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1. 发明申请

WO2018024828A1 IMPROVED PROCESS FOR THE PREPARATION OF CARBAMATES 审中-公开
标题翻译：改进的制备氨基甲酸酯的方法
公开(公告)号：WO2018024828A1
公开(公告)日：2018-02-08
申请号：PCT/EP2017/069659
申请日：2017-08-03
申请人： TAMINCO BVBA
发明人： VAN WAES, Frederik , MOONEN, Kristof , ULRICHTS, Dieter
IPC分类号： C07C269/04 , C07C271/20
摘要： A process for the preparation of N-(dialkylaminoalkyl)-carbamic acid esters, in particular (propyl N-[3-(dimethylamino)propyl] carbamate) comprising an oxidative carbonylation reaction of a compound of general structure (II) wherein each of R 1 and R 2 , equal to or different from each other, are independently selected from an alkyl group having 1 to 10 carbon atoms, which is optionally substituted by at least one halogen atom, an aryl group or an aralkyl group; R 3 is selected from an alkyl group having 1 to 36 carbon atoms, which is optionally substituted by at least one halogen atom, an aryl group or an aralkyl group; each of R', R" and R 4 , equal to or different from each other, are independently selected from H, an alkyl group having 1 to 10 carbon atoms, which is optionally substituted by at least one halogen atom, an aryl group or an aralkyl group; and n is an integer in the range from 1 to 8, with a hydroxyl compound of general formula (III), R 3 -OH (III) and in the presence of a catalyst system.
摘要翻译：制备包含一般化合物的氧化羰基化反应的N-（二烷基氨基烷基） - 氨基甲酸酯，特别是（N- [3-（二甲基氨基）丙基]氨基甲酸丙酯）的方法结构（II）其中R 1和R 2中的每一个彼此相同或不同，独立地选自具有1至10个碳原子的烷基，其中任选被至少一个卤素原子，芳基或芳烷基取代; R 3选自具有1至36个碳原子的烷基，其任选被至少一个卤素原子，芳基或芳烷基取代; 每个R'，R“ 和R 4彼此相同或不同，独立地选自H，具有1至10个碳原子的烷基，其任选被至少一个卤素原子取代，芳基或芳烷基; （III）的羟基化合物，R 3 -OH（III）在催化剂体系存在下反应，n为1至8的整数。

2. 发明申请

WO2013098575A1 PROCESS FOR THE PRODUCTION OF CHOLINE HYDROXIDE 审中-公开
标题翻译：生产氢氧化铝的方法
公开(公告)号：WO2013098575A1
公开(公告)日：2013-07-04
申请号：PCT/IB2011/003185
申请日：2011-12-29
申请人： TAMINCO N.V. , MOONEN, Kristof , ULRICHTS, Dieter , SCHELDEMAN, Daan
发明人： MOONEN, Kristof , ULRICHTS, Dieter , SCHELDEMAN, Daan
IPC分类号： C07C213/04
CPC分类号： C07C213/10 , C07C213/04 , C07C215/40
摘要： A continuous process for the production of choline hydroxide includes reacting ethylene oxide, trimethylamine, and water in a reaction zone to form a reaction mixture and extracting heat from the reaction mixture. Subsequently, phase separation of the reaction mixture is induced to obtain a choline hydroxide phase and an organic liquid phase comprising trimethylamine. A choline hydroxide solution (e.g., at a concentration of about 40% to 50% by weight, based on total weight of the choline hydroxide solution) is obtained from the choline hydroxide phase.
摘要翻译：用于生产氢氧化胆碱的连续方法包括在反应区中使环氧乙烷，三甲胺和水反应以形成反应混合物并从反应混合物中提取热量。随后，诱导反应混合物的相分离，得到含有三甲胺的氢氧化胆碱相和有机液相。从氢氧化胆碱相获得氢氧化胆碱溶液（例如浓度为约40％至50％重量，基于氢氧化胆碱溶液的总重量）。

3. 发明申请

WO2015165492A1 METHOD FOR PREPARING AN ANIMAL FEED SUPPLEMENT COMPOSITION 审中-公开
标题翻译：制备动物饲料补充组合物的方法
公开(公告)号：WO2015165492A1
公开(公告)日：2015-11-05
申请号：PCT/EP2014/058631
申请日：2014-04-28
申请人： TAMINCO
发明人： LAUWAERTS, Angelo , ULRICHTS, Dieter , LAGET, Mia
IPC分类号： A23K1/16
CPC分类号： A23K20/28 , A23K10/37 , A23K20/158 , A23K20/174 , A23K40/00 , A23V2002/00 , Y02P60/877 , A23V2250/1878 , A23V2250/304
摘要： The animal feed supplement composition comprises one or more feed supplement substances including at least one choline feed supplement substance. To prepare the feed supplement composition, the particles of a particulate absorbent carrier are allowed to absorb an aqueous solution of the choline feed supplement substance. In accordance with the invention, the absorbent particles are allowed to absorb also at least one medium chain fatty acid feed supplement substance, which may be a salt dissolved in water or a free fatty acid. The absorbent carrier may be an organic carrier, such as corn cob, or an inorganic carrier, in particular a silica material. The combination of the choline feed supplement substance and the medium chain fatty acid feed supplement substance enables to improve the flow properties of the product either in its dry state or after having been exposed to humid conditions. A higher load of active ingredients can also be obtained more easily.
摘要翻译：动物饲料补充剂组合物包含一种或多种包含至少一种胆碱饲料补充物质的饲料补充物质。为了制备饲料补充剂组合物，使颗粒状吸收剂载体的颗粒吸收胆碱饲料补充物质的水溶液。根据本发明，允许吸收性颗粒吸收至少一种中链脂肪酸饲料补充物质，其可以是溶于水或游离脂肪酸的盐。吸收性载体可以是有机载体，例如玉米芯，或无机载体，特别是二氧化硅材料。胆碱饲料补充物质和中链脂肪酸饲料补充物质的组合使得能够在干燥状态下或暴露于潮湿条件之后改善产品的流动性能。还可以更容易地获得更高的活性成分负荷。

4. 发明申请

WO2014167065A1 IMPROVED PROCESS FOR PREPARING CHOLINE HYDROXIDE 审中-公开
标题翻译：用于制备氢氧化铝的改进方法
公开(公告)号：WO2014167065A1
公开(公告)日：2014-10-16
申请号：PCT/EP2014/057294
申请日：2014-04-10
申请人： TAMINCO
发明人： MOONEN, Kristof , ULRICHTS, Dieter , SCHELDEMAN, Daan
IPC分类号： C07C213/04 , C07C215/40 , C07C213/10
CPC分类号： C07C213/04 , C07C213/10 , C07C215/40
摘要： Disclosed is a process for the production of choline hydroxide includes reacting at a temperature above 30.0° C ethylene oxide, trimethylamine, and water in the presence of an aqueous medium in such amounts as to form a diluted choline hydroxide solution having a choline hydroxide concentration of less than 40 wt% and removing at least a portion of the aqueous medium from the diluted choline hydroxide solution to form a concentrated aqueous choline hydroxide solution having a choline hydroxide concentration which is at least 1.05 times the choline hydroxide concentration of the diluted choline hydroxide solution. The process allows for large scale, continuous production of concentrated aqueous choline hydroxide solutions of good quality under economically advantaged consumption factors for ethylene oxide.
摘要翻译：公开了一种生产氢氧化胆碱的方法，包括在水性介质存在下，在高于30.0℃环氧乙烷，三甲胺和水的温度下反应，其量使得形成氢氧化胆碱浓度为小于40重量％，并且从稀释的氢氧化胆碱溶液中除去至少一部分水性介质，以形成氢氧化胆碱浓度的浓缩的胆碱氢氧化物溶液，其浓度为稀释的氢氧化胆碱溶液的胆碱氢氧化物浓度的至少1.05倍。该方法允许在环氧乙烷的经济有利的消耗因子下大规模，连续地生产具有良好质量的浓缩的氢氧化胆碱水溶液。

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