITROGEN-CONTAINING EXPLOSIVES AND BLUE ORGANIC LED 审中-公开
标题翻译：含氮炸药和蓝色有机发光二极管的荧光检测
公开(公告)号：WO2009011806A2
公开(公告)日：2009-01-22
申请号：PCT/US2008/008553
申请日：2008-07-10
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , SANCHEZ, Jason
发明人： TROGLER, William, C. , SANCHEZ, Jason
IPC分类号： G01N23/04 , C08F12/02 , H05B33/14
CPC分类号： C09K11/06 , C09K2211/1491
摘要： The invention provides a sensor for detecting nitrogen containing high explosives. The sensor includes a substrate and a blue-photoluminescent metallofluorene copolymer to be carried on said substrate during testing for nitrogen containing high explosives. The copolymer is preferably a blue- photoluminescent metallofluorene copolymer, and preferably is a vinyl bridged silafluorene copolymer. A method for detecting nitrogen containing high explosives involves exposing a copolymer to an analyte, preferably by spraying the copolymer or otherwise coating the substrate after it has been exposed to analyte and then exciting the copolymer to luminesce. The copolymer is observed for fluorescence quenching, which can be through human or electronic observation. The invention also provides for synthesis of a vinyl bridged silafluorene polymer by providing diethynylmetallofluorene and dihydrosilafluorene as precursors and conducting catalytic hydrosilation of the precursors. In a blue emitting organic light emitting diode of the invention, an emitting layer is blue-photoluminescent metallofluorene copolymer.
摘要翻译：本发明提供了一种用于检测含氮高爆炸药的传感器。该传感器包括衬底和在测试含氮高爆炸物时在所述衬底上携带的蓝光致发光金属芴共聚物。该共聚物优选为蓝光致发光金属芴共聚物，并且优选为乙烯基桥联的硅杂芴共聚物。用于检测含氮高爆炸药的方法涉及将共聚物暴露于分析物，优选通过喷雾共聚物或以其他方式涂覆衬底，之后将衬底暴露于分析物，然后激发共聚物发光。观察共聚物的荧光猝灭，其可以通过人或电子观察。本发明还提供了通过提供二乙炔基金属芴和二氢硅烷芴作为前体并且进行前体的催化氢化硅烷化来合成乙烯基桥联的硅杂芴聚合物。在本发明的蓝色发光有机发光二极管中，发光层是蓝光发光的金属芴共聚物。

4. 发明申请

WO2008005096A2 DETECTION OF NITRO-AND NITRATE-CONTAINING COMPOUNDS 审中-公开
标题翻译：含有硝酸和硝酸的化合物的检测
公开(公告)号：WO2008005096A2
公开(公告)日：2008-01-10
申请号：PCT/US2007/010583
申请日：2007-05-01
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , SANCHEZ, Jason , TOAL, Sarah , WANG, Zheng , DUGAN, Regina, E.
发明人： TROGLER, William, C. , SANCHEZ, Jason , TOAL, Sarah , WANG, Zheng , DUGAN, Regina, E.
CPC分类号： G01N21/6428 , G01N21/77 , G01N2021/7786 , Y10T436/17 , Y10T436/173076 , Y10T436/173845
摘要： A method of the invention is a method of detecting nitramines and nitrate esters believed to be present on a sampling substrate. In the method, a sampling substrate is exposed to a first reagent that is formulated to react with nitramine- and nitrate ester-type explosives to release nitrite. The sampling substrate is then exposed to a second reagent that contains an acid to react with the nitrite and a diaminoaromatic. present in either the first or second reagent, to form a triazole that will luminesce. Another method of the invention combines this process for nitramine- and nitrate ester-based explosives detection with a technique to detect nitroaromatic-based explosives using luminescent polymers, for a three-step process for the detection of explosives in these three classes.
摘要翻译：本发明的方法是检测被认为存在于采样基质上的硝胺和硝酸酯的方法。在该方法中，将采样衬底暴露于配制成与硝胺和硝酸酯型炸药反应以释放亚硝酸盐的第一试剂。然后将采样衬底暴露于含有酸的第二试剂，以与亚硝酸盐和二氨基芳族化合物反应。存在于第一或第二试剂中，以形成将发光的三唑。本发明的另一种方法将用硝酸和硝酸酯类爆炸物检测的方法与使用发光聚合物检测基于硝基芳族化合物的爆炸物的技术结合，用于在这三类中检测爆炸物的三步法。

5. 发明申请

WO2008140635A3 FLUORESCENCE DETECTION OF NITROGEN-CONTAINING EXPLOSIVES AND BLUE ORGANIC LED 审中-公开
公开(公告)号：WO2008140635A3
公开(公告)日：2008-11-20
申请号：PCT/US2008/001193
申请日：2008-01-29
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , SANCHEZ, Jason
发明人： TROGLER, William, C. , SANCHEZ, Jason
IPC分类号： G01N23/222 , H05B33/14
摘要： The invention provides a sensor for detecting nitrogen containing high explosives. The sensor includes a substrate and a blue-photoluminescent metallofluorene copolymer to be carried on said substrate during testing for nitrogen containing high explosives. The copolymer is preferably a blue- photoluminescent metallofluorene copolymer, and preferably is a vinyl bridged silafluorene copolymer. A method for detecting nitrogen containing high explosives involves exposing a copolymer to an analyte, preferably by spraying the copolymer or otherwise coating the substrate after it has been exposed to analyte and then exciting the copolymer to luminesce. The copolymer is observed for fluorescence quenching, which can be through human or electronic observation. The invention also provides for synthesis of a vinyl bridged silafluorene polymer by providing diethynylmetallofluorene and dihydrosilafluorene as precursors and conducting catalytic hydrosilation of the precursors. In a blue emitting organic light emitting diode of the invention, an emitting layer is blue-photoluminescent metallofluorene copolymer.

6. 发明申请

WO2009023697A2 HOLLOW SILICA NANOSPHERES AND METHODS OF MAKING SAME 审中-公开
标题翻译：空心二氧化硅纳米球及其制备方法
公开(公告)号：WO2009023697A2
公开(公告)日：2009-02-19
申请号：PCT/US2008/072972
申请日：2008-08-13
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , ESENER, Sadik, C. , MESSMER, Davorka , LIND, Johan, Ulrik , POHAKU, Kristina , YANG, Jian
发明人： TROGLER, William, C. , ESENER, Sadik, C. , MESSMER, Davorka , LIND, Johan, Ulrik , POHAKU, Kristina , YANG, Jian
IPC分类号： C01B33/12 , B82B3/00 , A61K9/51
CPC分类号： A61K47/6923 , A61K9/0019 , A61K9/14 , A61K9/1611 , A61K9/2009 , A61K9/5115 , A61K9/5192 , A61K39/0011 , A61K47/59 , A61K47/6455 , A61K47/6925 , A61K48/0041 , A61K49/04 , A61K49/183 , A61K2039/53 , A61K2039/6093 , B82Y5/00 , C01B33/12 , C01B33/18 , C12N15/87 , Y10S977/773 , Y10T428/2982
摘要： The disclosure provide hollow nanospheres and methods of making and using the same. The methods and compositions of the disclosure are useful for drug delivery and gene transfer.
摘要翻译：本公开提供了中空纳米球及其制备和使用方法。本公开的方法和组合物可用于药物递送和基因转移。

7. 发明申请

WO2009017631A3 PEROXIDE CHEMICAL SENSOR AND SENSING METHOD 审中-公开
公开(公告)号：WO2009017631A3
公开(公告)日：2009-02-05
申请号：PCT/US2008/008916
申请日：2008-07-23
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , TROGLER, William, C. , BOHRER, Forest , KUMMEL, Andrew, C.
发明人： TROGLER, William, C. , BOHRER, Forest , KUMMEL, Andrew, C.
IPC分类号： G01N27/26 , G01N27/327
摘要： Sensors, sensing systems and sensing methods of the invention provide for detection of peroxides, including for example, vapor-phase H 2 O 2 and organic peroxides such as di-tert-buty\ peroxide. A sensor and sensing method of the invention uses at least two phthalocyanines, one of which exhibits an oxidation reaction with peroxides and the other of which exhibits a reduction reaction with peroxides. A peroxide is readily identified by a sensor of the invention when one of the at least two phthalocyanines exhibits increased resistance to current flow and the other of the at least two phthalocyanines exhibits decreased resistance to current flow.

8. 发明申请

WO2008147497A2 ULTRA-THIN ORGANIC TFT CHEMICAL SENSOR, MAKING THEREOF, AND SENSING METHOD 审中-公开
标题翻译：超薄有机TFT化学传感器及其制造方法及传感方法
公开(公告)号：WO2008147497A2
公开(公告)日：2008-12-04
申请号：PCT/US2008/005743
申请日：2008-05-05
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA , KUMMEL, Andrew, C. , YANG, Dengliang , TROGLER, William, C. , GREDIG, Thomas
发明人： KUMMEL, Andrew, C. , YANG, Dengliang , TROGLER, William, C. , GREDIG, Thomas
IPC分类号： G01N27/30 , G01N27/41 , H01L29/78
CPC分类号： G01N27/4141 , G01N33/0057 , H01L51/0545
摘要： An embodiment of the invention is an organic thin film transistor chemical sensor. The sensor includes a substrate. A gate electrode is isolated from drain and source electrodes by gate dielectric. An organic ultra-thin semiconductor thin film is arranged with respect to the gate, source and drain electrodes to act as a conduction channel in response to appropriate gate, source and drain potentials. The organic ultra-thin film is permeable to a chemical analyte of interest and consists of one or a few atomic or molecular monolayers of material. An example sensor array system includes a plurality of sensors of the invention. In a preferred embodiment, a sensor chip having a plurality of sensors is mounted in a socket, for example by wire bonding. The socket provides thermal and electrical interference isolation for the sensor chip from associated sensing circuitry that is mounted on a common substrate, such as a PCB (printed circuit board). A method of operating an organic thin film transistor chemical sensor exposes the sensor to a suspected analyte. A low duty cycle voltage pulse train is applied to the gate electrode to reduce baseline drift while sensing for a conduction channel change.
摘要翻译：本发明的一个实施例是有机薄膜晶体管化学传感器。传感器包括基板。栅极通过栅极电介质与漏极和源极隔离。相对于栅极，源极和漏极布置有机超薄半导体薄膜，以响应于适当的栅极，源极和漏极电位而用作导电沟道。有机超薄膜对目的化学分析物是可渗透的，由一种或几种原子或分子单层的材料组成。示例性传感器阵列系统包括本发明的多个传感器。在优选实施例中，具有多个传感器的传感器芯片例如通过引线接合安装在插座中。该插座为传感器芯片提供热和电干扰隔离，该隔离装置与安装在公共基板（例如PCB（印刷电路板））上的相关感测电路相连。操作有机薄膜晶体管化学传感器的方法将传感器暴露于可疑分析物。一个低占空比电压脉冲串施加到栅电极，以减少基线漂移，同时检测导通通道的变化。

9. 发明申请

WO2010044920A1 DETECTION OF EXPLOSIVES THROUGH LUMINESCENCE 审中-公开
标题翻译：通过发光检测爆炸物
公开(公告)号：WO2010044920A1
公开(公告)日：2010-04-22
申请号：PCT/US2009/045930
申请日：2009-06-02
申请人： REDXDEFENSE, LLC , MILLER, Dale, R. , TOAL, Sarah, J. , WATSON, Russell, P. , TROGLER, William, C.
发明人： MILLER, Dale, R. , TOAL, Sarah, J. , WATSON, Russell, P. , TROGLER, William, C.
IPC分类号： G01N21/00
CPC分类号： G01N21/643 , G01N21/6428 , G01N31/22 , G01N2021/6432 , Y10T436/13 , Y10T436/173076 , Y10T436/173845
摘要： A method of simultaneously detecting peroxide and nitrogen-based explosives includes the steps of applying a conversion reagent to a sample, the conversion reagent oxidizing in the presence of peroxide and inorganic nitrate explosives; applying a test reagent including a luminescent compound to the sample; exciting the luminescent compound with ultraviolet light; and simultaneously determining the presence of one or more explosives based on quenching, brightening or a shift in wavelength of the luminescence over time. Explosives may also be detected based on color changes of the sample. Optionally, phase transfer reagents, catalysts, colorimetric agents and zinc dust may be added to improve detection of explosives. Alternatively, an assay-type method may be utilized wherein a sample is added to the conversion and/or test reagents and the reagent is spotted on a substrate before exposure to ultraviolet light.
摘要翻译：同时检测过氧化物和氮基爆炸物的方法包括以下步骤：将转化试剂施用于样品，转化试剂在过氧化物和无机硝酸盐炸药存在下氧化; 将样品中含有发光性化合物的试剂涂布于样品中; 用紫外线激发发光化合物; 并且同时确定基于随着时间的发光的猝灭，增亮或波长的偏移的一种或多种爆炸物的存在。也可以根据样品的颜色变化来检测爆炸物。任选地，可以加入相转移试剂，催化剂，比色剂和锌粉以改善爆炸物的检测。或者，可以使用测定型方法，其中将样品加入到转化和/或测试试剂中，并且在暴露于紫外光之前将试剂点样在基底上。

10. 发明申请

WO2016149711A1 SILICA NANOSTRUCTURES, LARGE-SCALE FABRICATION METHODS, AND APPLICATIONS THEREOF 审中-公开
标题翻译：二氧化硅纳米结构，大规模制造方法及其应用
公开(公告)号：WO2016149711A1
公开(公告)日：2016-09-22
申请号：PCT/US2016/023492
申请日：2016-03-21
申请人： THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
发明人： KUMMEL, Andrew, C. , LIBERMAN, Alexander , VIVEROS, Robert , TROGLER, William, C.
IPC分类号： C01B33/16 , B82B1/00 , B82Y5/00
CPC分类号： C01B33/16 , A61K49/1824 , B82B1/00 , B82Y15/00 , B82Y40/00 , C01B33/027 , C01B33/146 , H01G4/08
摘要： Methods, systems, and devices are disclosed for fabricating and utilizing nanoscale material structures such as nanoflakes and nanoshells.
摘要翻译：公开了用于制造和利用纳米级材料结构例如纳米片和纳米壳的方法，系统和装置。

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