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1. 发明申请

WO2006060602A2 PARTICLE SIZE CONTROL FOR ACETYLENIC AGENTS USEFUL IN CONDITION MONITORING SYSTEMS 审中-公开
标题翻译：在条件监测系统中有用的乙酰化剂的颗粒尺寸控制
公开(公告)号：WO2006060602A2
公开(公告)日：2006-06-08
申请号：PCT/US2005/043520
申请日：2005-12-01
申请人： TEMPTIME CORPORATION , PRUSIK, Thaddeus , SMITH, Dawn , LEUBNER, Ingo
发明人： PRUSIK, Thaddeus , SMITH, Dawn , LEUBNER, Ingo
IPC分类号： C07C273/16
CPC分类号： C07C273/189 , C07C275/20
摘要： Precipitation of polyacetylenic agents can be effected with control of a particle size parameter such as mean size or spread, by mixing a warm solution of the acetylenic agent with a cold precipitation fluid and appropriate selection of a constituent of the cold precipitation fluid and/or of the temperature conditions and collecting the precipitated acetylenic agent. Precipitation additives such as nitrocellulose or gelatin can usefully be employed. Solvents such as aqueous methanol and ethyl 3-ethoxypropionate can be useful. Polyacetylenic agents, e.g. substituted diacetylenics are useful to provide visual changes in condition-monitoring indicators such as time-temperature indicators, "TTIs", useful as freshness indicators for radiation exposure monitoring and for other purposes. Controlled, small and/or consistent particle sizes of such polyacetylenic agents are helpful in providing consistent commercial properties, especially in inks in which they may be formulated.
摘要翻译：通过将炔属试剂的温溶液与冷沉淀流体混合并适当选择冷沉淀液和/或冷沉淀液的组分，可以通过控制粒径参数如平均尺寸或扩展来实现聚乙炔化剂的沉淀温度条件并收集沉淀的炔属剂。可以有效地使用沉淀添加剂如硝酸纤维素或明胶。溶剂如甲醇水溶液和3-乙氧基丙酸乙酯是有用的。聚乙炔化剂，例如取代的二乙酰基可用于提供条件监测指标的视觉变化，例如时间 - 温度指标“TTI”，作为辐射暴露监测的新鲜度指标和用于其他目的。这种聚乙炔化剂的受控的，小的和/或一致的粒度有助于提供一致的商业性质，特别是在它们可以配制的油墨中。

2. 发明申请

WO2010114752A1 CO-CRYSTALLIZABLE DIACETYLENIC MONOMER COMPOSITIONS, CRYSTAL PHASES AND MIXTURES, AND RELATED METHODS 审中-公开
标题翻译：可结晶的二乙烯单体组合物，晶体相和混合物及相关方法
公开(公告)号：WO2010114752A1
公开(公告)日：2010-10-07
申请号：PCT/US2010/028500
申请日：2010-03-24
申请人： TEMPTIME CORPORATION , CASTILLO MARTINEZ, Elizabeth , BAUGHMAN, Ray, H. , HALL, Lee, J. , KOZLOV, Mikhail , SMITH, Dawn, E. , PRUSIK, Thaddeus , LENTZ, Carl, M.
发明人： CASTILLO MARTINEZ, Elizabeth , BAUGHMAN, Ray, H. , HALL, Lee, J. , KOZLOV, Mikhail , SMITH, Dawn, E. , PRUSIK, Thaddeus , LENTZ, Carl, M.
IPC分类号： C08G18/10
CPC分类号： C07C275/20 , C08F238/02 , G01N31/229
摘要： Solid polymerizable diacetylenic monomer compositions, including compositions co-crystallized from a diversity of solvent systems under diverse cooling conditions, can exhibit diffraction patterns associated with the color development reactivities of the compositions. High reactivity compositions are disclosed and high reactivity and low reactivity phases can be identified. A low angle powder X-ray diffraction peak can indicate the presence of one or more crystal phases in a composition. A fingerprint region can exhibit fingerprint patterns of diffraction peaks associated with different reactivities. Information about polymerization of the diacetylenic monomers is disclosed using 13C nuclear magnetic resonance ("NMR") characterization. Diacetylenic monomer compositions useful in ambient condition indicators, for example time-temperature indicators are disclosed.
摘要翻译：固体可聚合二炔单体组合物，包括在不同冷却条件下从多种溶剂体系共结晶的组合物可以显示与组合物的显色反应性相关的衍射图。公开了高反应性组合物，并且可以鉴定出高反应性和低反应性相。低角度粉末X射线衍射峰可以指示组合物中存在一个或多个结晶相。指纹区域可以显示与不同反应性相关的衍射峰的指纹图谱。使用13C核磁共振（“NMR”）表征公开了关于二乙炔单体的聚合的信息。公开了用于环境条件指示剂的二乙炔单体组合物，例如时间 - 温度指示剂。

3. 发明申请

WO2008002833A2 ADJUVANT-MEDIATED REACTIVITY ENHANCEMENT OF POLYMERIZABLE POLYACETYLENIC MATERIALS 审中-公开
标题翻译：可聚合聚乙烯材料的添加剂介导的反应活性增强
公开(公告)号：WO2008002833A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/071868
申请日：2007-06-22
申请人： TEMPTIME CORPORATION , PRUSIK, Thaddeus , SMITH, Dawn , BAUGHMAN, Ray, H.
发明人： PRUSIK, Thaddeus , SMITH, Dawn , BAUGHMAN, Ray, H.
IPC分类号： C09D11/00
CPC分类号： C09D11/50
摘要： Indicator inks, indicators formed by printing or otherwise utilizing the inks and host products utilizing the indicators are disclosed. Reactivity-enhancing adjuvants stimulate enhanced thermal reactivity of diacetylenic or other indicator agents capable of responding to ambient thermal conditions with a visual change signaling an end point. The diacetylenic or other agents may be sensitive or relatively insensitive to ambient temperatures. Use of a reactivity-enhancing adjuvant provides a useful means for adapting the reactivities of indicator agents to the response characteristics of prospective host products, for example perishables such as vaccines or fresh fish and maturables such as fruit, cheese and wine. Some exemplary adjuvants include low- temperature polymerization initiators, for example methyl ethyl ketone peroxide and polymerization accelerators, for example cobalt compounds. Such initiators and accelerators can also be used in combination.
摘要翻译：公开了指示剂油墨，通过使用指示剂印刷或以其它方式利用油墨和主体产品形成的指示剂。反应性增强佐剂刺激能够响应于环境热条件的二乙炔或其他指示剂的增强的热反应性，其中以指示终点的视觉改变。二乙炔或其它试剂可能对环境温度敏感或相对不敏感。使用反应性增强佐剂提供了一种有用的方法，用于使指示剂的反应性适应于预期宿主产物的反应特性，例如易腐食物例如疫苗或鲜鱼以及可食用如水果，奶酪和葡萄酒。一些示例性的助剂包括低温聚合引发剂，例如甲基乙基酮过氧化物和聚合促进剂，例如钴化合物。这样的引发剂和促进剂也可以组合使用。

4. 发明申请

WO2007056727A2 FREEZE INDICATORS SUITABLE FOR MASS PRODUCTION 审中-公开
标题翻译：冷冻指示剂适用于大量生产
公开(公告)号：WO2007056727A2
公开(公告)日：2007-05-18
申请号：PCT/US2006/060613
申请日：2006-11-07
申请人： TEMPTIME CORPORATION , TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn
发明人： TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn
IPC分类号： G01K1/02
CPC分类号： G01K1/02 , G01K3/005 , G01K11/06 , G01K11/12 , G01K2207/04 , Y10S252/962
摘要： A freeze indicator employs, as active indicator element, dispersion of solid particles in a liquid medium which can be water or aqueous and which coagulates to provide an irreversible appearance change when subject to freezing. The liquid dispersion can be contained in an indicator volume around which extends a vapor block layer. The vapor block layer can prevent loss of liquid vapor from the dispersion and consequent drying out and dysfunctionality of the freeze indicator. For containing an aqueous medium, bilayer and trilayer laminate materials can be used which have a low water vapor transmission rate. The active indicator element can be a dilute colloidal dispersion of a metal such as gold or silver or other inorganic pigment material in water or an aqueous medium. Some embodiments avoid use of dispersants and the like and employ an active indicator element consisting of inorganic pigment particles, water and optionally an ice nucleating agent. Heavy water, or deuterated water can be components of the water, if desired.
摘要翻译：冷冻指示器使用固体颗粒在液体介质中的分散体作为活性指示剂元素，液体介质可以是水或水，并在凝固时提供不可逆的外观变化。液体分散体可以包含在延伸蒸气阻挡层的指示体积中。蒸气阻挡层可以防止液体蒸气从分散体中的损失，从而导致冷冻指示器的干燥和功能失调。为了含有水性介质，可以使用具有低水蒸汽透过率的双层和三层层压材料。活性指示剂元素可以是诸如金或银之类的金属或其它无机颜料材料在水或水介质中的稀释胶体分散体。一些实施方案避免使用分散剂等并且使用由无机颜料颗粒，水和任选的冰核成核剂组成的活性指示剂元件。如果需要，重水或氘代水可以是水的组分。

5. 发明申请

WO2009059035A1 CRYSTALLIZED DIACETYLENIC INDICATOR COMPOUNDS AND METHODS OF PREPARING THE COMPOUNDS 审中-公开
标题翻译：结晶二乙酸指示剂化合物及其制备方法
公开(公告)号：WO2009059035A1
公开(公告)日：2009-05-07
申请号：PCT/US2008/081835
申请日：2008-10-30
申请人： TEMPTIME CORPORATION , BAUGHMAN, Ray, H. , HALL, Lee, J. , KOZLOV, Mikhail , SMITH, Dawn, E. , PRUSIK, Thaddeus
发明人： BAUGHMAN, Ray, H. , HALL, Lee, J. , KOZLOV, Mikhail , SMITH, Dawn, E. , PRUSIK, Thaddeus
IPC分类号： C07C7/14
CPC分类号： G01K11/12 , C07C273/02 , C07C275/20 , C09B69/10 , G01K3/04 , G01N21/78 , G01N31/22 , G01N31/229
摘要： Crystallized diacetylenic compounds having certain crystallographic and other characteristics; diacetylenic compounds and mixtures crystallized from diacetylenic solutions; methods of preparing and identifying solvent systems for dissolving diacetylenic compounds; diacetylenic solutions; methods of recrystallizing diacetylenic compounds; crystals of 2,4-hexadiyn-1,6- bis(alkylurea) compounds; and ambient condition indicators and time-temperature condition indicators comprising crystallized diacetylenic compounds.
摘要翻译：具有某些晶体学特性的结晶二炔化合物; 二乙炔化合物和从二乙炔溶液中结晶的混合物; 制备和鉴定溶解二乙炔化合物的溶剂体系的方法; 二乙酰溶液; 二乙炔化合物重结晶方法; 2,4-己二炔-1,6-双（烷基脲）化合物的晶体; 环境条件指标和包含结晶二乙炔化合物的时间 - 温度条件指标。

6. 发明申请

WO2007056752A2 COMBINATION FREEZE INDICATORS 审中-公开
标题翻译：组合冻结指示器
公开(公告)号：WO2007056752A2
公开(公告)日：2007-05-18
申请号：PCT/US2006/060681
申请日：2006-11-08
申请人： TEMPTIME CORPORATION , TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn
发明人： TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn
IPC分类号： G01K1/02
CPC分类号： G01K3/04 , G01K3/005 , G01K2207/04
摘要： A combination temperature exposure indicator suitable for attachment to, or association with, a host product has a substrate, a freeze indicator supported by the substrate and a cumulative ambient time-temperature indicator also supported by the substrate. The freeze indicator can provide a visual indication of exposure of the freeze indicator to a freezing or near- freezing temperature and the cumulative time-temperature indicator can provide a visual indication of exposure of the cumulative time-temperature indicator to a predetermined cumulative time-temperature value. Also disclosed are: a combination freeze indicator and threshold temperature indicator; a combination threshold indicator and cumulative temperature indicator; and three-way combination indicators that can provide indications of cumulative past temperature exposure, exposure to freezing temperatures and exposure to a temperature above a threshold.
摘要翻译：组合温度曝光指示剂适于附着于主体产品或与主产品相关联，具有底物，由基底支撑的结冰指示剂和也由基底支持的累积环境时间温度指示剂。冷冻指示器可以提供冷冻指示器暴露于冷冻或接近冷冻温度的可视指示，并且累积时间 - 温度指示器可以提供累积时间 - 温度指示器暴露于预定累积时间温度的视觉指示值。还公开了：组合冻结指示器和阈值温度指示器; 组合阈值指标和累积温度指标; 和三路组合指示器，可以提供累积过去的温度暴露，暴露于冷冻温度和暴露于高于阈值的温度的指示。

7. 发明申请

WO2008027814A3 COLOR-RETAINING EXCESS-TEMPERATURE EXPOSURE INDICATOR 审中-公开
公开(公告)号：WO2008027814A3
公开(公告)日：2008-03-06
申请号：PCT/US2007/076844
申请日：2007-08-27
申请人： TEMPTIME CORPORATION , ABBASSI, Omar , PRUSIK, Thaddeus , SMITH, Dawn, E.
发明人： ABBASSI, Omar , PRUSIK, Thaddeus , SMITH, Dawn, E.
IPC分类号： G01K11/00
摘要： An excess temperature indicator can provide a visual indication of past exposure of perishable, maturing and other host products to an elevated temperature exceeding a threshold temperature. The indicator can have an upper layer provided with a viewing window and a wick attached to the upper layer. A reservoir of heat- fusible indicator material can be disposed in contact with the wick, to fuse and move along the wick changing the visual appearance of a first portion of the wick viewable through the window, in response to an excess temperature event. Also, the indicator can have a region of fused upper layer material attaching the wick to the upper layer. Optionally, a window seal can extend around the viewing window to prevent migration of the indicator material. The indicator can be employed to monitor vaccines, foods and other products providing an enduring visual signal of exposure to potentially damaging temperature conditions.

8. 发明申请

WO2008144348A1 FREEZE INDICATORS, FLEXIBLE FREEZE INDICATORS AND MANUFACTURING METHODS 审中-公开
标题翻译：冷冻指示器，灵活冻结指示器和制造方法
公开(公告)号：WO2008144348A1
公开(公告)日：2008-11-27
申请号：PCT/US2008/063629
申请日：2008-05-15
申请人： TEMPTIME CORPORATION , TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn, E. , BAUGHMAN, Ray, H.
发明人： TAYLOR, Dene, H. , PRUSIK, Thaddeus , SMITH, Dawn, E. , BAUGHMAN, Ray, H.
IPC分类号： G01K3/00
CPC分类号： G01K3/005 , G01K3/04 , G01K11/06 , Y10S252/962
摘要： Freeze indicators providing a visual indication of exposure of the freeze indicator to a freezing or near-freezing temperature and their manufacture are disclosed. The freeze indicators employ colloidal dispersions as active elements and include flexible freeze indicators, freeze indicators protected against drying out and freeze indicators employing core shell composites, for example gold coated pigments as active indicator elements. Also disclosed are: a combination freeze indicator and threshold temperature indicator; a combination threshold indicator and cumulative temperature indicator; and three-way combination indicators that can provide indications of cumulative past temperature exposure, exposure to freezing temperatures and exposure to a temperature above a threshold.
摘要翻译：公开了冻结指示器，其提供了将冷冻指示剂暴露于冷冻或接近冻结温度的视觉指示及其制造。冻结指示剂使用胶体分散体作为活性元素，并且包括柔性冻结指示剂，防止干燥的冷冻指示剂和使用核壳复合材料的冷冻指示剂，例如作为活性指示剂元素的金涂层颜料。还公开了：组合冻结指示器和阈值温度指示器; 组合阈值指标和累积温度指标; 和三路组合指示器，可以提供累积过去的温度暴露，暴露于冷冻温度和暴露于高于阈值的温度的指示。

9. 发明申请

WO2013002748A1 COMPUTING SYSTEMS AND METHODS FOR ELECTRONICALLY INDICATING THE ACCEPTABILITY OF A PRODUCT 审中-公开
标题翻译：电子系统和电子显示产品可接受性的方法
公开(公告)号：WO2013002748A1
公开(公告)日：2013-01-03
申请号：PCT/US2011/001158
申请日：2011-06-28
申请人： TEMPTIME CORPORATION , GRABINER, Fred , LENTZ, Carl M. , MOORE, Emily , PRUSIK, Thaddeus , PURO, Nicholas
发明人： GRABINER, Fred , LENTZ, Carl M. , MOORE, Emily , PRUSIK, Thaddeus , PURO, Nicholas
IPC分类号： G08B1/00
CPC分类号： G06Q10/0838 , G06Q10/0833 , G06Q50/28
摘要： Computing systems and methods for electronically indicating the acceptability of a product. An image capture and communication device may analyze a product label that includes one or more monitors, authentication elements, and identification elements. The image capture and communication device may determine the type and features of the monitors, authentication elements, and identification elements and, based on the type of the monitors, authentication elements, and identification elements. The image capture and communication device may transmit data based on the type and features to a host server, which may transmit data associated with the host product to the image capture and communication device in, inter alia , the form of an acceptability report.
摘要翻译：用于电子指示产品可接受性的计算系统和方法。图像捕获和通信设备可以分析包括一个或多个监视器，认证元件和识别元件的产品标签。图像捕获和通信设备可以基于监视器的类型，认证元件和识别元件来确定监视器，认证元件和识别元件的类型和特征。图像捕获和通信设备可以基于类型和特征将数据发送到主机服务器，主机服务器可以特别地以可接受性报告的形式将与主机产品相关联的数据传送到图像捕获和通信设备。

10. 发明申请

WO2006118820A2 METHOD OF MONITORING MATURING CONSUMABLE PRODUCTS AND PRODUCTS USEFUL THEREIN 审中-公开
标题翻译：监控成品消耗品和有用产品的方法
公开(公告)号：WO2006118820A2
公开(公告)日：2006-11-09
申请号：PCT/US2006/015109
申请日：2006-04-21
申请人： TEMPTIME CORPORATION , PRUSIK, Thaddeus , MARTIN, Jean-paul , GOZLAN, Serge P.
发明人： PRUSIK, Thaddeus , MARTIN, Jean-paul , GOZLAN, Serge P.
IPC分类号： G06Q99/00 , G07G1/14 , G06Q30/00
CPC分类号： G01N31/229 , G06Q30/0241
摘要： A monitoring process for a maturing consumable product, especially one lacking a clear visual indication of maturity or ripeness, e.g. certain pears (26), other fruit, some cheeses, aged beef, sausages and wine, employs a visual indicator (16) responsive to cumulative exposure to temperature, humidity, atmospheric conditions and/or other environmental conditions. The maturity indicator (16) responds by changing its visual appearance, or providing another signal, after elapse of a condition exposure correlated with the conditions anticipated to be required for a desired maturity stage of the maturing product. Optionally the indicator can be incorporated in a label (10) adhered to the maturing product or its package. The maturity indicator (16) can employ various indicator technologies including an active chemical agent, e.g. a polyacetylenic agent, adhesive diffusion technology, an oxidative reaction, a silver salt redox reaction, an enzyme based reaction or an electronic condition exposure indicator. The visual maturity indicator (16) can enable a customer readily to determine the ripeness or maturity of a product (26) without having to handle the product or otherwise physically inspect it.
摘要翻译：成熟消费品的监测过程，特别是缺乏成熟度或成熟度的清晰视觉指示的监测过程。某些梨（26），其他水果，一些奶酪，老年牛肉，香肠和葡萄酒，使用对温度，湿度，大气条件和/或其他环境条件的累积暴露敏感的视觉指示器（16）。成熟度指标（16）通过改变其视觉外观或在经过与成熟期产品的期望成熟期所需的条件相关的条件暴露后提供另一信号来做出响应。任选地，指示剂可以并入粘附到成熟产品或其包装上的标签（10）中。成熟度指标（16）可以采用各种指标技术，包括活性化学试剂，聚乙炔化剂，粘合剂扩散技术，氧化反应，银盐氧化还原反应，基于酶的反应或电子暴露指示剂。视觉成熟度指示器（16）可以使客户容易地确定产品（26）的成熟度或成熟度，而不必处理产品或以其他方式实际检查产品。

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